Analysis Tests Standard Results Appearance A white or almost white powder Complies Identification a.
Cas:1134-47-0
Min.Order:1 Gram
FOB Price: $100.0 / 500.0
Type:Trading Company
inquiryBaclofen CAS 1134-47-0 Purity: 99% Min Application: Intermediates Appearance: Powder Package: Bag Delivery: 3-5days Our Advantage & Service 1.Top quality: Using high quality material and establishing a strict quality control system,a
Cas:1134-47-0
Min.Order:1 Kilogram
FOB Price: $10.0 / 50.0
Type:Trading Company
inquiryservice we can provide: 1. mixed container, we can mix different items in one container. 2. quality control, before shipment, free sample for test. after shipment, keep sample for 3 years 3. prompt shipment with professional documents 4. packing as y
Cas:1134-47-0
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquiryDayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:1134-47-0
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
Cas:1134-47-0
Min.Order:1 Metric Ton
FOB Price: $1.0 / 3.0
Type:Manufacturers
inquiryGood quality Competitive price On time delivery Our Advantages: Full experience of large numbers containers loading in main Chinese seaports Packing with pallet as buyer's special request Best service after shipment with e-mail
Cas:1134-47-0
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
We can provide GMP validation service that complies with SFDA, FDA, WHO and EU EMPA.Excellent registration team could help us easlily to register our products in different countries.If you and your customer are interested in some products or need C
Cas:1134-47-0
Min.Order:1 Gram
Negotiable
Type:Manufacturers
inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:1134-47-0
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiry1. ISO 2. IN STOCK 3. FAST REPLY QUALIFED ; EFFICIENCY; RESPONSIBLE Appearance:WHITE POWDER Storage:in cool Package:25kg/drum Application:active pharmaceutical ingredient Transportation:as request Port:any port
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Name:Baclofen CAS NO: 1134-47-0 Grade:Medical scientific research and export Molecular formula:C10H12ClNO2 Molecular weight:213.6608 Product Quality 12 years of chemical raw materials Mature operation of the industry System stability Data
Cas:1134-47-0
Min.Order:25 Kilogram
FOB Price: $1.0 / 2.0
Type:Other
inquiryBaclofen Basic information Product Name: Baclofen Synonyms: -(Aminomethyl)-4-chlorobenzenpropanoicacid;-(p-Chlorophenyl)-aminobutyricacid;ba34647;baclon;beta-(4-chlorophenyl)gaba;beta-(a
Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:1134-47-0
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by email in time prod
Cas:1134-47-0
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:1134-47-0
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:1134-47-0
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryCAS 1134-47-0 Name Baclofen MW 213.66100 MF C10H12ClNO2 Appearance White to very pale yellow solid Appearance:White powde
Appearance:white to very faintly yellow solid Storage:Room temperature Package:25kg/drum Application:Chemicals Transportation:Express/Sea/Air Port:Any port in china
Cas:1134-47-0
Min.Order:25 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryApplications Lithium hydride is used as condensation agent, reducing agent, alkylation reagent and desiccant in organic synthesis, and is also a good hydrogen storage material Advantages: Hubei XinRunde Chemical Co., Ltd is a renowned
Cas:1134-47-0
Min.Order:10 Gram
FOB Price: $1500.0 / 2000.0
Type:Other
inquiryBaclofen CAS:1134-47-0 Name Baclofen Synonyms beta-(Aminomethyl)-4-chlorobenzenepropanoic acid; Lioresal Molecular Structure Molecular Formula C10H12ClNO2
1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:1134-47-0
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryWe are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery
Cas:1134-47-0
Min.Order:10 Gram
FOB Price: $1.45
Type:Trading Company
inquiryProduct Name: Baclofen CAS: 1134-47-0 MF: C10H12ClNO2 MW: 213.66 EINECS: 214-486-9 Mol File: 1134-47-0.mol Baclofen Structure Baclofen Chemical Properties Melting point 208-210°C Boiling point 364.3±32.0 °C(
Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:1134-47-0
Min.Order:1 Kilogram
FOB Price: $421.0 / 485.0
Type:Trading Company
inquiryBeluga chemical professional supply High-quality Baclofen manufacturer 1. Beluga Chemical has a professional RESEARCH and development team and strong technical force to ensure technical support and research capabilities. 2. Made in China and expo
Cas:1134-47-0
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryWe have overseas warehouses in California, New Laredo Mexico, Vancouver Canada, Amsterdam Netherlands, and Melbourne Australia. Overseas warehouses can provide some of the best-selling products. We look forward to the cooperation of local powerful d
Cas:1134-47-0
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryProduct Detail Minimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,
Cas:1134-47-0
Min.Order:20 Metric Ton
Negotiable
Type:Trading Company
inquiry4-amino-3-(4-chlorophenyl)butanoic acid
Conditions | Yield |
---|---|
With hydrogenchloride In water at 130℃; for 24h; Sealed tube; | 97% |
4-amino-3-(4-chlorophenyl)butanoic acid
Conditions | Yield |
---|---|
With sodium L-ascorbate; fluorescein free acid In aq. phosphate buffer for 0.5h; pH=7.4; Irradiation; | 87% |
4-(4-chlorophenyl)pyrrolidin-2-one
4-amino-3-(4-chlorophenyl)butanoic acid
Conditions | Yield |
---|---|
With hydrogenchloride; water In water for 16h; Reflux; | 81% |
With hydrogenchloride for 2h; Heating; | 54% |
Conditions | Yield |
---|---|
With sodium sulfamate; sodium hypobromide at -5 - 55℃; for 2.16667h; | 79.4% |
4-amino-3-(4-chlorophenyl)butanoic acid
Conditions | Yield |
---|---|
With ammonia; hydrogen In water at 25 - 30℃; for 6h; | 70% |
ethyl 4-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-3-(4-chlorophenyl)butanoate
4-amino-3-(4-chlorophenyl)butanoic acid
Conditions | Yield |
---|---|
With hydrogenchloride; hydrazine hydrate In ethanol Heating; | 58% |
4-amino-3-(4-chlorophenyl)butanoic acid
Conditions | Yield |
---|---|
With ammonium hydroxide In methanol at 60℃; for 2h; pH=6.9 - 7; | 41% |
ethyl 3-(4-chlorophenyl)-3-hydroxybutanoate
4-amino-3-(4-chlorophenyl)butanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: 1.) p-toluenesulfonic acid, 2.) 10percent NaOH / 1.) toluene, reflux, 3 h, 2.) reflux, 2 h 2: 37 percent / 1.) N-bromosuccinimide, 2.) NH3 / 1.) CCl4, reflux, 48 h, 2.) THF, 3 h 3: 16 percent / NH3 / tetrahydrofuran / 3 h 4: 65 percent / 1 M NH4OH / 1 h / 70 °C 5: 59 percent / H2, Raney nickel W-5 / ethanol / 16 h / 3040 Torr / Ambient temperature 6: 54 percent / 6 M HCl / 2 h / Heating View Scheme | |
Multi-step reaction with 6 steps 1: 1.) p-toluenesulfonic acid, 2.) 10percent NaOH / 1.) toluene, reflux, 3 h, 2.) reflux, 2 h 2: 37 percent / N-bromosuccinimide / CCl4 / 48 h / Heating 3: 16 percent / NH3 / tetrahydrofuran / 3 h 4: 65 percent / 1 M NH4OH / 1 h / 70 °C 5: 59 percent / H2, Raney nickel W-5 / ethanol / 16 h / 3040 Torr / Ambient temperature 6: 54 percent / 6 M HCl / 2 h / Heating View Scheme |
(E)-3-(4-chlorophenyl)but-2-enoic acid
4-amino-3-(4-chlorophenyl)butanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 37 percent / 1.) N-bromosuccinimide, 2.) NH3 / 1.) CCl4, reflux, 48 h, 2.) THF, 3 h 2: 16 percent / NH3 / tetrahydrofuran / 3 h 3: 65 percent / 1 M NH4OH / 1 h / 70 °C 4: 59 percent / H2, Raney nickel W-5 / ethanol / 16 h / 3040 Torr / Ambient temperature 5: 54 percent / 6 M HCl / 2 h / Heating View Scheme | |
Multi-step reaction with 5 steps 1: 37 percent / N-bromosuccinimide / CCl4 / 48 h / Heating 2: 16 percent / NH3 / tetrahydrofuran / 3 h 3: 65 percent / 1 M NH4OH / 1 h / 70 °C 4: 59 percent / H2, Raney nickel W-5 / ethanol / 16 h / 3040 Torr / Ambient temperature 5: 54 percent / 6 M HCl / 2 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1: 240 g / Zn / benzene / Heating 2: 1.) p-toluenesulfonic acid, 2.) 10percent NaOH / 1.) toluene, reflux, 3 h, 2.) reflux, 2 h 3: 37 percent / 1.) N-bromosuccinimide, 2.) NH3 / 1.) CCl4, reflux, 48 h, 2.) THF, 3 h 4: 16 percent / NH3 / tetrahydrofuran / 3 h 5: 65 percent / 1 M NH4OH / 1 h / 70 °C 6: 59 percent / H2, Raney nickel W-5 / ethanol / 16 h / 3040 Torr / Ambient temperature 7: 54 percent / 6 M HCl / 2 h / Heating View Scheme | |
Multi-step reaction with 7 steps 1: 240 g / Zn / benzene / Heating 2: 1.) p-toluenesulfonic acid, 2.) 10percent NaOH / 1.) toluene, reflux, 3 h, 2.) reflux, 2 h 3: 37 percent / N-bromosuccinimide / CCl4 / 48 h / Heating 4: 16 percent / NH3 / tetrahydrofuran / 3 h 5: 65 percent / 1 M NH4OH / 1 h / 70 °C 6: 59 percent / H2, Raney nickel W-5 / ethanol / 16 h / 3040 Torr / Ambient temperature 7: 54 percent / 6 M HCl / 2 h / Heating View Scheme |
4-(4-chlorophenyl)-1,5-dihydro-2H-pyrrol-2-one
4-amino-3-(4-chlorophenyl)butanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 59 percent / H2, Raney nickel W-5 / ethanol / 16 h / 3040 Torr / Ambient temperature 2: 54 percent / 6 M HCl / 2 h / Heating View Scheme |
(Z)-4-amino-3-(4-chlorophenyl)but-2-enoic acid
4-amino-3-(4-chlorophenyl)butanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 65 percent / 1 M NH4OH / 1 h / 70 °C 2: 59 percent / H2, Raney nickel W-5 / ethanol / 16 h / 3040 Torr / Ambient temperature 3: 54 percent / 6 M HCl / 2 h / Heating View Scheme |
(Z)-4-Bromo-3-(4-chloro-phenyl)-but-2-enoic acid
4-amino-3-(4-chlorophenyl)butanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 16 percent / NH3 / tetrahydrofuran / 3 h 2: 65 percent / 1 M NH4OH / 1 h / 70 °C 3: 59 percent / H2, Raney nickel W-5 / ethanol / 16 h / 3040 Torr / Ambient temperature 4: 54 percent / 6 M HCl / 2 h / Heating View Scheme |
4-amino-3-(4-chlorophenyl)butanoic acid
Conditions | Yield |
---|---|
With hydrogenchloride In water Cooling with ice; |
4-amino-3-(4-chlorophenyl)butanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: acetic acid / chloroform / 1 h / 0 - 20 °C 1.2: 20 °C 2.1: trifluoroacetic acid / 1,2-dichloro-ethane / 2 h / 80 °C 3.1: nickel dichloride; sodium tetrahydroborate / methanol; tetrahydrofuran / 1 h / 0 - 20 °C 4.1: hydrogenchloride; water / water / 16 h / Reflux View Scheme |
4-amino-3-(4-chlorophenyl)butanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: trifluoroacetic acid / 1,2-dichloro-ethane / 2 h / 80 °C 2: nickel dichloride; sodium tetrahydroborate / methanol; tetrahydrofuran / 1 h / 0 - 20 °C 3: hydrogenchloride; water / water / 16 h / Reflux View Scheme |
4-amino-3-(4-chlorophenyl)butanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: nickel dichloride; sodium tetrahydroborate / methanol; tetrahydrofuran / 1 h / 0 - 20 °C 2: hydrogenchloride; water / water / 16 h / Reflux View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: cesium fluoride; tetrabutyl-ammonium chloride; bis-triphenylphosphine-palladium(II) chloride / toluene; water / 18 h / 20 °C / Inert atmosphere 2.1: acetic acid / chloroform / 1 h / 0 - 20 °C 2.2: 20 °C 3.1: trifluoroacetic acid / 1,2-dichloro-ethane / 2 h / 80 °C 4.1: nickel dichloride; sodium tetrahydroborate / methanol; tetrahydrofuran / 1 h / 0 - 20 °C 5.1: hydrogenchloride; water / water / 16 h / Reflux View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: potassium tert-butylate / toluene; methanol / 0.5 h / 20 °C / 4500.45 Torr / Inert atmosphere 1.2: 0.11 h / 25 °C / 4500.45 Torr / Inert atmosphere 2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 50 °C / 6000.6 Torr 3.1: lithium hydroxide; water / toluene / 1 h / 50 °C / 3750.38 Torr 4.1: hydrogen / methanol / 60 °C / 45004.5 Torr View Scheme | |
Multi-step reaction with 5 steps 1: diammonium phosphate / water / 5 h / 15 - 20 °C 2: potassium hydroxide / 2 h / 85 - 90 °C 3: urea / 1 h / 130 - 140 °C 4: sodium hydroxide / water / 1.5 h / 65 - 70 °C 5: sodium hypobromide; sodium sulfamate / 2.17 h / -5 - 55 °C View Scheme |
methyl 4-chlorocinnamate
4-amino-3-(4-chlorophenyl)butanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 50 °C / 6000.6 Torr 2: lithium hydroxide; water / toluene / 1 h / 50 °C / 3750.38 Torr 3: hydrogen / methanol / 60 °C / 45004.5 Torr View Scheme |
methyl (+/-)-3-(4-chlorophenyl)-4-nitrobutanoate
4-amino-3-(4-chlorophenyl)butanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: lithium hydroxide; water / toluene / 1 h / 50 °C / 3750.38 Torr 2: hydrogen / methanol / 60 °C / 45004.5 Torr View Scheme |
(+/-)-4-nitro-3-(4-chloro)butanoic acid
4-amino-3-(4-chlorophenyl)butanoic acid
Conditions | Yield |
---|---|
With hydrogen In methanol at 60℃; under 45004.5 Torr; | 493 mg |
2-(4-chlorophenylmethylene)acetoacetic acid ethyl ester
4-amino-3-(4-chlorophenyl)butanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: potassium hydroxide / 2 h / 85 - 90 °C 2: urea / 1 h / 130 - 140 °C 3: sodium hydroxide / water / 1.5 h / 65 - 70 °C 4: sodium hypobromide; sodium sulfamate / 2.17 h / -5 - 55 °C View Scheme |
3-(4-chlorophenyl)pentane-1,5-dioic acid
4-amino-3-(4-chlorophenyl)butanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: urea / 1 h / 130 - 140 °C 2: sodium hydroxide / water / 1.5 h / 65 - 70 °C 3: sodium hypobromide; sodium sulfamate / 2.17 h / -5 - 55 °C View Scheme |
Conditions | Yield |
---|---|
With thionyl chloride at 0 - 80℃; for 5h; | 99% |
With hydrogenchloride at 20℃; for 24h; |
Conditions | Yield |
---|---|
With hydrogenchloride at 105℃; for 0.5h; | 98% |
With hydrogenchloride at 20℃; for 24h; |
Conditions | Yield |
---|---|
With thionyl chloride for 0.5h; Ambient temperature; | 98% |
With thionyl chloride | 95% |
With hydrogenchloride | 89% |
With hydrogenchloride at 20℃; for 24h; |
4-amino-3-(4-chlorophenyl)butanoic acid
4-(4-chlorophenyl)pyrrolidin-2-one
Conditions | Yield |
---|---|
With aluminum oxide In toluene for 16h; Heating / reflux; | 90% |
With aluminum oxide In toluene for 5h; Heating; | 88% |
With silica gel In toluene for 6h; Heating; | 85% |
2-chloroethyl isothiocyanate
4-amino-3-(4-chlorophenyl)butanoic acid
3-(4-chlorophenyl)-4-[3-(2-chloroethyl)ureido]butyric acid
Conditions | Yield |
---|---|
With sodium hydroxide for 1h; Ambient temperature; | 89% |
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In ethanol at 60℃; for 0.75h; | 84% |
di-tert-butyl dicarbonate
4-amino-3-(4-chlorophenyl)butanoic acid
4-((tert-butoxycarbonyl)amino)-3-(4-chlorophenyl)butanoic acid
Conditions | Yield |
---|---|
Stage #1: di-tert-butyl dicarbonate; 4-amino-3-(4-chlorophenyl)butanoic acid With sodium hydroxide; water In 1,4-dioxane at 0 - 20℃; for 4h; Stage #2: With citric acid In 1,4-dioxane; water pH=3; | 84% |
cis,trans-2,5-dimethoxytetrahydrofuran
4-amino-3-(4-chlorophenyl)butanoic acid
3-(4-chlorophenyl)-4-pyrrol-1-ylbutyric acid
Conditions | Yield |
---|---|
With acetic acid for 1h; Heating; | 82% |
With acetic acid Clauson-Kaas reaction; |
Conditions | Yield |
---|---|
With sulfur; 1-dodecylthiol In N,N-dimethyl-formamide at 20℃; for 2h; Sealed tube; chemoselective reaction; | 76% |
Conditions | Yield |
---|---|
With sodium hydroxide for 1h; Ambient temperature; | 75% |
4-amino-3-(4-chlorophenyl)butanoic acid
ethyl isocyanate
3-(4-chlorophenyl)-4-(3-ethylureido)butyric acid
Conditions | Yield |
---|---|
With sodium hydroxide Addition; | 74% |
With sodium hydroxide for 1h; Ambient temperature; | 45% |
Conditions | Yield |
---|---|
With sodium hydroxide for 1h; Ambient temperature; | 63% |
2-oxoheptadecanoic acid
4-amino-3-(4-chlorophenyl)butanoic acid
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide In water; N,N-dimethyl-formamide at 20℃; for 1h; Sealed tube; Darkness; chemoselective reaction; | 61% |
octanol
4-amino-3-(4-chlorophenyl)butanoic acid
A
1-Chlorooctane
B
4-Amino-3-(4-chloro-phenyl)-butyric acid octyl ester; hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride at 130℃; | A n/a B 54% |
4-amino-3-(4-chlorophenyl)butanoic acid
2,4,6-triphenylpyrylium tetrafluoroborate
Conditions | Yield |
---|---|
In ethanol at 85 - 90℃; for 4h; Schlenk technique; | 54% |
4-amino-3-(4-chlorophenyl)butanoic acid
trifluoroacetic anhydride
A
4-(4-chlorophenyl)pyrrolidin-2-one
B
3-(4-chlorophenyl)-4-(2,2,2-trifluoroacetylamino)-butyric acid
Conditions | Yield |
---|---|
In diethyl ether at 20℃; for 0.5h; Friedel-Crafts cyclization; | A 42% B 38% |
4-amino-3-(4-chlorophenyl)butanoic acid
Conditions | Yield |
---|---|
Stage #1: 6-bromo-3-methyl-2-phenylquinoline-4-carboxylic acid With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; for 0.5h; Stage #2: 4-amino-3-(4-chlorophenyl)butanoic acid In N,N-dimethyl-formamide at 60℃; for 3h; | 41% |
Conditions | Yield |
---|---|
With sodium hydroxide for 1h; Ambient temperature; | 40% |
2,5-dioxopyrrolidin-1-yl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl carbonate
4-amino-3-(4-chlorophenyl)butanoic acid
Conditions | Yield |
---|---|
With potassium carbonate In water; N,N-dimethyl-formamide Inert atmosphere; | 38.4% |
4-amino-3-(4-chlorophenyl)butanoic acid
3,5-dinitrobenzoic anhydride
Conditions | Yield |
---|---|
With pyridine; dmap In acetonitrile at 20℃; for 0.25h; |
Conditions | Yield |
---|---|
With hydrogenchloride at 20℃; for 24h; |
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