chengdu and import and export trade co., LTD., who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do res
Cas:13716-10-4
Min.Order:10 Kilogram
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inquiryhigh quality Appearance:colorless liquid Storage:Sealed, dry, microtherm , avoid light and smell Package:According to the demand of customer Application:Pharmaceutical intermediates Transportation:by air or by sea Port:shanghai
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:13716-10-4
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inquiryPuyang Huicheng Electronic Material Co., Ltd was founded in 2002, which is focus on high complex new type intermediates and fine chemical custom synthesis, LED&OLED materials and related intermediates, catalyst design and synthesi
Cas:13716-10-4
Min.Order:100 Gram
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Type:Manufacturers
inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis
Cas:13716-10-4
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:13716-10-4
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.
Cas:13716-10-4
Min.Order:1 Metric Ton
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:13716-10-4
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:13716-10-4
Min.Order:10 Kilogram
Negotiable
Type:Trading Company
inquiryCAS No.: 13716-10-4 Molecular formula: C8H18ClP Molecular weight: 180.66 EINECS number: Related Categories: Chlorophosphines; Ligand; Catalysis and Inorganic Chemistry; Phosphorus Compounds; Phosphorus Precursors; Phosphines; Phosphine Compou
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Cas:13716-10-4
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:13716-10-4
Min.Order:0
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Type:Lab/Research institutions
inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:13716-10-4
Min.Order:4 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryChemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff
Cas:13716-10-4
Min.Order:100 Gram
Negotiable
Type:Other
inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:13716-10-4
Min.Order:100 Gram
FOB Price: $100.0 / 2000.0
Type:Lab/Research institutions
inquirySuperior quality, moderate price & quick delivery. Appearance:Colorless to light yellow liquid Storage:In Room Temperature Package:25kg/drum, or as per your request. Application:For medicine , pesticide intermediates Transportation:as per y
Cas:13716-10-4
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providing h
Cas:13716-10-4
Min.Order:0
Negotiable
Type:Other
inquiryWe are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED
Cas:13716-10-4
Min.Order:1 Gram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryroduct Name: Di-tert-butylchlorophosphane CAS: 13716-10-4 MF: C8H18ClP MW: 180.66 EINECS: Mol File: 13716-10-4.mol Di-tert-butylchlorophosphane Structure Di-tert-butylchlorophosphane Chemical Properties Melting point 2-3°
Cas:13716-10-4
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:13716-10-4
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryHigh quality, competitive price, fast delivery and first-class service we possesses have won the trust and praise of customers. Standard: BP/USP/EP The purity is equal or greater than 99%. As a supplier, we can provide high-quality products. Cle
Cas:13716-10-4
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:13716-10-4
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:13716-10-4
Min.Order:1 Metric Ton
FOB Price: $1.5
Type:Trading Company
inquiryHigh quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
Cas:13716-10-4
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryGOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
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Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Trading Company
inquiryStock products, own laboratoryAppearance:Colorless liquid Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:13716-10-4
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryISO/factory/goodqualityAppearance:off white Storage:Dry,cool place Package:drum Application:active pharmaceutical ingredients Transportation:by air/sea/express Port:shenzhen/shanghai
Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
Cas:13716-10-4
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquirytetra-tert-butyldiphosphane
di(tert-butyl)chlorophosphine
Conditions | Yield |
---|---|
With Dichlorophenylphosphine for 2h; | 83% |
di-tert-butylphosphine
di(tert-butyl)chlorophosphine
Conditions | Yield |
---|---|
With n-octyl trichloroacetate at 70 - 84℃; for 0.666667h; Product distribution / selectivity; | 78.2% |
With tetrachloromethane at 20℃; for 48h; also at 100 deg C, 30 min.; Yield given; |
tert-butylmagnesium chloride
di(tert-butyl)chlorophosphine
Conditions | Yield |
---|---|
With phosphorus trichloride In diethyl ether for 0.5h; Heating; | 60% |
With phosphorus trichloride In diethyl ether | |
With phosphorus trichloride In diethyl ether at 20℃; Inert atmosphere; Schlenk technique; |
tertiary butyl chloride
di(tert-butyl)chlorophosphine
Conditions | Yield |
---|---|
Stage #1: tertiary butyl chloride With magnesium In diethyl ether at 20℃; Inert atmosphere; Schlenk technique; Stage #2: With phosphorus trichloride In diethyl ether at -40℃; Inert atmosphere; Schlenk technique; | 50% |
Stage #1: tertiary butyl chloride With magnesium In diethyl ether at 20℃; Inert atmosphere; Schlenk technique; Stage #2: With phosphorus trichloride In diethyl ether at -40℃; Inert atmosphere; Schlenk technique; | 50% |
(i) Mg, Et2O, (ii) PCl3; Multistep reaction; |
tetrachloromethane
2-Methyl-1-(1,2,2-tri-tert-butyl-diphosphanyl)-propan-1-one
A
di(tert-butyl)chlorophosphine
B
tert-butylpivaloylphosphinic acid chloride
C
tert-butylpivaloylphosphinic acid chloride
D
1-(tert-Butyl-trichloromethyl-phosphanyl)-2-methyl-propan-1-one
Conditions | Yield |
---|---|
at 20℃; for 48h; |
tetrachloromethane
2-Methyl-1-(1,2,2-tri-tert-butyl-diphosphanyl)-propan-1-one
A
di(tert-butyl)chlorophosphine
B
tert-butylpivaloylphosphinic acid chloride
C
1-(tert-Butyl-trichloromethyl-phosphanyl)-2-methyl-propan-1-one
D
Di-tert-butyl(trichloromethyl)phosphine
Conditions | Yield |
---|---|
at 20℃; for 48h; |
Di-tert-butylphosphine
A
1,1,2,2-tetrachloroethylene
B
di(tert-butyl)chlorophosphine
C
N,N,N',N'-Tetramethylformamidinium chloride
Conditions | Yield |
---|---|
With tetrachloromethane In diethyl ether at 20℃; for 48h; |
pivaloyl chloride
2-Methyl-1-(1,2,2-tri-tert-butyl-diphosphanyl)-propan-1-one
A
di(tert-butyl)chlorophosphine
B
tert-butylpivaloylphosphinic acid chloride
C
di-tert-butylpivaloylphosphine
D
1-(tert-Butyl-isobutyryl-phosphanyl)-2,2-dimethyl-propan-1-one
Conditions | Yield |
---|---|
at 20℃; for 48h; |
<(di-tert-butylphosphino)(trimethylsilyl)amino>lithium
di(tert-butyl)chlorophosphine
Conditions | Yield |
---|---|
With phosphorus trichloride In diethyl ether; hexane at 20℃; |
2-Methyl-1-(1,2,2-tri-tert-butyl-diphosphanyl)-propan-1-one
A
di(tert-butyl)chlorophosphine
B
tert-butylpivaloylphosphinic acid chloride
C
di-tert-butylpivaloylphosphine
D
1-(tert-Butyl-isobutyryl-phosphanyl)-2,2-dimethyl-propan-1-one
Conditions | Yield |
---|---|
With pivaloyl chloride at 20℃; for 48h; |
2-Methyl-1-(1,2,2-tri-tert-butyl-diphosphanyl)-propan-1-one
A
di(tert-butyl)chlorophosphine
B
tert-butylpivaloylphosphinic acid chloride
C
1-(tert-Butyl-trichloromethyl-phosphanyl)-2-methyl-propan-1-one
D
Di-tert-butyl(trichloromethyl)phosphine
Conditions | Yield |
---|---|
With tetrachloromethane at 20℃; for 48h; |
1,1-Di-tert-butyl-2-diphosphan
A
di(tert-butyl)chlorophosphine
B
chlorophosphane
Conditions | Yield |
---|---|
With hexachloroethane Product distribution; |
chloro-diphenylphosphine
A
di(tert-butyl)chlorophosphine
B
di-tert-butylphosphine
D
1.1-Diisobutyl-2.2-diphenyldiphosphin
E
Tetraphenyldiphosphin
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane at -40 - 20℃; for 24h; Schlenk technique; | A n/a B 8 %Spectr. C 9 %Spectr. D 17 %Spectr. E 41 %Spectr. |
tert-butylmagnesium chloride
A
di(tert-butyl)chlorophosphine
B
tert-butyldichlorophosphine
Conditions | Yield |
---|---|
With phosphorus trichloride In diethyl ether at 20℃; |
di(tert-butyl)chlorophosphine
di-tert-butylphosphine oxide
Conditions | Yield |
---|---|
In dichloromethane at 20℃; Inert atmosphere; Glovebox; | 100% |
With water; triethylamine In tetrahydrofuran for 0.666667h; | 89% |
With ethylene glycol; triethylamine In tetrahydrofuran at 0 - 130℃; | 31% |
di(tert-butyl)chlorophosphine
1-(4-fluorophenyl)ethylamine
C16H27FNP
Conditions | Yield |
---|---|
100% |
di(tert-butyl)chlorophosphine
Conditions | Yield |
---|---|
Stage #1: (RC,SFc,SP)-1-[2-(1-dimethylaminoethyl)ferrocen-1-yl]phenylphosphino-1'-bromoferrocene With n-butyllithium In hexane; tert-butyl methyl ether at -5 - 0℃; Stage #2: di(tert-butyl)chlorophosphine In hexane; tert-butyl methyl ether at 0 - 20℃; | 100% |
di(tert-butyl)chlorophosphine
trans-1,3-cyclohexanediol
Conditions | Yield |
---|---|
With sodium hydride In paraffin oil Inert atmosphere; Schlenk technique; Glovebox; | 100% |
2,2-dimethyl-1,2,3,4-tetrahydroquinoline
di(tert-butyl)chlorophosphine
1-(Di-tert-butyl-phosphanyl)-2,2-dimethyl-1,2,3,4-tetrahydro-quinoline
Conditions | Yield |
---|---|
99% |
Conditions | Yield |
---|---|
Stage #1: indole With n-butyllithium In tetrahydrofuran; hexane at 0℃; for 0.25h; Inert atmosphere; Stage #2: di(tert-butyl)chlorophosphine In tetrahydrofuran; hexane at 0 - 20℃; Inert atmosphere; | 99% |
Stage #1: indole With n-butyllithium In tetrahydrofuran; hexane at 0℃; for 0.25h; Schlenk technique; Inert atmosphere; Sealed tube; Stage #2: di(tert-butyl)chlorophosphine In tetrahydrofuran; hexane at 0 - 20℃; Schlenk technique; Inert atmosphere; Sealed tube; | 99% |
Stage #1: indole With n-butyllithium In tetrahydrofuran at 0℃; for 0.5h; Inert atmosphere; Schlenk technique; Stage #2: di(tert-butyl)chlorophosphine In tetrahydrofuran at 0 - 25℃; for 12h; | 95% |
With n-butyllithium In tetrahydrofuran; hexane at 0 - 20℃; | |
Stage #1: indole With n-butyllithium In tetrahydrofuran; hexane at 0℃; for 1h; Inert atmosphere; Schlenk technique; Sealed tube; Stage #2: di(tert-butyl)chlorophosphine In tetrahydrofuran; hexane at 0 - 20℃; Inert atmosphere; Schlenk technique; Sealed tube; |
di(tert-butyl)chlorophosphine
P,P-bis(1,1-dimethylethyl)phosphinoselenoic chloride
Conditions | Yield |
---|---|
With selenium In toluene for 0.25h; Heating; | 99% |
di(tert-butyl)chlorophosphine
(8S)-8-hydroxy-5,6,7,8-tetrahydroquinoline
(S)-5,6,7,8-tetrahydroquinolin-8-yl di-tert-butylphosphinite
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran; N,N-dimethyl-formamide at 0 - 20℃; for 96h; | 99% |
Conditions | Yield |
---|---|
In toluene for 25h; Heating / reflux; Under Ar or N2; | 99% |
lithium aluminium tetrahydride
borane-THF
di(tert-butyl)chlorophosphine
di-tert-butylphosphine borane
Conditions | Yield |
---|---|
In tetrahydrofuran for 60h; Cooling with ice; Schlenk technique; | 99% |
di(tert-butyl)chlorophosphine
3,5-dihydroxy-N,N-(dimethylamino)benzene
Conditions | Yield |
---|---|
With sodium hydride Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With sodium hydride Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
In dichloromethane at -30 - 20℃; for 0.25h; Inert atmosphere; | 99% |
In dichloromethane at -35℃; for 0.25h; Inert atmosphere; | 99% |
di(tert-butyl)chlorophosphine
3,5-dimethylaminoaniline
Conditions | Yield |
---|---|
Stage #1: 3,5-dimethylaminoaniline With n-butyllithium In tetrahydrofuran; hexane at -78 - 20℃; for 1h; Inert atmosphere; Schlenk technique; Stage #2: di(tert-butyl)chlorophosphine In tetrahydrofuran; hexane at -78 - 20℃; for 18h; Schlenk technique; Inert atmosphere; | 99% |
di(tert-butyl)chlorophosphine
palladium
phenylmagnesium bromide
bis(di-tert-butylphenylphosphine)palladium(II) dichloride
Conditions | Yield |
---|---|
Stage #1: palladium With hydrogenchloride; nitric acid; cyclo-octa-1,5-diene In ethanol; water at 50℃; Stage #2: di(tert-butyl)chlorophosphine; phenylmagnesium bromide In tetrahydrofuran; ethanol; water at 50 - 70℃; Temperature; | 98.8% |
Conditions | Yield |
---|---|
With cesium fluoride; palladium diacetate In 1,4-dioxane; dichloromethane; water | 98% |
ferrocene
di(tert-butyl)chlorophosphine
(ferrocenyl)di(tert-butyl)phosphine
Conditions | Yield |
---|---|
With aluminum (III) chloride In hexane at 0℃; for 3h; Temperature; Inert atmosphere; | 98% |
Stage #1: ferrocene With potassium tert-butylate; tert.-butyl lithium In diethyl ether at -78 - -70℃; for 1h; Inert atmosphere; Schlenk technique; Stage #2: di(tert-butyl)chlorophosphine In diethyl ether at 0℃; Inert atmosphere; Schlenk technique; | 71% |
With tert.-butyl lithium In not given addn. of excess chlorophosphine to lithioferrocene (prepd. from t-BuLi and ferrocene); repeated sublimation (85°C, 0.01 mmHg); elem. anal.; | 27% |
Stage #1: ferrocene With potassium tert-butylate; tert.-butyl lithium In tetrahydrofuran; pentane at -73 - 0℃; Inert atmosphere; Stage #2: di(tert-butyl)chlorophosphine In tetrahydrofuran; pentane at 0 - 20℃; for 12h; Inert atmosphere; |
di(tert-butyl)chlorophosphine
(C5H5)2NbH(PH(C(CH3)3)2)
Conditions | Yield |
---|---|
In tetrahydrofuran byproducts: LiCl; absence of air and moisture; stirring Nb-complex soln. with phosphine (-78°C, 15 min), warming to room temp.; decantation, drying (vac.), extn. into ether, filtration, solvent removal; elem. anal.; | 98% |
Conditions | Yield |
---|---|
Stage #1: propan-1-ol; di(tert-butyl)chlorophosphine With sodium In diethyl ether at 20℃; for 16h; Inert atmosphere; Stage #2: With water In diethyl ether Inert atmosphere; | 98% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene at 20℃; for 5h; Schlenk technique; Inert atmosphere; | 96% |
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 0 - 20℃; for 36h; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran Inert atmosphere; | 97% |
In toluene Heating; |
(R)-5H,6H,7H-cyclopenta[b]pyridin-7-ol
di(tert-butyl)chlorophosphine
(R)-6,7-dihydro-5H-[1]pyrindin-7-yl di-tert-butylphosphinite
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran; N,N-dimethyl-formamide at 0 - 20℃; for 39h; | 97% |
di(tert-butyl)chlorophosphine
(E)-6-(1-((2,6-dimethylphenyl)imino)ethyl)pyridin-2(1H)-one
(E)-N-(1-(6-((di-tert-butylphosphino)oxy)-pyridin-2-yl)ethylidene)-2,6-dimethylaniline
Conditions | Yield |
---|---|
Stage #1: (E)-6-(1-((2,6-dimethylphenyl)imino)ethyl)pyridin-2(1H)-one With sodium hydride In tetrahydrofuran at 20℃; for 0.166667h; Inert atmosphere; Schlenk technique; Stage #2: di(tert-butyl)chlorophosphine In tetrahydrofuran for 3h; Inert atmosphere; Schlenk technique; | 97% |
6-methyl-2-phenylpyridine
di(tert-butyl)chlorophosphine
Conditions | Yield |
---|---|
Stage #1: 6-methyl-2-phenylpyridine With tert.-butyl lithium In tetrahydrofuran; pentane at -78℃; for 2h; Inert atmosphere; Schlenk technique; Stage #2: di(tert-butyl)chlorophosphine In tetrahydrofuran; pentane at -78 - 20℃; Inert atmosphere; Schlenk technique; | 97% |
Conditions | Yield |
---|---|
Stage #1: C19H17N5 With n-butyllithium In tetrahydrofuran at -80 - 0℃; for 1h; Inert atmosphere; Stage #2: di(tert-butyl)chlorophosphine at -80 - 20℃; Inert atmosphere; | 96.36% |
Conditions | Yield |
---|---|
In diethyl ether; pentane at -78 - 20℃; | 96% |
In pentane 1) - 80 deg C, 2) -20 to 20 deg C, 15 min, 3) 20 deg C, 30 min; | 87% |
di(tert-butyl)chlorophosphine
benzylmagnesium chloride
benzyl(di-tert-butyl)phosphane
Conditions | Yield |
---|---|
Stage #1: di(tert-butyl)chlorophosphine; benzylmagnesium chloride In tetrahydrofuran for 48h; Heating / reflux; Stage #2: With water; ammonium chloride In tetrahydrofuran at 20℃; | 96% |
In tetrahydrofuran for 48h; Heating / reflux; | 96% |
Stage #1: di(tert-butyl)chlorophosphine; benzylmagnesium chloride In tetrahydrofuran for 48h; Heating / reflux; Stage #2: With ammonium chloride In tetrahydrofuran; water at 20℃; | 96% |
copper(ll) bromide In tetrahydrofuran at 40 - 45℃; for 4h; | 88.3% |
1H-imidazole
di(tert-butyl)chlorophosphine
1-(di-tert-butylphosphino)imidazole
Conditions | Yield |
---|---|
With triethylamine In diethyl ether at 20℃; for 24h; Inert atmosphere; Schlenk technique; | 96% |
With triethylamine In diethyl ether at 20℃; Inert atmosphere; | 95% |
di(tert-butyl)chlorophosphine
Conditions | Yield |
---|---|
Stage #1: 2'-bromo-1,1':3',1'-terphenyl With magnesium In tetrahydrofuran for 4h; Inert atmosphere; Reflux; Stage #2: di(tert-butyl)chlorophosphine With tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 20℃; for 6h; Reflux; Inert atmosphere; | 96% |
di(tert-butyl)chlorophosphine
3-methyl-4-bromo-N,N-dimethylaniline
Conditions | Yield |
---|---|
Stage #1: 3-methyl-4-bromo-N,N-dimethylaniline With magnesium In tetrahydrofuran for 2h; Inert atmosphere; Reflux; Stage #2: di(tert-butyl)chlorophosphine With tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 20℃; for 6h; Reflux; Inert atmosphere; | 96% |
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