CAS No.124-09-4,Hexamethylenediamine Suppliers,MSDS download

Dayang Chem (Hangzhou) Co.,Ltd.

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Henan Allgreen Chemical Co.,Ltd

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Ality Chemical Corporation

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Henan Tianfu Chemical Co., Ltd.

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Henan Sinotech Import&Export Corporation

CAS 124-09-4 EINECS 204-679-6 Other Names 1,6-hexylenediamine MF C6H16N2

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Changchun Artel lmport and Export trade company

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1,6-Hexanediamine CAS NO.124-09-4

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Hangzhou Keyingchem Co.,Ltd

High qualityHangzhou Keying Chem Co., Ltd. Is a comprehensive enterprise, dedicated to the development, production and marketing of chemicals. As a technology innovative and service professional enterprise, Our company mainly engages in global phar

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Hangzhou Fandachem Co.,Ltd

Hangzhou Fanda Chemical Co.,Ltd (FandaChem) , a China-based chemical company, specialize in exporting 1,6-Diaminohexane cas:124-09-4;Please contact us by email freely. We are leading exporter in China. If you really need this cargo, pl

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SHANGHAI T&W PHARMACEUTICAL CO., LTD.

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Hangzhou J&H Chemical Co., Ltd.

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Zibo Hangyu Biotechnology Development Co., Ltd

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HANGZHOU YUNUO CHEMICAL CO.,LTD

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Zibo Dorne chemical technology co. LTD

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Henan Wentao Chemical Product Co., Ltd.

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Hangzhou Huarong Pharm Co., Ltd.

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Hangzhou Zhongqi chem Co.,Ltd.

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Kono Chem Co.,Ltd

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GIHI CHEMICALS CO.,LIMITED

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Hunan chemfish Pharmaceutical co.,Ltd

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Zhuozhou Wenxi import and Export Co., Ltd

Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard

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Antimex Chemical Limied

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Hunan Russell Chemicals Technology Co.,Ltd

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Hubei Langyou International Trading Co., Ltd

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Hunan Longxianng Runhui Trading Co.,Ltd

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Amadis Chemical Co., Ltd.

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HENAN SUNLAKE ENTERPRISE CORPORATION

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Synthetic route

RuHCl(H2)(PCy3)2: RuHCl(H2)(PCy3)2

: 111-69-3
hexanedinitrile

: 2797-51-5
quinoclamine

: 124-09-4
1,6-Hexanediamine

Conditions

Conditions	Yield
In N-butylamine	100%

...Expand

: 111-69-3
hexanedinitrile

A: 111-49-9
hexamethylene imine

B: 124-09-4
1,6-Hexanediamine

Conditions

Conditions	Yield
With hydrogen; Ni(NO3)2, Cu(NO3)2, Cr(NO3)3, Na2CO3; calcined at 380 deg C for 18 h; pretreatment is given in full text In 1,2,4-Trimethylbenzene; ammonia at 80℃; for 24h; Product distribution / selectivity;	A 1.1% B 97%
With hydrogen; Ni(NO3)2, Cu(NO3)2, Cr(NO3)3, Na2CO3; calcined at 380 deg C for 18 h In 1,2,4-Trimethylbenzene; ammonia at 80℃; for 24h; Product distribution / selectivity;	A 1.3% B 90.1%
With ammonium hydroxide; hydrogen In water; isopropyl alcohol at 130℃; under 41254.1 Torr; for 4h; Autoclave;	A 9% B 90%
With hydrogen; iron catalyst at 140℃; under 233483 Torr;

: 1080571-11-4
C6H16N2*C7H16N2O2

: 124-09-4
1,6-Hexanediamine

Conditions

Conditions	Yield
With 2,5-dimethyl-2-ethyl hexanoic acid In water at 120 - 180℃; for 2h; Product distribution / selectivity;	95%

: 58491-62-6
furan-2,5-dicarbonitrile

: 124-09-4
1,6-Hexanediamine

Conditions

Conditions	Yield
With hydrogen; titanium(IV) oxide; platinum In ethanol at 100℃; under 7500.75 Torr; for 4h;	95%

: 111-69-3
hexanedinitrile

: 124-09-4
1,6-Hexanediamine

Conditions

Conditions	Yield
With sodium tetrahydroborate; nickel; sodium hydroxide In methanol; water at 30 - 60℃;	90%
With hydrogen In ethanol at 75℃; under 1500.15 - 15001.5 Torr; for 3h;	80%
With ammonia; hydrogen In toluene at 120℃; under 22502.3 Torr; for 16h; Autoclave;	75%

: 13028-54-1
1,6-diazidohexane

: 124-09-4
1,6-Hexanediamine

Conditions

Conditions	Yield
With aluminum oxide; potassium hydroxide; hydrazine In neat (no solvent) for 1h; Milling;	90%

: 1072-21-5
hexanedial

: 124-09-4
1,6-Hexanediamine

Conditions

Conditions	Yield
With ammonia; hydrogen In methanol at -5 - 0℃; under 41254.1 Torr; for 0.5h; Pressure; Temperature; Autoclave;	82%
With Co-doped zirconium dioxide; ammonia; hydrogen; N-butylamine In methanol at 119.84℃; for 10h; Autoclave; chemoselective reaction;	63%

: 629-11-8
1,6-hexanediol

: 124-09-4
1,6-Hexanediamine

Conditions

Conditions	Yield
Stage #1: 1,6-hexanediol With chlorocarbonylhydrido[4,5-bis(dicyclohexylphosphinomethyl)acridine]ruthenium(II); ammonia In toluene at 0℃; under 3750.38 Torr; for 1h; Autoclave; Stage #2: In toluene at 155℃; for 16h; Autoclave;	81%
With ammonium hydroxide; 4.04 wt.% ruthenium and 0.7 wt.% rhenium on carbon; ammonia at 160℃; under 5175.52 - 35253.5 Torr; for 3h; Reagent/catalyst; Inert atmosphere;	23.4%
With ammonia at 220 - 260℃;

: 111-69-3
hexanedinitrile

A: 124-09-4
1,6-Hexanediamine

B: 2432-74-8
1-amino-5-cyanopentane

Conditions

Conditions	Yield
With Rh/Al2O3; hydrogen In ethanol at 80℃; for 6h;	A 24.4% B 75.6%
With hydrogen; active elemental iron component In ammonia at 70 - 220℃; under 75007.5 - 300030 Torr;
Stage #1: hexanedinitrile With potassium hydroxide; hydrogen; nickel at 50℃; under 15001.5 Torr; Stage #2: With phosphoric acid Purification / work up;

: C-(6-Methoxy-2-p-tolyl-quinolin-4-yl)-N-[6-(6-methoxy-2-p-tolyl-quinolin-4-ylmethanesulfonylamino)-hexyl]-methanesulfonamide

A: 124-09-4
1,6-Hexanediamine

B: 117839-37-9
6-methoxy-2-(p-tolyl)quinoline

C: 117839-39-1
6-methoxy-4-methyl-2-(p-tolyl)quinoline

Conditions

Conditions	Yield
In isopropyl alcohol Irradiation; 350 nm;	A 32% B n/a C n/a

...Expand

: 629-11-8
1,6-hexanediol

A: 111-49-9
hexamethylene imine

B: 124-09-4
1,6-Hexanediamine

C: 4048-33-3
6-amino-1-hexanol

Conditions

Conditions	Yield
With ammonia; hydrogen In water at 180℃; under 7500.75 - 27752.8 Torr; for 4h; Reagent/catalyst; Solvent; Pressure; Time;	A 19.5% B 23.4% C 17%
With ammonia; chlorocarbonylhydrido[4,5-bis(dicyclohexylphosphinomethyl)acridine]ruthenium(II) In toluene at 155℃; under 25502.6 Torr; for 12h; Autoclave; Inert atmosphere;
With ammonia; hydrogen In tert-butyl alcohol at 220℃; under 120012 Torr; for 6h; Kinetics; Reagent/catalyst;	A 66.5 %Chromat. B 21.2 %Chromat. C 6.5 %Chromat.
With ammonia; hydrogen In tert-butyl alcohol at 220℃; under 120012 Torr; for 6h; Kinetics; Reagent/catalyst;	A 7.5 %Chromat. B 17.6 %Chromat. C 68.8 %Chromat.
With ammonia; hydrogen In tert-butyl alcohol at 220℃; under 120012 Torr; for 6h; Kinetics;	A 23 %Chromat. B 31.3 %Chromat. C 19.1 %Chromat.

...Expand

: 111-69-3
hexanedinitrile

A: 124-09-4
1,6-Hexanediamine

B: 2432-74-8
1-amino-5-cyanopentane

C: 2321-76-8
2-iminocyclopentanecarbonitrile

Conditions

Conditions	Yield
With potassium hydroxide; hydrogen; nickel at 50℃; under 15001.5 Torr; Purification / work up;	A n/a B n/a C 12%

...Expand

: 105-60-2
caprolactam

A: 111-49-9
hexamethylene imine

B: 124-09-4
1,6-Hexanediamine

Conditions

Conditions	Yield
With 1,4-dioxane; barium copper chromite at 260℃; under 147102 Torr; Hydrogenation;

: 105-60-2
caprolactam

: 124-09-4
1,6-Hexanediamine

Conditions

Conditions	Yield
With nickel kieselguhr; ammonia at 200℃; under 147102 Torr; Hydrogenation;
Multi-step reaction with 4 steps 1: sodium hydroxide; water / 3 h / 130 °C 2: tetrahydrofuran / 10 h / 70 °C 3: phosphoric acid; ammonia / 6.5 h / 140 - 280 °C 4: potassium hydroxide; hydrogen; palladium on activated charcoal / ethanol / 75 - 80 °C / 11251.1 Torr View Scheme
Multi-step reaction with 4 steps 1: sodium hydroxide; water / 3 h / 130 °C 2: 2 h / 20 °C 3: phosphorus pentoxide; ammonia / 9.5 h / 140 - 280 °C 4: potassium hydroxide; hydrogen; palladium on activated charcoal / ethanol / 75 - 90 °C / 11251.1 Torr View Scheme
Multi-step reaction with 5 steps 1: sodium hydroxide; water / 3 h / 130 °C 2: 2 h / 47 °C 3: phosphoric acid; ammonia / 5.5 h / 140 - 270 °C 4: potassium hydroxide; hydrogen / ethanol / 75 - 85 °C / 11251.1 Torr 5: ethanol; sodium hydroxide / 2 h / Reflux View Scheme

: 111-49-9
hexamethylene imine

: 124-09-4
1,6-Hexanediamine

Conditions

Conditions	Yield
With ammonia; hydrogen; nickel at 200℃; unter Druck;
With Isopropylbenzene; ammonia In water

: 100-64-1
Cyclohexanone oxime

: 124-09-4
1,6-Hexanediamine

Conditions

Conditions	Yield
With silicic acid pumice stone; ammonia; cobalt at 190℃; Hydrogenation;
With silicic acid pumice stone; ammonia; copper at 190℃; Hydrogenation;
With silicic acid pumice stone; ammonia; nickel at 190℃; Hydrogenation;

: 84211-42-7
2,7-diaminooctanedioic acid

: 124-09-4
1,6-Hexanediamine

Conditions

Conditions	Yield
bei der trocknen Destillation;
bei der trocknen Destillation;

: 642470-70-0
N-(5-cyano-pentyl)-benzamide

: 124-09-4
1,6-Hexanediamine

Conditions

Conditions	Yield
durch Reduktion und Verseifung;

: 10513-98-1
1,6-bis-(N-phthalimido)hexane

: 124-09-4
1,6-Hexanediamine

Conditions

Conditions	Yield
With hydrogenchloride at 180 - 190℃;

: 110-83-8
cyclohexene

: 124-09-4
1,6-Hexanediamine

Conditions

Conditions	Yield
With methanol; ozone at -80℃; anschl. Hydrieren des mit NH3 versetzten Reaktionsgemisches an einem Kobalt-Katalysator bei 50grad/200 at;
With ozone; isopropyl alcohol at -80℃; anschl. Hydrieren des mit NH3 versetzten Reaktionsgemisches an einem Kobalt-Katalysator bei 50grad/200 at;
Multi-step reaction with 3 steps 1: dihydrogen peroxide; phosphoric acid; sodium tungstate; hydrogenchloride; 1-hexadecyl-3-methyl-3H-imidazol-1-ium; bromide / water / 4 h / 70 °C 2: sodium periodate; silica gel / dichloromethane / 2 h / 40 °C / Reflux 3: ammonia; hydrogen / methanol / 0.5 h / -5 - 0 °C / 41254.1 Torr / Autoclave View Scheme

: 592-42-7
1,5-Hexadien

: 124-09-4
1,6-Hexanediamine

Conditions

Conditions	Yield
With sodium hypochlorite; dimethylborane; ammonia 2.) 0 deg C, 10 min; Yield given. Multistep reaction;

: 111-69-3
hexanedinitrile

A: 111-49-9
hexamethylene imine

B: 124-09-4
1,6-Hexanediamine

C: 2432-74-8
1-amino-5-cyanopentane

Conditions

Conditions	Yield
With hydrogen; aluminum oxide; nickel at 169.9℃; under 760 Torr; Product distribution; varying space velocity of catalysts;
With hydrogen; nickel monophosphide; silica gel In ethanol at 199.85℃; under 760 Torr; Product distribution; Further Variations:; Catalysts;	A 16 % Chromat. B 65 % Chromat. C 19 % Chromat.
With potassium hydroxide; hydrogen; [Ni0.60Mg0.15Al0.25(OH)2](CO32-)0.09(NO3-)0.18 at 79.85℃; under 18751.5 Torr; Product distribution; Further Variations:; Catalysts; Reagents; Temperatures;

...Expand

: 89333-68-6
6-bis(trimethylsilyl)amino-1-hexene

: 124-09-4
1,6-Hexanediamine

Conditions

Conditions	Yield
With sodium hypochlorite; dimethylborane; ammonia 1.) 0 deg C, 1 h, 2.) O deg C; Yield given. Multistep reaction;

: 121511-53-3
N,N'-Bis-[1-(4-hexadecyloxy-phenyl)-meth-(E)-ylidene]-hexane-1,6-diamine

A: 124-09-4
1,6-Hexanediamine

B: 59117-18-9
p-n-hexadecyloxybenzaldehyde

Conditions

Conditions	Yield
With hydrogenchloride; water; cetyltrimethylammonim bromide In chloroform at 25℃; Rate constant;
With 2-methyl-propan-1-ol; sulfuric acid; sodium dodecyl-sulfate In hexane; water at 27℃; Kinetics;

: 121511-46-4
N,N'-Bis-[1-(2-hexadecyloxy-phenyl)-meth-(E)-ylidene]-hexane-1,6-diamine

A: 124-09-4
1,6-Hexanediamine

B: 5376-76-1
o-(hexadecyloxy)benzaldehyde

Conditions

Conditions	Yield
With hydrogenchloride; water; cetyltrimethylammonim bromide In chloroform at 25℃; Rate constant;
With 2-methyl-propan-1-ol; sulfuric acid; sodium dodecyl-sulfate In hexane; water at 27℃; Kinetics;

: C7H16N2S2*H(1+)

A: 75-15-0
carbon disulfide

B: 124-09-4
1,6-Hexanediamine

Conditions

Conditions	Yield
With buffer In water at 25℃; Rate constant; Mechanism; SIE;

ε-benzoylamino-caproic acid nitrile: ε-benzoylamino-caproic acid nitrile

: 124-09-4
1,6-Hexanediamine

Conditions

Conditions	Yield
With ethanol; sodium anschl. mit Benzoylchlorid und Erhitzen mit HCl auf 170-180grad;
With ethanol; sodium anschl. mit Benzoylchlorid und Erhitzen mit HCl auf 170-180grad;

1.4-dicyano-buten-(1 or 2): 1.4-dicyano-buten-(1 or 2)

: 124-09-4
1,6-Hexanediamine

Conditions

Conditions	Yield
With tetrahydrofuran; nickel Fuller's earth-catalyst; ammonia at 110 - 120℃; under 36775.4 Torr; Hydrogenation;
With methanol; ammonia; cobalt at 60 - 80℃; under 110326 Torr; Hydrogenation;

: 107-10-8
propylamine

: 7722-84-1
dihydrogen peroxide

: iron(II) sulfate

: 124-09-4
1,6-Hexanediamine

...Expand

: 124-09-4
1,6-Hexanediamine

: 111-49-9
hexamethylene imine

Conditions

Conditions	Yield
	100%
MnZSM-5(30) zeolite In water at 400℃; Cyclization;	95.6%
With tris(triphenylphosphine)ruthenium(II) chloride In diphenylether at 180℃; for 5h;	78%

: 124-09-4
1,6-Hexanediamine

: 3029-19-4
pyrene-1-aldehyde

: N,N'-Bis-[1-pyren-1-yl-meth-(E)-ylidene]-hexane-1,6-diamine

Conditions

Conditions	Yield
In methanol	100%
In toluene for 3h; Heating;	93%

: 124-09-4
1,6-Hexanediamine

: 150785-44-7
N,N'-bis(tert-butoxycarbonyl)-N-(γ,γ-dimethylallyl)-S-methylisothiourea

: 623580-13-2
N-(γ,γ-dimethylallyl)-N,N'-bis-(tert-butoxycarbonyl)-N''-(6-aminohexyl)-guanidine

Conditions

Conditions	Yield
In tetrahydrofuran at 50℃; for 3h;	100%
In tetrahydrofuran; water at 50℃; for 1h;	72%
In tetrahydrofuran

: 124-09-4
1,6-Hexanediamine

: 2483-46-7
Boc-Lys(Boc)-OH

: Boc-L-Lys(Boc)-NH(CH2)6NH2

Conditions

Conditions	Yield
With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; benzotriazol-1-ol at 20℃; for 1h; Acylation;	100%

: 124-09-4
1,6-Hexanediamine

: 1571-08-0
methyl 4-formylbenzoate

: 106872-64-4
1,6-bis(4-methoxycarbonylbenzylidene)hexanediamine

Conditions

Conditions	Yield
In toluene for 0.5h; Condensation; Heating;	100%
In toluene for 1h; Reflux; Dean-Stark trap;	100%

: 124-09-4
1,6-Hexanediamine

N-carboxyethylchitin ethyl ester; Mn=12000, Mw=49000, degree of CO2Et substitution per sugar unit =1.17: N-carboxyethylchitin ethyl ester; Mn=12000, Mw=49000, degree of CO2Et substitution per sugar unit =1.17

N-carboxyethylchitin 6-aminohexylamide: N-carboxyethylchitin 6-aminohexylamide

Conditions

Conditions	Yield
In ethanol; water at 70℃; for 24h;	100%

: 124-09-4
1,6-Hexanediamine

: 24424-99-5
di-tert-butyl dicarbonate

: 16644-54-5
N,N'-bis(tert-butoxycarbonyl)-1,6-hexanediamine

Conditions

Conditions	Yield
Stage #1: 1,6-Hexanediamine With triethylamine at 20℃; for 0.5h; Inert atmosphere; Stage #2: di-tert-butyl dicarbonate at 20℃; for 12h; Inert atmosphere;	100%
In methanol at 20℃; for 1h;	91%
With succinimidinium N-sulfonic acid hydrogen sulfate In neat (no solvent) at 20℃; for 0.25h; Green chemistry;	89%
In 1,4-dioxane at 20℃; for 48h;
With hydrogenchloride In methanol at 0 - 20℃;

: 124-09-4
1,6-Hexanediamine

: 1173-43-9
fluoresceinyl 5-isothiocyanate

: 5-(3-(6-aminohexyl)thioureido)-2-(3-hydroxy-6-oxo-6H-xanthen-9-yl)benzoic acid

Conditions

Conditions	Yield
With triethylamine In methanol; N,N-dimethyl-formamide at 20℃; for 6h;	100%

: 124-09-4
1,6-Hexanediamine

: 886448-06-2
C12H21NO2

: 297748-90-4
N,N'-bis[1-n-propoxy-2,2,6,6-tetramethylpiperidin-4-yl]hexane-1,6-diamine

Conditions

Conditions	Yield
With hydrogen; platinum on carbon In ethanol at 100℃; under 37503.8 Torr;	100%

: 124-09-4
1,6-Hexanediamine

hexamethylaminediamine: hexamethylaminediamine

: 111-49-9
hexamethylene imine

Conditions

Conditions	Yield
	100%

: 124-09-4
1,6-Hexanediamine

: 1737-93-5
3,5-dichloro-2,4,6-trifluoropyridine

: 54981-54-3
N-(3,5-Dichlor-2,6-difluor-4-pyridyl)-hexan-1,6-diamin

Conditions

Conditions	Yield
In methanol; ethanol excess of alkyldiamine in CH3OH, 50 - 70 °C, 20 min stirring;;	100%
In methanol; ethanol

: 124-09-4
1,6-Hexanediamine

: 322474-21-5
N,N'-bis-Boc-S-methyl-isothiourea

: 623580-13-2
N-(γ,γ-dimethylallyl)-N,N'-bis-(tert-butoxycarbonyl)-N''-(6-aminohexyl)-guanidine

Conditions

Conditions	Yield
In tetrahydrofuran at 50℃; for 3h;	100%

: 124-09-4
1,6-Hexanediamine

: 590-86-3
isovaleraldehyde

: 78987-59-4
C16H36N2

Conditions

Conditions	Yield
With sodium tetrahydroborate In ethanol for 24h;	100%

: 124-09-4
1,6-Hexanediamine

: C34H47NO6

: C34H58N2O3

Conditions

Conditions	Yield
In dichloromethane	100%

: 124-09-4
1,6-Hexanediamine

: 598-21-0
2-Bromoacetyl bromide

: 6722-88-9
N,N′-(hexane-1,6-diyl) bis(2-bromoethanamide)

Conditions

Conditions	Yield
With potassium carbonate In dichloromethane; water at 5 - 20℃; for 12h;	100%
With potassium carbonate In chloroform; water at 5 - 20℃; for 24.5h;	99%
In chloroform; water at 5℃; for 2h;

: 124-09-4
1,6-Hexanediamine

: 617-09-4
di-o-tolyl carbonate

: 6030-54-2
1,6-bis(methoxycarbonylamino)hexane

Conditions

Conditions	Yield
With hydrogenchloride In methanol	99.9%

: 124-09-4
1,6-Hexanediamine

: 2050-95-5
diisoamyl carbonate

: 16644-34-1
N,N'-hexanediyl-bis-carbamic acid bis(3-methylbutyl) ester

Conditions

Conditions	Yield
With sodium methylate In methanol at 80℃; Product distribution / selectivity; Industry scale;	99.7%
With sodium methylate In methanol at 80℃; Product distribution / selectivity; Inert atmosphere;
With sodium methylate In methanol at 80℃; Product distribution / selectivity; Inert atmosphere;
With sodium methylate In methanol at 80℃; Product distribution / selectivity; Inert atmosphere;
With sodium methylate In methanol at 80℃; Product distribution / selectivity;	99.7 %Chromat.

: 124-09-4
1,6-Hexanediamine

: 103-71-9
phenyl isocyanate

: 822-06-0
Hexamethylene diisocyanate

Conditions

Conditions	Yield
With phosgene In chlorobenzene at 10 - 130℃; for 4 - 5h; Solvent;	99.6%

: 102-09-0
bis(phenyl) carbonate

: 124-09-4
1,6-Hexanediamine

: 4223-31-8
N,N′-hexanediyl bis-carbamic acid diphenyl ester

Conditions

Conditions	Yield
With lead(II) oxide In phenol at 50℃; Product distribution / selectivity; Industry scale;	99.5%
With phenol at 50℃; Product distribution / selectivity; Industry scale;	99.5%
With phenol at 50℃; Industrial scale;	99.5%

: 124-09-4
1,6-Hexanediamine

: 616-38-6
carbonic acid dimethyl ester

: 6030-54-2
1,6-bis(methoxycarbonylamino)hexane

Conditions

Conditions	Yield
With hydrogenchloride; sodium methylate In methanol	99.5%
With sodium methylate In methanol at 50℃; for 2.5h;	98.1%
With water; sodium methylate In methanol at 50℃; for 5.5h;	98.1%

: 124-09-4
1,6-Hexanediamine

: 1422-70-4
bis(2,2,3,3-tetrafluoropropyl) carbonate

: 384812-59-3
C14H20F8N2O4

Conditions

Conditions	Yield
at 70℃; for 1h;	99.4%

: 124-09-4
1,6-Hexanediamine

: 50903-59-8
N-t-butyloxycarbonyl-Nε-benzyloxycarbonyl-lysine pentafluorophenyl ester

: bis-(N-t-butyloxycarbonyl-Nε-benzyloxycarbonyl)lysinehexamethylenediamide

Conditions

Conditions	Yield
Stage #1: 1,6-Hexanediamine; N-t-butyloxycarbonyl-Nε-benzyloxycarbonyl-lysine pentafluorophenyl ester In N,N-dimethyl-formamide at 20℃; Stage #2: With diethylaminopropylamine In N,N-dimethyl-formamide for 0.5h;	99.16%

: 124-09-4
1,6-Hexanediamine

: 110-13-4
2,5-hexanedione

: 6970-82-7
1,6-bis(2,5-dimethyl-1H-pyrrol-1-yl)hexane

Conditions

Conditions	Yield
In neat (no solvent) at 20℃; for 0.083h; Concentration; Paal-Knorr Pyrrole Synthesis; Green chemistry;	99%
With gallium(III) triflate In neat(no solvent) at 30℃; for 0.583333h; Paal-Knorr condensation;	94%
scandium tris(trifluoromethanesulfonate) at 30℃; Paal-Knorr reaction;	93%

: 124-09-4
1,6-Hexanediamine

: 57-13-6
urea

: 2188-09-2
1,6-hexamethylene diurea

Conditions

Conditions	Yield
With phenol at 50 - 120℃; for 3.5h; Reagent/catalyst; Temperature; Inert atmosphere;	99%
In toluene at 90 - 220℃; under 9750.98 Torr; Industry scale;	98%
With N-benzyl-trimethylammonium hydroxide In 2-methoxy-ethanol at 100℃; for 3h; Reagent/catalyst; Solvent; Temperature; Time; Concentration;	97.2%

: 124-09-4
1,6-Hexanediamine

: 88579-78-6
2,5-di-iodo-1,1,1,6,6,6-hexafluoro-3,4-diazahexa-2,4-diene

: 2,17-di-iodo-1,1,1,18,18,18-hexafluoro-5,14-bis(trifluoromethyl)-3,4,6,13,15,16-hexa-azaoctadeca-2,4,14,16-tetraene

Conditions

Conditions	Yield
In diethyl ether for 26h; Ambient temperature;	99%

: 102-09-0
bis(phenyl) carbonate

: 124-09-4
1,6-Hexanediamine

: 108-95-2
phenol

: 4223-31-8
N,N′-hexanediyl bis-carbamic acid diphenyl ester

Conditions

Conditions	Yield
at 45 - 60℃; for 1.33333h; Product distribution / selectivity;	99%
at 50 - 60℃; for 1.33333h; Product distribution / selectivity;

...Expand

: 124-09-4
1,6-Hexanediamine

: 107-13-1
acrylonitrile

: 51851-40-2
N,N,N',N'-(tetrakis(cyanoethyl)hexamethylenediamine)

Conditions

Conditions	Yield
In methanol at 50℃; for 48h;	99%
In water at 20 - 80℃; for 6h; Michael addition;	96%
Stage #1: 1,6-Hexanediamine; acrylonitrile With acetic acid In ethanol for 11h; Heating / reflux; Stage #2: With ammonia In water; ethyl acetate at 20℃;

: 124-09-4
1,6-Hexanediamine

: 1609-86-5
Tert-butyl isocyanate

: 15772-96-0
tBu-NH-CO-NH-(CH2)6-NH-CO-NH-tBu

Conditions

Conditions	Yield
In chloroform for 1h;	99%

: 124-09-4
1,6-Hexanediamine

: 58-85-5
biotin

: 65953-56-2
N-(6-aminohexyl)-5-((3aS,4S,6aR)-3a,6a-dimethyl-2-oxohexahydro-1H-thieno[3,4-d] imidazol-4-yl)pentanamide

Conditions

Conditions	Yield
Stage #1: biotin With di(succinimido) carbonate; triethylamine In N,N-dimethyl-formamide at 20℃; for 6h; Inert atmosphere; Stage #2: 1,6-Hexanediamine In N,N-dimethyl-formamide Inert atmosphere;	99%

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