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inquiryAppearance:White?powder or colorless liquid Storage:Store below +30°C. Package:25kg/drum Application:2-Amino-2-methylpropanol is used for the preparation of buffer solutions, suitable for the determination of alkaline phosphatase. Transportation:Ex
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inquiryProduct Name: 2-Amino-2-methyl-1-propanol CAS: 124-68-5 MF: C4H11NO MW: 89.14 EINECS: 204-709-8 Mol File: 124-68-5.mol 2-Amino-2-methyl-1-propanol Structure 2-Amino-2-methyl-1-propanol Chemical Properties Melting point 24-28 &
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inquiry2-Amino-2-methyl-1-propanol CAS: 124-68-5 Specification Items Specification Product name 2-Amino-2-methyl-1-propanol CAS# 124-68-5 Appearance
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inquiryConditions | Yield |
---|---|
With hydrogenchloride In water at 80℃; for 4h; | A 96% B 80% |
Conditions | Yield |
---|---|
With tricresyl phosphate; hydrogen; palladium diacetate In diphenylether at 140℃; under 22502.3 - 60006 Torr; Autoclave; | 93% |
Conditions | Yield |
---|---|
With sulfuric acid In water at 40 - 50℃; for 1h; pH=3 - 5.4; | 91% |
2-(ethylamino)-2-methylpropanol hydrochloride
A
formaldehyd
B
ethylamine
C
2-Amino-2-methyl-1-propanol
D
acetaldehyde
E
acetone
Conditions | Yield |
---|---|
With water at 25℃; Product distribution; Mechanism; anodic oxidation, carbonate buffer, pH 10; effect of substituents investigated with different types of β-alkanolamines; | A 50% B 44% C 14% D 26% E 66% |
2-(ethylamino)-2-methylpropanol hydrochloride
A
formaldehyd
B
ethylamine
C
2-Amino-2-methyl-1-propanol
D
acetone
Conditions | Yield |
---|---|
With water at 25℃; anodic oxidation, pH 10, carbonate buffer; Further byproducts given; | A 50% B 44% C 14% D 66% |
2-nitro-2-methylpropanol
A
N-(1-hydroxy-2-methylprop-2-yl)-hydroxylamine
B
2-Amino-2-methyl-1-propanol
Conditions | Yield |
---|---|
With citrate buffer; potassium chloride In ethanol at 30℃; cotrolled potential electrolysis, cathod: Hg, vs. S.C.E.; | A 64% B 25% |
2-methyl-3-(vinyloxy)propan-2-amine
B
2-Amino-2-methyl-1-propanol
Conditions | Yield |
---|---|
With mercury(II) diacetate In benzene Heating; | A 3% B n/a |
Conditions | Yield |
---|---|
With methanol; carbon dioxide; nickel at 70℃; under 25742.8 Torr; Hydrogenation; | |
With methanol; nickel at 30℃; under 25742.8 Torr; Hydrogenation; | |
With nickel Hydrogenation; |
Conditions | Yield |
---|---|
With ethanol; nickel at 100℃; under 257428 Torr; Hydrogenation; |
Conditions | Yield |
---|---|
With tetrahydrofuran; lithium aluminium tetrahydride | |
With lithium aluminium tetrahydride In tetrahydrofuran | |
With sodium tetrahydroborate; iodine In tetrahydrofuran for 20h; Heating; | |
With sodium tetrahydroborate; iodine In tetrahydrofuran Reflux; | |
With lithium aluminium tetrahydride In tetrahydrofuran |
Conditions | Yield |
---|---|
(i) MeCN, Cl2, (ii) H2O; Multistep reaction; |
2-ammonio-2-methyl-1-propanol cation
C14H13NO
A
1-methyl-4-(phenylacetyl)pyridinium cation
B
2-Amino-2-methyl-1-propanol
Conditions | Yield |
---|---|
In water at 25℃; Equilibrium constant; Rate constant; |
N-chloro-2-amino-2-methylpropan-1-ol
A
2-Amino-2-methyl-1-propanol
Conditions | Yield |
---|---|
In water at 25℃; Rate constant; Thermodynamic data; E(a); |
A
statine
B
2-Amino-2-methyl-1-propanol
Conditions | Yield |
---|---|
With hydrogenchloride for 1h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts; |
3-(N-succinimido)-2-propanol
2-Amino-2-methyl-1-propanol
Conditions | Yield |
---|---|
With hydrogenchloride; sodium tetrahydroborate In isopropyl alcohol |
Conditions | Yield |
---|---|
at 100℃; under 250073 Torr; Hydrogenation; |
2-amino-2-methylpropionic acid methyl ester
2-Amino-2-methyl-1-propanol
Conditions | Yield |
---|---|
With hydrogen; Nishimura catalyst <(45.9% Rh/19.9% Pt) oxide> In methanol at 25℃; under 75007.5 Torr; |
methyl 2-aminoisobutyrate hydrochloride
2-Amino-2-methyl-1-propanol
Conditions | Yield |
---|---|
With sodium tetrahydroborate; sodium hydrogencarbonate |
2-((tert-butyloxycarbonyl)amino)-2-methylpropan-1-ol
2-Amino-2-methyl-1-propanol
Conditions | Yield |
---|---|
With trifluoroacetic acid In dichloromethane |
B
2-Amino-2-methyl-1-propanol
(+)-pinanediol (1R)-1-acetylamino-1-[3-(4,4-dimethyl-4,5-dihydro-oxazol-2-yl)phenyl]methylboronate
A
2-Amino-2-methyl-1-propanol
Conditions | Yield |
---|---|
With hydrogenchloride In water at 120℃; for 1h; |
Conditions | Yield |
---|---|
at 125℃; Inert atmosphere; Schlenk technique; |
N-(1-hydroxy-2-methylpropan-2-yl)-1-naphthamide
2-Amino-2-methyl-1-propanol
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol at 135℃; for 0.166667h; Microwave irradiation; |
2-(hydroxymethyl)-2-methylpropylamine
2-Amino-2-methyl-1-propanol
Conditions | Yield |
---|---|
With sodium hypochlorite; sodium hydroxide In water at 0 - 70℃; for 0.333333h; Temperature; Hofmann Rearrangement; | 103 g |
Conditions | Yield |
---|---|
With cerium(III) nitrate hexahydrate In methanol |
N-(1-cyano-1-methyl-ethyl)formamide
A
N-(1-hydroxy-2-methylpropan-2-yl)formamide
B
2-Amino-2-methyl-1-propanol
Conditions | Yield |
---|---|
With (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); hydrogen In 1,4-dioxane; water at 140℃; under 33753.4 Torr; for 18h; Reagent/catalyst; Pressure; Autoclave; | A n/a B 24 %Spectr. |
With (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); hydrogen In 1,4-dioxane; water at 20 - 150℃; under 41254.1 - 101260 Torr; for 48h; Autoclave; | A n/a B 73 %Chromat. |
With (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); water; hydrogen; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine] In 1,4-dioxane at 150℃; under 41254.1 - 101260 Torr; for 48h; Catalytic behavior; Pressure; Reagent/catalyst; Temperature; Autoclave; | A 22 %Chromat. B 58.3 %Chromat. |
2-Amino-2-methyl-1-propanol
Conditions | Yield |
---|---|
With hydrogenchloride In water at 80℃; |
N-(1-cyano-1-methyl-ethyl)formamide
2-Amino-2-methyl-1-propanol
Conditions | Yield |
---|---|
With chloro(1,5-cyclooctadiene)rhodium(I) dimer; water; hydrogen; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In 1,4-dioxane at 140℃; under 41254.1 Torr; for 18h; Catalytic behavior; Reagent/catalyst; Pressure; Autoclave; | 24 %Spectr. |
Conditions | Yield |
---|---|
With sulfuric acid In water at 50 - 120℃; for 3h; Product distribution / selectivity; | 100% |
With chlorosulfonic acid In diethyl ether at 0℃; | 96% |
With sulfuric acid In water at 150 - 170℃; for 4h; | 94% |
pyridine-2-carbaldehyde
2-Amino-2-methyl-1-propanol
4,4-dimethyl-2-pyridin-2-yl-1,3-oxazolidine
Conditions | Yield |
---|---|
In ethanol for 2h; Ambient temperature; | 100% |
In ethanol at 20℃; for 3h; | 94% |
pyridine-4-carbaldehyde
2-Amino-2-methyl-1-propanol
4-(4,4-Dimethyl-oxazolidin-2-yl)-pyridine
Conditions | Yield |
---|---|
In ethanol for 2h; Ambient temperature; | 100% |
3-pyridinecarboxaldehyde
2-Amino-2-methyl-1-propanol
3-(4,4-Dimethyl-oxazolidin-2-yl)-pyridine
Conditions | Yield |
---|---|
In ethanol for 2h; Ambient temperature; | 100% |
benzoic acid ethyl ester
2-Amino-2-methyl-1-propanol
N-(2-hydroxyl-1,1-dimethylethyl) benzamide
Conditions | Yield |
---|---|
Stage #1: 2-Amino-2-methyl-1-propanol With n-butyllithium; lanthanum(III) chloride In 1,2-dichloro-ethane at 0℃; Metallation; after the reagent addition stirring for 15 min at this temperature under nitrogen, than warming to reflux; Stage #2: benzoic acid ethyl ester for 1h; Amidation; reflux; | 100% |
With sodium hydride 1.) toluene, RT, 1 h, 2.) toluene, 30 min; Yield given. Multistep reaction; | |
With n-butyllithium; lanthanum(lll) triflate 1) toluene, 0 deg C, 15 min then 0 to 100 deg C, 2) toluene, reflux, 12 h; Yield given. Multistep reaction; |
di-tert-butyl dicarbonate
2-Amino-2-methyl-1-propanol
2-((tert-butyloxycarbonyl)amino)-2-methylpropan-1-ol
Conditions | Yield |
---|---|
In acetonitrile at 20℃; Condensation; | 100% |
With triethylamine In dichloromethane at 20℃; for 2.83333h; | 100% |
Stage #1: di-tert-butyl dicarbonate With molybdenium(VI) dioxodichloride In dichloromethane at 20℃; for 0.5h; Stage #2: 2-Amino-2-methyl-1-propanol In dichloromethane at 20℃; for 10h; | 99% |
5-methoxy-3-methylbenzoic acid chloride
2-Amino-2-methyl-1-propanol
Conditions | Yield |
---|---|
In dichloromethane at 25℃; for 24h; | 100% |
2-Amino-2-methyl-1-propanol
ortho-toluoyl chloride
N-(1-hydroxy-2-methylpropan-2-yl)-2-methylbenzamide
Conditions | Yield |
---|---|
In dichloromethane at 0℃; for 0.5h; | 100% |
With triethylamine In dichloromethane at 0℃; | |
With triethylamine In dichloromethane at 0℃; for 3h; Inert atmosphere; |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene Heating; | 100% |
n-pentyl methyl ketone
2-Amino-2-methyl-1-propanol
2,4,4-trimethyl-2-pentyloxazolidine
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene Heating; | 100% |
5-Nonanone
2-Amino-2-methyl-1-propanol
2,2-dibutyl-4,4-dimethyloxazolidine
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene Heating; | 100% |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene Heating; | 100% |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene Heating; | 100% |
dipentyl ketone
2-Amino-2-methyl-1-propanol
4,4-dimethyl-2,2-dipentyloxazolidine
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene Heating; | 100% |
methyl nonyl ketone
2-Amino-2-methyl-1-propanol
2,4,4-trimethyl-2-nonyloxazolidine
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene Heating; | 100% |
10-Nonadecanon
2-Amino-2-methyl-1-propanol
4,4-dimethyl-2,2-dinonyloxazolidine
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene Heating; | 100% |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene Heating; | 100% |
2,3-dimethoxyterephthalic acid chloride
2-Amino-2-methyl-1-propanol
N,N'-bis(2-hydroxy-1,1-dimethylethyl)-2,3-dimethoxyterephthalamide
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 2h; | 100% |
In dichloromethane; water | 6.27 g (100%) |
2,3-bis(benzyloxy)benzoyl chloride
2-Amino-2-methyl-1-propanol
2,3-dibenzyloxy-N-(2-hydroxy-1,1-dimethylethyl)benzamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 6.5h; | 100% |
2-hydroxy-3-phenylbenzaldehyde
2-Amino-2-methyl-1-propanol
Conditions | Yield |
---|---|
for 1h; Heating; | 100% |
2-Amino-2-methyl-1-propanol
2,2'-dihydroxybiphenyl-3-carboxaldehyde
Conditions | Yield |
---|---|
for 1h; Heating; | 100% |
acetic anhydride
2-Amino-2-methyl-1-propanol
N-(1-hydroxy-2-methylpropan-2-yl)acetamide
Conditions | Yield |
---|---|
Stage #1: acetic anhydride With molybdenium(VI) dioxodichloride In dichloromethane at 20℃; for 0.5h; Stage #2: 2-Amino-2-methyl-1-propanol In dichloromethane at 20℃; for 0.5h; | 100% |
Stage #1: acetic anhydride; 2-Amino-2-methyl-1-propanol In ethyl acetate at 20℃; for 18h; Inert atmosphere; Stage #2: With potassium carbonate In ethyl acetate at 20℃; Inert atmosphere; chemoselective reaction; | 98% |
With Methylenediphosphonic acid at 20℃; for 1h; neat (no solvent); chemoselective reaction; | 95% |
With sodium hydrogencarbonate In water at 20℃; for 16h; | |
With triethylamine In chloroform at 20℃; for 24h; Temperature; chemoselective reaction; | 99 %Spectr. |
2,2-dimethylpropanoic anhydride
2-Amino-2-methyl-1-propanol
N-(2-hydroxy-1,1-dimethylethyl)-2,2-dimethylpropionamide
Conditions | Yield |
---|---|
Stage #1: 2,2-dimethylpropanoic anhydride With molybdenium(VI) dioxodichloride In dichloromethane at 20℃; for 0.5h; Stage #2: 2-Amino-2-methyl-1-propanol In dichloromethane at 20℃; for 1h; | 100% |
benzoyl chloride
2-Amino-2-methyl-1-propanol
4,5-dihydro-4,4-dimethyl-2-phenoxazole
Conditions | Yield |
---|---|
Stage #1: benzoyl chloride; 2-Amino-2-methyl-1-propanol In dichloromethane at 20℃; for 18h; Stage #2: With thionyl chloride In dichloromethane Further stages.; | 100% |
Stage #1: benzoyl chloride; 2-Amino-2-methyl-1-propanol With triethylamine In dichloromethane at 0 - 20℃; for 10h; Stage #2: With thionyl chloride In chloroform at 0 - 20℃; for 24h; Stage #3: With sodium hydroxide In methanol at 0 - 20℃; for 12h; | 92% |
3-methyl-4-isocyanato-benzoic acid methyl ester
2-Amino-2-methyl-1-propanol
4-(3-[1,1-dimethyl-2-hydroxy-ethyl]-ureido)-3-methyl-benzoic acid methyl ester
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 2h; | 100% |
In tetrahydrofuran at 20℃; for 2h; |
1-[[[(2,5-dioxopyrrolidin-1-yl)oxy]carbonyl]oxy]ethyl 2-methylpropanoate
2-Amino-2-methyl-1-propanol
[N-(2-hydroxy-tert-butyl)carbamoyloxy]ethyl 2-methylpropanoate
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water; acetonitrile at 20℃; for 12h; | 100% |
Conditions | Yield |
---|---|
With sodium hydride In mineral oil at 160℃; Inert atmosphere; | 100% |
With sodium hydride at 140℃; for 4h; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
With sodium hydride In mineral oil at 160℃; Inert atmosphere; | 100% |
2-tert-butylmalonyl dichloride
2-Amino-2-methyl-1-propanol
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 2h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With sodium hydride In mineral oil at 160℃; Inert atmosphere; | 100% |
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