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4-nitrophenol acetate
p-aminophenyl acetate
Conditions | Yield |
---|---|
With hydrogen; 5percent Pd/C In ethyl acetate at 20℃; under 2280.15 Torr; for 4h; | 100% |
With 1,1,3,3-Tetramethyldisiloxane In ethanol at 20℃; for 0.5h; Inert atmosphere; Sonication; chemoselective reaction; | 99% |
With hydrogen at 130℃; under 750.075 Torr; for 6h; chemoselective reaction; | 99% |
Conditions | Yield |
---|---|
With 50wtpercent Cs2.5H0.5PW12O40 supported on MCM-41 In acetonitrile at 50℃; for 0.5h; | 94% |
p-aminophenyl acetate
Conditions | Yield |
---|---|
With ammonium formate; magnesium In ethylene glycol for 0.0333333h; microwave irradiation; | 93% |
p-aminophenyl acetate
Conditions | Yield |
---|---|
With aluminium(III) iodide In benzene for 0.166667h; Reduction; Heating; | 92% |
With hydrazinium monoformate; zinc In methanol at 20℃; for 0.116667h; |
p-aminophenyl acetate
Conditions | Yield |
---|---|
With water at 100℃; for 3h; | 91% |
sodium hydrogen sulfate; silica gel In dichloromethane for 2h; Heating; | 90% |
With trifluoroacetic acid In dichloromethane at 20℃; for 2h; Green chemistry; | 84% |
In water at 125℃; for 2.5h; Green chemistry; | 90 %Chromat. |
4-amino-phenol
2,2'-bipyridyl-6-yl acetate
A
p-aminophenyl acetate
B
4-acetoxyacetanilide
C
<2,2'-bipyridin>-6(1H)-one
Conditions | Yield |
---|---|
With cesium fluoride In N,N-dimethyl-formamide for 0.333333h; Product distribution; Ambient temperature; other esters, reagent; | A 84% B 5% C n/a |
With cesium fluoride In N,N-dimethyl-formamide for 0.333333h; Ambient temperature; | A 84% B 5% C n/a |
Conditions | Yield |
---|---|
CoCl2 In acetonitrile for 2h; Ambient temperature; | 83% |
4-acetoxyacetanilide
A
p-aminophenyl acetate
B
4-acetaminophenol
C
4-amino-phenol
Conditions | Yield |
---|---|
In water at 150 - 200℃; Green chemistry; | A 70% B n/a C n/a |
acetic acid-(4-benzylidenamino-phenyl ester)
p-aminophenyl acetate
sulfuric acid
acetic acid-(4-benzylidenamino-phenyl ester)
A
p-aminophenyl acetate
B
benzaldehyde
Conditions | Yield |
---|---|
With 4-hydroxyacetophenone monooxygenase from P. fluorescens ACB; oxygen; NADPH In phosphate buffer at 30℃; for 1h; pH=8.0; Enzyme kinetics; Baeyer-Villiger oxidation; |
4-nitro-phenol
p-aminophenyl acetate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Et3N; DMAP / CH2Cl2 2: H2; Pd-C / methanol View Scheme | |
Multi-step reaction with 2 steps 1: pyridine / acetone / 4 h / 20 °C / Reflux 2: iron; ammonium chloride / ethanol; water / 2 h / Reflux View Scheme |
4-benzylidenamino-phenol
p-aminophenyl acetate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NaOH-solution; benzene 2: benzene; diluted sulfuric acid View Scheme |
Conditions | Yield |
---|---|
In 5-(Oxiran-2-yl-methoxy)-2-1(3-trifluoromethyl)phenyl]benzoxazole |
Conditions | Yield |
---|---|
Stage #1: p-aminophenol hydrochloride In tetrahydrofuran Stage #2: acetic anhydride With triethylamine In tetrahydrofuran Stage #3: With N,N,N,N,-tetramethylethylenediamine In tetrahydrofuran |
4-chlorobenzonitrile
p-aminophenyl acetate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium hydroxide / water / 10 h / 140 °C / 2250.23 Torr / Autoclave 1.2: 0.5 h / 80 °C 2.1: 5% Pd/C; hydrogen / ethyl acetate / 6.5 h / 65 °C / 3750.38 Torr View Scheme |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 5℃; |
4-N-tert-butoxycarbonylaminophenol
p-aminophenyl acetate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: triethylamine / dichloromethane / 2 h / 0 - 20 °C / Green chemistry 2: trifluoroacetic acid / dichloromethane / 2 h / 20 °C / Green chemistry View Scheme |
4-amino-phenol
p-aminophenyl acetate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: methanol / 16 h / 100 °C / Green chemistry 2: triethylamine / dichloromethane / 2 h / 0 - 20 °C / Green chemistry 3: trifluoroacetic acid / dichloromethane / 2 h / 20 °C / Green chemistry View Scheme |
Conditions | Yield |
---|---|
With hydrazine hydrate In chloroform for 1.25h; chemoselective reaction; |
Conditions | Yield |
---|---|
With Au/Al2O3; hydrogen at 90℃; under 37503.8 Torr; Flow reactor; | A 7 %Chromat. B 86 %Chromat. |
4-Aminoacetophenone
p-aminophenyl acetate
Conditions | Yield |
---|---|
With dihydrogen peroxide In 1,4-dioxane at 100℃; Baeyer-Villiger Ketone Oxidation; |
Conditions | Yield |
---|---|
With indium(III) bromide In dichloromethane for 3h; Reflux; | 97.5% |
p-aminophenyl acetate
dimedone
4-(5,5-dimethyl-3-oxocyclohex-1-enylamino)phenyl acetate
Conditions | Yield |
---|---|
With silica-supported phosphorous pentoxide at 80℃; for 0.0666667h; Neat (no solvent); chemoselective reaction; | 95% |
With silica-supported LiHSO4 at 80℃; for 0.116667h; Neat (no solvent); | 92% |
With silica sulfuric acid at 80℃; for 0.116667h; Neat (no solvent); | 92% |
With zeolite ZSM-5 In ethanol for 0.666667h; Reflux; | 90% |
p-aminophenyl acetate
4-bromophenyl acetate
Conditions | Yield |
---|---|
Stage #1: p-aminophenyl acetate With boron trifluoride diethyl etherate; lithium bromide In acetonitrile at 0℃; for 0.166667h; Stage #2: With tert.-butylnitrite In acetonitrile at 0 - 20℃; for 1h; | 95% |
p-aminophenyl acetate
4-amino-3-bromophenyl acetate
Conditions | Yield |
---|---|
With N-Bromosuccinimide In dichloromethane at 20℃; for 20h; | 83% |
p-aminophenyl acetate
carbon monoxide
Conditions | Yield |
---|---|
With palladium(II) trifluoroacetate; C86H59F15NO2P; caesium carbonate In 1,3,5-trimethyl-benzene at 45℃; under 760.051 Torr; for 48h; enantioselective reaction; | 82% |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In tetrahydrofuran at 0 - 20℃; for 8.5h; | 77.1% |
p-aminophenyl acetate
bis(pinacol)diborane
4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl acetate
Conditions | Yield |
---|---|
With tert.-butylnitrite; dibenzoyl peroxide In acetonitrile at 20℃; for 2h; Sandmeyer reaction; | 73% |
With tert-butyl nitrite; benzoyl peroxide In acetonitrile MeCN, AcOC6H4NH2 (1 mmol) and tBuONO (1.5 mmol) added to B2pin2 (1 mmol)and benzoyl peroxide (0.02 mmol), mixt. stirred at room temp. for 2 h; soln. concd. (under reduced pressure), residue chromd.; | 73% |
4-formylphenyl acetate
p-aminophenyl acetate
tert-butylisonitrile
propionic acid
Conditions | Yield |
---|---|
In methanol at 20℃; for 5h; Ugi Condensation; Inert atmosphere; | 73% |
p-aminophenyl acetate
2-methyl-5-nitrobenzoyl chloride
2-methyl-5-nitro-N-(4-acetoxyphenyl)benzamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 5h; Ambient temperature; | 71% |
p-aminophenyl acetate
3-(2-chlorocarbonyl-ethyldisulfanyl)-propionyl chloride
Conditions | Yield |
---|---|
With sodium hydroxide In dichloromethane | 69% |
Conditions | Yield |
---|---|
Stage #1: p-aminophenyl acetate; benzenediazonium tetrafluoroborate; acetonitrile With potassium carbonate at 90℃; for 2h; Green chemistry; Stage #2: With [bis(acetoxy)iodo]benzene at 25℃; for 2h; Green chemistry; chemoselective reaction; | 63% |
Conditions | Yield |
---|---|
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical In toluene at 120℃; for 48h; | 62% |
p-aminophenyl acetate
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane at 5 - 25℃; for 2h; | 61.6% |
p-aminophenyl acetate
di-tert-butyl dicarbonate
Conditions | Yield |
---|---|
With bismuth (III) nitrate pentahydrate In neat (no solvent) at 40℃; for 0.166667h; | 61% |
p-aminophenyl acetate
4-Nitrophenacyl bromide
Conditions | Yield |
---|---|
With sodium carbonate In methanol for 12h; Ambient temperature; | 60% |
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