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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

6-Bromoindanone Manufacturer/High quality/Best price/In stock

Cas:14548-39-1

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 6-Bromoindanone supplier in China

Cas:14548-39-1

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

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Wuhan Fortuna Chemical Co.,Ltd

Manufacturer supply 6-Bromoindanone CAS 14548-39-1 with attractive price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/F

Manufacturer supply 6-Bromoindanone CAS 14548-39-1 with attractive price

Cas:14548-39-1

Min.Order:10 Kilogram

FOB Price: $10.0

Type:Trading Company

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Enke Pharma-tech Co.,Ltd. (Cangzhou, China )

Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api, intermedi

6-Bromoindanone

Cas:14548-39-1

Min.Order:1 Kilogram

FOB Price: $5.0

Type:Manufacturers

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

6-Bromo-1-indanone

Cas:14548-39-1

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Ality Chemical Corporation

6-Bromoindanone Basic information Uses Product Name: 6-Bromoindanone Synonyms: 6-bromofluorenone;6-BROMO-2,3-DIHYDROINDEN-1-ONE;6-BROMO-1-INDANONE;6-BROMO-INDAN-1-ONE;6-BROMO INDANONE;6-Bromo-1-indanone,98%;1H-Inden-1-one,6-bromo-2,3-dihydro-;6

Factory Supply 6-Bromo-1-indanone

Cas:14548-39-1

Min.Order:1 Gram

Negotiable

Type:Other

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Henan Tianfu Chemical Co., Ltd.

14548-39-1 6-Bromoindanone Basic information Product Name: 6-Bromoindanone Synonyms: 6-BROMO-2,3-DIHYDROINDEN-1-ONE;6-BROMO-1-INDANONE;6-BROMO-INDAN-1-ONE;6-BROMO INDANONE;6-Bromo-1-in

6-Bromoindanone

Cas:14548-39-1

Min.Order:1 Metric Ton

Negotiable

Type:Lab/Research institutions

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Jinan Finer Chemical Co., Ltd

Product Description Product website: http://www.finerchem.com Product Name 6-Bromoindanone CAS No. 14548-39-1

6-Bromoindanone

Cas:14548-39-1

Min.Order:1 Gram

FOB Price: $12.0

Type:Lab/Research institutions

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Pharmaceutical Grade CAS 14548-39-1 with competitive price

Cas:14548-39-1

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages High purity, all above 98.5%, no impurities after dissolution We will test each batch to ensure quality OEM and private brand services designed for free Various cap colors available We can also provide MT1 peptide powd

6-Bromoindanone

Cas:14548-39-1

Min.Order:1 Kilogram

FOB Price: $50.0 / 100.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

CAS No. 14548-39-1 Other Names 6-Bromoindanone MF C9H7BrO EINECS No. 688-934-0 Type Pharmaceutical Intermediates, Syntheses Material Interme

6-Bromoindanone

Cas:14548-39-1

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

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Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

6-Bromoindanone

Cas:14548-39-1

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

1H-Inden-1-one,6-bromo-2,3-dihydro- 14548-39-1

Cas:14548-39-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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LIDE PHARMACEUTICALS LIMITED

Advantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the

1H-Inden-1-one,6-bromo-2,3-dihydro-/ LIDE PHARMA- Factory supply / Best price

Cas:14548-39-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese

6-Bromoindanone

Cas:14548-39-1

Min.Order:1 Kilogram

FOB Price: $76.0 / 85.0

Type:Trading Company

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Hebei Mojin Biotechnology Co.,Ltd

1. Customs clearance 1) By Express: Normally there is no specical need for the recipient to clear the customs. If the customs has an objection,our rich experienced and professional group will help you clear the customs. 2) By Air and by Sea: Our

Best Price CAS 14548-39-1 6-Bromoindanone C9H7BrO 99%

Cas:14548-39-1

Min.Order:20 Kilogram

FOB Price: $10.0 / 25.0

Type:Trading Company

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

1H-Inden-1-one,6-bromo-2,3-dihydro-

Cas:14548-39-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hangzhou JINLAN Pharm-Drugs Technology Co., Ltd

Specification:USP/EP Month production ablity:50kg/Month Low price& High quality Manufacturer Appearance:white powder Storage:Room Temperature Package:in aluminum bag and foil bag or as customers' require Application:14548-39-1 Transportat

6-Bromoindan-1-one

Cas:14548-39-1

Min.Order:1 Gram

Negotiable

Type:Other

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

6-Bromoindanone

Cas:14548-39-1

Min.Order:0

Negotiable

Type:Manufacturers

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Triumph International Development Limilted

Appearance:white or light yellow crystalline powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:By

6-Bromo-1-indanone

Cas:14548-39-1

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

6-BroMo-1-indanone

Cas:14548-39-1

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

6-BroMo-1-indanone

Cas:14548-39-1

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

6-bromo-2,3-dihydro-1H-inden-1-one

Cas:14548-39-1

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Hope Chem Co., Ltd

1. Product advantages: exquisite appearance and unique functions. 2. Product Advantages: Our products are the best,fast speed ,in large stock 3. High-quality products and thoughtful service are your greatest satisfaction. 4. The product

6-Bromo-1-indanone

Cas:14548-39-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hangzhou Lingrui Chemical Co.,Ltd.

advantage: 1. The best price, satisfactory quality; 2. customers have the right to choose the delivery of parcels (EMS, DHL, FedEx, UPS); 3. customers have the right to choose from the recent effective packaging methods of their products packaging

6-Bromoindanone Best price/In stock

Cas:14548-39-1

Min.Order:1 Gram

Negotiable

Type:Other

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

1H-Inden-1-one,6-bromo-2,3-dihydro-

Cas:14548-39-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Chemlyte Solutions

Chemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff

Featured products 6-BroMo-1-indanone

Cas:14548-39-1

Min.Order:100 Gram

Negotiable

Type:Other

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SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

6-BroMo-1-indanone

Cas:14548-39-1

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

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Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

6-Bromo-1-indanone, >=99%

Cas:14548-39-1

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

6-BroMo-1-indanone

Cas:14548-39-1

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Synthetic route

3-(4-bromophenyl)propionic acid
1643-30-7

3-(4-bromophenyl)propionic acid

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

Conditions
ConditionsYield
With trifluorormethanesulfonic acid In dichloromethane at 80℃; for 1h; Friedel-Crafts Acylation; High pressure; Inert atmosphere; Green chemistry;100%
With chlorosulfonic acid at 0℃; for 1h; Friedel-Crafts reaction;98%
With aluminum (III) chloride In dichloromethane for 3h; Reflux;80%
6-hydroxy-1-indanone
62803-47-8

6-hydroxy-1-indanone

tert-butyldimethylsilyl chloride
18162-48-6

tert-butyldimethylsilyl chloride

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

Conditions
ConditionsYield
With 1H-imidazole In dichloromethane98%
3-(4-bromophenyl)propanoyl chloride
55394-81-5

3-(4-bromophenyl)propanoyl chloride

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

Conditions
ConditionsYield
With aluminium trichloride In carbon disulfide91%
With aluminium trichloride In carbon disulfide for 3h; Heating / reflux;47%
With aluminium trichloride In dichloromethane
C15H13BrN2O3
1383443-48-8

C15H13BrN2O3

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

Conditions
ConditionsYield
With trifluorormethanesulfonic acid In chloroform at 50℃; for 4h; Friedel Crafts acylation; Inert atmosphere;88%
6-aminoindan-1-one
69975-65-1

6-aminoindan-1-one

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

Conditions
ConditionsYield
Stage #1: 6-aminoindan-1-one With hydrogenchloride; sodium nitrite In water at 0℃;
Stage #2: With copper(I) bromide In water at 0 - 20℃; for 2h;
71%
3-(4-bromophenyl)propionic acid
1643-30-7

3-(4-bromophenyl)propionic acid

A

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

B

6-bromo-2-[3-(4-bromophenyl)-1-oxopropyl]-indan-1-one
1610628-81-3

6-bromo-2-[3-(4-bromophenyl)-1-oxopropyl]-indan-1-one

Conditions
ConditionsYield
With trifluorormethanesulfonic acid; trifluoroacetic acid In dichloromethane at 20℃; for 2h;A 8%
B 70%
3-(4-bromophenyl)propionic acid
1643-30-7

3-(4-bromophenyl)propionic acid

A

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

B

C18H14Br2O2

C18H14Br2O2

Conditions
ConditionsYield
Stage #1: 3-(4-bromophenyl)propionic acid With trifluoroacetic anhydride In dichloromethane at 20℃; for 0.25h;
Stage #2: With trifluorormethanesulfonic acid In dichloromethane at 20℃; for 2h;
A 8%
B 70%
Stage #1: 3-(4-bromophenyl)propionic acid With trifluoroacetic anhydride In dichloromethane at 20℃; for 0.25h;
Stage #2: With trifluorormethanesulfonic acid In dichloromethane at 20℃; for 2h;
A 62%
B n/a
inden-1-one
83-33-0

inden-1-one

A

4-bromo-2,3-dihydroinden-1-one
15115-60-3

4-bromo-2,3-dihydroinden-1-one

B

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

C

5-Bromo-1-indanone
34598-49-7

5-Bromo-1-indanone

D

4,7-dibromo-1-indanone
103515-98-6

4,7-dibromo-1-indanone

Conditions
ConditionsYield
With aluminium trichloride; bromine at 110℃; for 0.5h; Further byproducts given;A 47%
B 21%
C 3%
D 2%
inden-1-one
83-33-0

inden-1-one

A

4-bromo-2,3-dihydroinden-1-one
15115-60-3

4-bromo-2,3-dihydroinden-1-one

B

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

C

5-Bromo-1-indanone
34598-49-7

5-Bromo-1-indanone

D

4,6-dibromo-1-indanone

4,6-dibromo-1-indanone

Conditions
ConditionsYield
With aluminium trichloride; bromine at 110℃; for 0.5h; Further byproducts given;A 47%
B 21%
C 3%
D 1%
6-bromo-1H-indene
33065-61-1

6-bromo-1H-indene

A

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

B

(+)-(1S)-6-bromoinden-1-ol

(+)-(1S)-6-bromoinden-1-ol

Conditions
ConditionsYield
With Pseudomonas putida UV4 for 7h;A 28%
B 16%
inden-1-one
83-33-0

inden-1-one

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

Conditions
ConditionsYield
Stage #1: inden-1-one With aluminum (III) chloride for 0.216667h;
Stage #2: With bromine at 0 - 80℃; for 0.25h;
19%
Multi-step reaction with 3 steps
1.1: potassium nitrate; sulfuric acid / 1.5 h / 0 - 5 °C
2.1: iron; ammonium chloride / water; ethanol / 80 °C
3.1: sodium nitrite; hydrogenchloride / water / 0 °C
3.2: 2 h / 0 - 20 °C
View Scheme
5-bromo-1H-indene
75476-78-7

5-bromo-1H-indene

A

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

B

5-bromo-1,2-dihydroxyindane

5-bromo-1,2-dihydroxyindane

Conditions
ConditionsYield
With Pseudomonas putida UV4 for 7h;A 4%
B n/a
3-(4-bromophenyl)propionic acid
1643-30-7

3-(4-bromophenyl)propionic acid

A

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

B

3-(4-bromo-3-sulfo-phenyl)-propionic acid

3-(4-bromo-3-sulfo-phenyl)-propionic acid

Conditions
ConditionsYield
With sulfuric acid
inden-1-one
83-33-0

inden-1-one

A

4-bromo-2,3-dihydroinden-1-one
15115-60-3

4-bromo-2,3-dihydroinden-1-one

B

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

Conditions
ConditionsYield
With aluminium trichloride; bromine 1.) 10 min, 2.) 80 deg C, 5 min; Yield given. Multistep reaction. Yields of byproduct given;
With hydrogenchloride; bromine; aluminium trichloride In tetrahydrofuran; hexane; water
3-(4-bromophenyl)propionic acid
1643-30-7

3-(4-bromophenyl)propionic acid

sulfuric acid
7664-93-9

sulfuric acid

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

p-bromo-hydrocinnamic acid

p-bromo-hydrocinnamic acid

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

Conditions
ConditionsYield
With sulfuric acid at 145℃; man giesst auf Eis;
5-(4-bromo-benzyl)-2,2-dimethyl-[1,3]dioxane-4,6-dione
198494-75-6

5-(4-bromo-benzyl)-2,2-dimethyl-[1,3]dioxane-4,6-dione

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: H2O / acetonitrile / 0.5 h / 120 °C / microwave irradiation
2: 98 percent / chlorosulfonic acid / 1 h / 0 °C
View Scheme
4-bromo-benzaldehyde
1122-91-4

4-bromo-benzaldehyde

LiPh2InH2

LiPh2InH2

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 63 percent / triethylammonium formate
2: H2O / acetonitrile / 0.5 h / 120 °C / microwave irradiation
3: 98 percent / chlorosulfonic acid / 1 h / 0 °C
View Scheme
trans-4-bromocinnamic acid
1200-07-3, 5676-63-1, 17916-60-8

trans-4-bromocinnamic acid

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: H2 / Pd/C / methanol
2: (COCl)2 / CH2Cl2
3: aluminum trichloride / CH2Cl2
View Scheme
4-bromo-benzaldehyde
1122-91-4

4-bromo-benzaldehyde

(S)-(Fmoc-amino)-(4-fluoro-phenyl)-acetic acid on Wang resin

(S)-(Fmoc-amino)-(4-fluoro-phenyl)-acetic acid on Wang resin

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: piperidine / pyridine
2: H2 / Pd/C / methanol
3: (COCl)2 / CH2Cl2
4: aluminum trichloride / CH2Cl2
View Scheme
5-Bromo-1-indanone
34598-49-7

5-Bromo-1-indanone

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 90 percent / sodium borohydride / methanol / 2 h / 20 °C
2: 92 percent / p-TsOH / benzene / 2 h / Heating
3: 28 percent / Pseudomonas putida UV4 / 7 h
View Scheme
5-bromo-1-indanol
34598-50-0

5-bromo-1-indanol

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 92 percent / p-TsOH / benzene / 2 h / Heating
2: 28 percent / Pseudomonas putida UV4 / 7 h
View Scheme
6-Bromo-2,3-dihydro-1H-inden-1-ol
75476-86-7

6-Bromo-2,3-dihydro-1H-inden-1-ol

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 87 percent / p-TsOH / benzene / 2 h / Heating
2: 4 percent / Pseudomonas putida UV4 / 7 h
View Scheme
diethyl 2-(4-bromobenzyl)malonate
70146-78-0

diethyl 2-(4-bromobenzyl)malonate

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: aq. KOH / 4.5 h / Heating
2: aq. H2SO4 / 18 h / Heating
3: (COCl)2; DMF / 18 h / 20 °C
4: AlCl3 / CH2Cl2 / 3.5 h / Heating
View Scheme
Multi-step reaction with 4 steps
1: 95 percent / KOH / acetic acid; H2O; tetrahydrofuran
2: 85 percent / 165 °C
3: thionyl chloride
4: 91 percent / AlCl3 / CS2
View Scheme
2-[(4-bromophenyl)methyl]propanedioic acid
92013-18-8

2-[(4-bromophenyl)methyl]propanedioic acid

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: aq. H2SO4 / 18 h / Heating
2: (COCl)2; DMF / 18 h / 20 °C
3: AlCl3 / CH2Cl2 / 3.5 h / Heating
View Scheme
Multi-step reaction with 3 steps
1: 85 percent / 165 °C
2: thionyl chloride
3: 91 percent / AlCl3 / CS2
View Scheme
1-bromomethyl-4-bromobenzene
589-15-1

1-bromomethyl-4-bromobenzene

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: NaH / 1,2-dimethoxy-ethane / 2 h / 20 °C
1.2: 57 percent / 1,2-dimethoxy-ethane / 18 h / Heating
2.1: aq. KOH / 4.5 h / Heating
3.1: aq. H2SO4 / 18 h / Heating
4.1: (COCl)2; DMF / 18 h / 20 °C
5.1: AlCl3 / CH2Cl2 / 3.5 h / Heating
View Scheme
Multi-step reaction with 5 steps
1: 74 percent / NaOEt / Heating
2: 95 percent / KOH / acetic acid; H2O; tetrahydrofuran
3: 85 percent / 165 °C
4: thionyl chloride
5: 91 percent / AlCl3 / CS2
View Scheme
Multi-step reaction with 2 steps
1: trifluoroacetic acid; lithium diisopropyl amide / tetrahydrofuran
2: hydrogenchloride; thionyl chloride / aluminium trichloride / dichloromethane
View Scheme
methyl 4-bromocinnamate
3650-78-0, 71205-17-9, 84878-00-2

methyl 4-bromocinnamate

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: hydrogen; palladium 10% on activated carbon / methanol
2: trifluorormethanesulfonic acid / 25 °C / Cooling with ice
View Scheme
methyl 3-(4-bromopehynl)propanoate
75567-84-9

methyl 3-(4-bromopehynl)propanoate

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

Conditions
ConditionsYield
With trifluorormethanesulfonic acid at 25℃; Cooling with ice;
6-nitroindan-1-one
24623-24-3

6-nitroindan-1-one

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: iron; ammonium chloride / water; ethanol / 80 °C
2.1: sodium nitrite; hydrogenchloride / water / 0 °C
2.2: 2 h / 0 - 20 °C
View Scheme
6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

6-Bromo-2,3-dihydro-1H-inden-1-ol
75476-86-7

6-Bromo-2,3-dihydro-1H-inden-1-ol

Conditions
ConditionsYield
With sodium tetrahydroborate In ethanol at 10 - 20℃; for 3h;100%
With sodium borohydrid In methanol99%
With methanol; sodium tetrahydroborate at 20℃; for 2h; Temperature; Concentration; Inert atmosphere;99%
6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

N-4-chlorophenylhydrazine
1073-69-4

N-4-chlorophenylhydrazine

N-(6-Bromo-indan-1-ylidene)-N'-(4-chloro-phenyl)-hydrazine

N-(6-Bromo-indan-1-ylidene)-N'-(4-chloro-phenyl)-hydrazine

Conditions
ConditionsYield
With acetic acid In ethanol for 0.5h; Heating / reflux;100%
6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

phenylboronic acid
98-80-6

phenylboronic acid

6-phenyl-1-indanone
170497-64-0

6-phenyl-1-indanone

Conditions
ConditionsYield
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In ethanol; benzene Suzuki coupling; Heating;99%
6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

dimethyl zinc(II)
544-97-8

dimethyl zinc(II)

6-bromo-1,1-dimethyl-2,3-dihydro-1H-indene
67159-88-0

6-bromo-1,1-dimethyl-2,3-dihydro-1H-indene

Conditions
ConditionsYield
Stage #1: dimethyl zinc(II) With titanium tetrachloride In dichloromethane; toluene at -30 - 20℃; for 0.5h; Inert atmosphere;
Stage #2: 6-bromoindan-1-one In dichloromethane; toluene at -10℃; for 4h;
99%
Stage #1: dimethyl zinc(II) With titanium(III) chloride In dichloromethane; toluene at 40℃; for 0.333333h;
Stage #2: 6-bromoindan-1-one In dichloromethane; toluene at 20℃; for 18h;
94%
Stage #1: dimethyl zinc(II) With titanium tetrachloride In dichloromethane; toluene at 40℃; for 0.333333h;
Stage #2: 6-bromoindan-1-one In dichloromethane; toluene at 20℃; for 18h;
94%
methanesulfonamide
3144-09-0

methanesulfonamide

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

C10H11NO3S

C10H11NO3S

Conditions
ConditionsYield
With bis(η3-allyl-μ-chloropalladium(II)); potassium carbonate; tert-butyl XPhos In 1,4-dioxane at 80℃; for 3h; Inert atmosphere; Schlenk technique;98%
6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

potassium isopropenyltrifluoroborane

potassium isopropenyltrifluoroborane

C12H12O

C12H12O

Conditions
ConditionsYield
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; potassium carbonate In 1,4-dioxane; water at 90℃; for 5h; Inert atmosphere; Sealed tube;97%
6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

bis(pinacol)diborane
73183-34-3

bis(pinacol)diborane

6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2,3-dihydro-1 H-inden-1-one
915402-06-1

6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2,3-dihydro-1 H-inden-1-one

Conditions
ConditionsYield
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate In toluene at 90℃; for 12h; Inert atmosphere;96%
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate In toluene at 90℃; for 12h; Inert atmosphere;96%
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate In N,N-dimethyl-formamide at 100℃; for 1h; Microwave irradiation;95%
6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

Methyltriphenylphosphonium bromide
1779-49-3

Methyltriphenylphosphonium bromide

6-bromo-1-methylenyl-2,3-dihydro-1H-indene

6-bromo-1-methylenyl-2,3-dihydro-1H-indene

Conditions
ConditionsYield
Stage #1: Methyltriphenylphosphonium bromide With potassium tert-butylate In tetrahydrofuran at 20℃; for 1h; Inert atmosphere;
Stage #2: 6-bromoindan-1-one In tetrahydrofuran at 20℃; Inert atmosphere;
96%
Stage #1: Methyltriphenylphosphonium bromide With potassium tert-butylate In tetrahydrofuran at 20℃; for 0.583333h;
Stage #2: 6-bromoindan-1-one In tetrahydrofuran at 20℃; for 1h;
Stage #3: With water In tetrahydrofuran
93.4%
Stage #1: Methyltriphenylphosphonium bromide With n-butyllithium In tetrahydrofuran; hexanes at 0℃; for 1h;
Stage #2: 6-bromoindan-1-one In tetrahydrofuran; hexanes
62%
Stage #1: Methyltriphenylphosphonium bromide With potassium tert-butylate In tetrahydrofuran for 1h; Inert atmosphere; Cooling with ice;
Stage #2: 6-bromoindan-1-one In tetrahydrofuran for 0.5h; Cooling with ice;
60%
6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

ethylene glycol
107-21-1

ethylene glycol

6‘-bromo-2‘,3‘-dihydrospiro[[1,3]dioxolane-2,1‘-indene]
866848-94-4

6‘-bromo-2‘,3‘-dihydrospiro[[1,3]dioxolane-2,1‘-indene]

Conditions
ConditionsYield
With toluene-4-sulfonic acid In benzene at 115℃; for 48h; Dean-Stark; Inert atmosphere;95%
With toluene-4-sulfonic acid In benzene at 115℃; for 48h; Dean-Stark; Inert atmosphere;95%
With toluene-4-sulfonic acid In benzene Heating;
With toluene-4-sulfonic acid In benzene for 24h; Heating / reflux;
With toluene-4-sulfonic acid In toluene at 125℃;10.5 g
6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

methyl iodide
74-88-4

methyl iodide

6-bromo-2,2-dimethyl-2,3-dihydro-1H-inden-1-one

6-bromo-2,2-dimethyl-2,3-dihydro-1H-inden-1-one

Conditions
ConditionsYield
With sodium hydride In tetrahydrofuran; mineral oil at 23℃; for 16h; Inert atmosphere;95%
Stage #1: 6-bromoindan-1-one; methyl iodide In tetrahydrofuran for 0.25h;
Stage #2: With sodium hydride In tetrahydrofuran; water for 2.5h;
84%
Stage #1: 6-bromoindan-1-one; methyl iodide In tetrahydrofuran at 20℃; for 0.25h;
Stage #2: With sodium hydride In tetrahydrofuran for 2h;
78.6%
6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

3,4-(methylenedioxy)-benzeneboronic acid
94839-07-3

3,4-(methylenedioxy)-benzeneboronic acid

6-benzo[1,3]dioxo-5-ylindan-1-one

6-benzo[1,3]dioxo-5-ylindan-1-one

Conditions
ConditionsYield
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In ethanol; benzene Suzuki coupling; Heating;94%
6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

6-bromo-1,1-dimethyl-2,3-dihydro-1H-indene
67159-88-0

6-bromo-1,1-dimethyl-2,3-dihydro-1H-indene

Conditions
ConditionsYield
Stage #1: With dimethyl zinc(II); titanium tetrachloride In dichloromethane; toluene at -40℃; for 0.333333h;
Stage #2: 6-bromoindan-1-one In dichloromethane; toluene at -40 - 20℃; for 18h;
94%
6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

6-bromo-2,3-dihydro-1H-inden-1-one oxime

6-bromo-2,3-dihydro-1H-inden-1-one oxime

Conditions
ConditionsYield
With hydroxylamine hydrochloride; potassium hydroxide In methanol; water for 3h; Reflux;94%
With hydroxylamine hydrochloride In methanol for 1h; Heating;
With pyridine; hydroxylamine hydrochloride In ethanol at 20℃; for 2h;
6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

(S,E)-N-(1-(4-bromophenyl)ethylidene)-2-methylpropane-2-sulfinamide
1039750-63-4

(S,E)-N-(1-(4-bromophenyl)ethylidene)-2-methylpropane-2-sulfinamide

C21H23Br2NO2S
1616493-88-9

C21H23Br2NO2S

Conditions
ConditionsYield
Stage #1: 6-bromoindan-1-one With lithium hexamethyldisilazane In tetrahydrofuran at -78℃; for 0.666667h; Inert atmosphere; Sealed tube;
Stage #2: (S,E)-N-(1-(4-bromophenyl)ethylidene)-2-methylpropane-2-sulfinamide In tetrahydrofuran at -78℃; for 24h; Inert atmosphere; Sealed tube; diastereoselective reaction;
94%
6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

4-biphenylboronic acid
5122-94-1

4-biphenylboronic acid

6-biphenyl-4-ylindan-1-one

6-biphenyl-4-ylindan-1-one

Conditions
ConditionsYield
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In ethanol; benzene Suzuki coupling; Heating;93%
(SS)-2-methyl-N-(2,2,2-trifluoroethylidene)-propane-2-sulfinamide

(SS)-2-methyl-N-(2,2,2-trifluoroethylidene)-propane-2-sulfinamide

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

(S)-N-((S)-1-((S)-6-bromo-1-oxo-2,3-dihydro-1H-inden-2-yl)-2,2,2-trifluoroethyl)-2-methylpropane-2-sulfinamide
1556948-49-2

(S)-N-((S)-1-((S)-6-bromo-1-oxo-2,3-dihydro-1H-inden-2-yl)-2,2,2-trifluoroethyl)-2-methylpropane-2-sulfinamide

Conditions
ConditionsYield
Stage #1: 6-bromoindan-1-one With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.666667h; Inert atmosphere;
Stage #2: (SS)-2-methyl-N-(2,2,2-trifluoroethylidene)-propane-2-sulfinamide In tetrahydrofuran at -78℃; for 4h; Inert atmosphere; diastereoselective reaction;
93%
6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

trans-2-(trifluoromethyl)cyclopropylboronic acid MIDA ester

trans-2-(trifluoromethyl)cyclopropylboronic acid MIDA ester

trans-6-(2-(trifluoromethyl)cyclopropyl)-2,3-dihydro-1H-inden-1-one

trans-6-(2-(trifluoromethyl)cyclopropyl)-2,3-dihydro-1H-inden-1-one

Conditions
ConditionsYield
With potassium carbonate; ruphos; palladium diacetate In water; toluene at 100℃; Suzuki Coupling; Inert atmosphere; Sealed vial;90%
6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

trans-2-(trifluoromethyl)cyclopropylboronic diester of N-methyliminodiacetic acid

trans-2-(trifluoromethyl)cyclopropylboronic diester of N-methyliminodiacetic acid

trans-6-(2-(trifluoromethyl)cyclopropyl)-2,3-dihydro-1H-inden-1-one

trans-6-(2-(trifluoromethyl)cyclopropyl)-2,3-dihydro-1H-inden-1-one

Conditions
ConditionsYield
With water; palladium diacetate; potassium carbonate; ruphos In toluene at 100℃; for 6h; Suzuki Coupling; Inert atmosphere;90%
thiophene boronic acid
6165-68-0

thiophene boronic acid

6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

6-thiophen-2-ylindan-1-one

6-thiophen-2-ylindan-1-one

Conditions
ConditionsYield
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In ethanol; benzene Suzuki coupling; Heating;89%
6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

p-methoxybenzyl chloride
824-94-2

p-methoxybenzyl chloride

6-bromo-1-((4-methoxybenzyl)oxy)-2,3-dihydro-1H-indene

6-bromo-1-((4-methoxybenzyl)oxy)-2,3-dihydro-1H-indene

Conditions
ConditionsYield
Stage #1: 6-bromoindan-1-one With sodium hydride In N,N-dimethyl-formamide at 4 - 23℃; for 1h;
Stage #2: p-methoxybenzyl chloride In N,N-dimethyl-formamide at 10 - 23℃; for 14h;
87%
6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

methylamine
74-89-5

methylamine

6-bromo-N-methyl-2,3-dihydro-1H-inden-1-amine
371251-07-9

6-bromo-N-methyl-2,3-dihydro-1H-inden-1-amine

Conditions
ConditionsYield
Stage #1: 6-bromoindan-1-one; methylamine In methanol at 20℃; for 3.5h;
Stage #2: With sodium tetrahydroborate In methanol at 20℃;
87%
Stage #1: 6-bromoindan-1-one; methylamine In methanol at 20℃; for 3.5h;
Stage #2: With methanol; sodium tetrahydroborate at 20℃;
6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

2-hydrazinobenzoic acid hydrochloride
33906-30-8, 52356-01-1

2-hydrazinobenzoic acid hydrochloride

o-[(2,3-dihydro-6-bromoinden-3-ylidene)hydrazino]-benzoic acid

o-[(2,3-dihydro-6-bromoinden-3-ylidene)hydrazino]-benzoic acid

Conditions
ConditionsYield
In ethanol; water at 20℃; for 1h;86%
6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

dimethyl amine
124-40-3

dimethyl amine

6-bromo-2,3-dihydro-N,N-dimethyl-1H-inden-1-amine
371249-89-7

6-bromo-2,3-dihydro-N,N-dimethyl-1H-inden-1-amine

Conditions
ConditionsYield
With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 120℃; for 0.0833333h; Microwave irradiation;85%
With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 120℃; for 0.0833333h; Product distribution / selectivity; Inert atmosphere; Microwave irradiation;85%
Stage #1: 6-bromoindan-1-one; dimethyl amine In 1,2-dichloro-ethane Sealed tube;
Stage #2: With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 120℃; for 0.0833333h; Product distribution / selectivity; Inert atmosphere; Microwave irradiation;
85%
6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

3,8,13-tribromo-10,15-dihydro-5H-diindeno[1,2-a:1',2'-c]fluorene

3,8,13-tribromo-10,15-dihydro-5H-diindeno[1,2-a:1',2'-c]fluorene

Conditions
ConditionsYield
With toluene-4-sulfonic acid; propionic acid In 1,2-dichloro-benzene at 105℃; for 16h;84%
With toluene-4-sulfonic acid; propionic acid In 1,2-dichloro-benzene at 105℃; for 16h;84%
With PPA at 120℃; for 12h;24%
6-bromoindan-1-one
14548-39-1

6-bromoindan-1-one

1,3,5-trimethylpyrazole-4-boronic acid pinacol ester
844891-04-9

1,3,5-trimethylpyrazole-4-boronic acid pinacol ester

6-(1,3,5-Trimethyl-1 H-pyrazol-4-yl)-indan-1-one
1096520-73-8

6-(1,3,5-Trimethyl-1 H-pyrazol-4-yl)-indan-1-one

Conditions
ConditionsYield
With potassium carbonate; tetrakis(triphenylphosphine) palladium(0) In 1,2-dimethoxyethane; water at 100℃; for 3h;84%

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