As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:146-77-0
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inquiry6-Amino-2-Chloropurine Riboside/2-Chloroadenosine[CAS:146-77-0] Item Inspection Standard Result Appearance White or pale yellow powder
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inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Product name: 2-chloro-adenosine Shelf life:2 years Purity:98%, 99% KONO Chem Co., Ltd, is a leading producer of standardized herbal extracts, natural active ingredients and APIs for pharmaceutical, health food and cosmetic industries. Ann
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inquiryLIDE PHARMACEUTICALS LIMITED is a professional chemicals and APIs leading manufacturer in China. Our core business line covers APIs, Intermediates, Herb extract, etc.
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiry1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W
Cas:146-77-0
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inquiryProduct Name 2-Chloroadenosine Appearance White Powder Grade Standard Excellent Storage Cool Dry Place Appearance: White powder Stor
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inquiry2-Chloroadenosine CAS:146-77-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedi
Cas:146-77-0
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inquiryPRODUCT DETAILS
Cas:146-77-0
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryAppearance:White to Off-White Crystalline Sold Storage:Store at +4°C Package:As customer request Application:Used for research and industrial manufacture.A selective A1-adenosine receptor agonist. Induces apoptosis Transportatio
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryNewCan Biotech Limited was established in 2021 and is primarily engaged in the research, development, production, and sales of sugars, nucleosides, nucleotides, phosphorylated monomers, as well as next-generation antiviral and antitumor drug intermed
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:146-77-0
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Cas:146-77-0
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inquiry2',3',5'-tri-O-acetyl-2-chloroadenosine
2-Chloroadenosine
Conditions | Yield |
---|---|
With methanol; sodium methylate for 1h; Reflux; | 96% |
Conditions | Yield |
---|---|
With hydrogenchloride; potassium dihydrogenphosphate; potassium hydroxide In water; dimethyl sulfoxide at 58 - 61℃; for 4h; pH=7.1-7.2; Enzymatic reaction; | 85% |
With potassium phosphate; Geobacillus thermoglucosidasius purine nucleoside phosphorylase; Thermus thermophilus pyrimidine nucleoside phosphorylase In water at 70℃; for 1h; pH=7; Enzymatic reaction; | |
With dipotassium hydrogenphosphate; purine nucleoside phosphorylase; pyrimidine nucleoside phosphorylase; glycine In aq. buffer at 60℃; pH=9; Equilibrium constant; Enzymatic reaction; |
(2R,3R,4R,5R)-4-(acetyloxy)-2-[(acetyloxy)methyl]-5-(2,6-dichloro-9H-purin-9-yl)tetrahydro-3-furanyl acetate
2-Chloroadenosine
Conditions | Yield |
---|---|
With ethanol; ammonia at 20℃; | 75% |
With ammonia In ethanol at 100℃; for 24h; | 73% |
With ammonium hydroxide In tetrahydrofuran for 72h; Ambient temperature; Yield given; |
2-chloro-2′,3′,5′-tri-O-(t-butyldimethylsilyl)adenosine
2-Chloroadenosine
Conditions | Yield |
---|---|
With potassium fluoride In methanol at 80℃; for 24h; | 74% |
Conditions | Yield |
---|---|
With hydrogenchloride; potassium dihydrogenphosphate; potassium hydroxide In water; dimethyl sulfoxide at 58 - 61℃; for 4h; pH=7.1-7.2; Enzymatic reaction; | 70% |
With Trypanosoma brucei purine nucleoside 2'-deoxyribosyltransferase, Y5F mutant In aq. phosphate buffer at 50℃; for 0.5h; pH=6.5; Enzymatic reaction; |
6-amino-2-chloro-9-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-9H-purine
2-Chloroadenosine
Conditions | Yield |
---|---|
With sodium methylate In methanol at 20℃; for 7h; | 67% |
2-chloro-6-methoxy-purine riboside
2-Chloroadenosine
Conditions | Yield |
---|---|
With methanol; ammonia |
2,8-dichloro-adenosine
2-Chloroadenosine
Conditions | Yield |
---|---|
With sodium hydroxide; Pd-BaSO4 Hydrogenation; |
2-Chloroadenosine
Conditions | Yield |
---|---|
With methanol; ammonia |
2,3,5-tri-O-acetyl-α-D-ribofuranosyl chloride
2-Chloroadenosine
Conditions | Yield |
---|---|
With xylene und Behandeln des Reaktionsprodukts mit methanol.NH3; |
(2R,3R,4R,5R)-2-((benzoyloxy)methyl)-5-(2,6-dichloro-9H-purin-9-yl)tetrahydrofuran-3,4-diyl dibenzoate
2-Chloroadenosine
Conditions | Yield |
---|---|
With ammonia In methanol at 20℃; | |
With ammonia In methanol at 100℃; for 24h; Autoclave; | 14 g |
With ammonia In methanol at 100℃; for 24h; Autoclave; | 14 g |
2-Chloroadenosine
Conditions | Yield |
---|---|
With ammonia In methanol at 60℃; for 11h; |
9-(2,3,5-tri-O-acetyl-β-D-ribofuranosyl)-2-chloro-6-(2-propylimidazol-1-yl)purine
2-Chloroadenosine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NaI / acetonitrile / 1.5 h / 60 °C 2: NH3 / methanol / 11 h / 60 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: SnCl4 / acetonitrile / 20 °C 2: NH3 / methanol / 20 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: SnCl4 / acetonitrile / 20 °C 2: NH3 / methanol / 20 °C View Scheme | |
Multi-step reaction with 3 steps 1: tin(IV) chloride / 0.25 h / 90 - 120 °C 2: ammonia / methanol / 24 h / 100 °C / Autoclave 3: 24 h / 20 °C View Scheme |
2-amino-6-chloro-9-(2,3,5-tri-O-acetyl-β-D-ribofuranosyl)purine
2-Chloroadenosine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Ph3CCl, K2CO3, isoamyl nitrite / CH2Cl2 / 0.5 h / Heating 2: conc. NH4OH / tetrahydrofuran / 72 h / Ambient temperature View Scheme | |
Multi-step reaction with 2 steps 1: benzyltriethylammonium nitrite; acetyl chloride / dichloromethane / 1 h / 0 °C / Inert atmosphere; Cooling with ice 2: ammonia / ethanol / 72 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: benzyltriethylammonium nitrite; acetyl chloride / dichloromethane / Inert atmosphere; Cooling with ice 2: ammonia; ethanol / 20 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: pyridine / dimethylformamide / 4.5 h / 75 °C 2: 70.85 percent / Et4NCl, Me2NPh, POCl3 / acetonitrile / 0.17 h / Heating 3: Ph3CCl, K2CO3, isoamyl nitrite / CH2Cl2 / 0.5 h / Heating 4: conc. NH4OH / tetrahydrofuran / 72 h / Ambient temperature View Scheme | |
Multi-step reaction with 4 steps 1: dmap; N,N-dimethyl-ethanamine / acetonitrile / 1 h / 20 °C 2: tetraethylammonium chloride; N,N-dimethyl-aniline; trichlorophosphate / 100 °C 3: benzyltriethylammonium nitrite; acetyl chloride / dichloromethane / 1 h / 0 °C / Inert atmosphere; Cooling with ice 4: ammonia / ethanol / 72 h / 20 °C View Scheme | |
Multi-step reaction with 4 steps 1: N,N-dimethyl-ethanamine; dmap / acetonitrile 2: tetraethylammonium chloride; trichlorophosphate; N,N-dimethyl-aniline / Inert atmosphere 3: benzyltriethylammonium nitrite; acetyl chloride / dichloromethane / Inert atmosphere; Cooling with ice 4: ammonia; ethanol / 20 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 70.85 percent / Et4NCl, Me2NPh, POCl3 / acetonitrile / 0.17 h / Heating 2: Ph3CCl, K2CO3, isoamyl nitrite / CH2Cl2 / 0.5 h / Heating 3: conc. NH4OH / tetrahydrofuran / 72 h / Ambient temperature View Scheme | |
Multi-step reaction with 3 steps 1: tetraethylammonium chloride; N,N-dimethyl-aniline; trichlorophosphate / 100 °C 2: benzyltriethylammonium nitrite; acetyl chloride / dichloromethane / 1 h / 0 °C / Inert atmosphere; Cooling with ice 3: ammonia / ethanol / 72 h / 20 °C View Scheme | |
Multi-step reaction with 3 steps 1: tetraethylammonium chloride; trichlorophosphate; N,N-dimethyl-aniline / Inert atmosphere 2: benzyltriethylammonium nitrite; acetyl chloride / dichloromethane / Inert atmosphere; Cooling with ice 3: ammonia; ethanol / 20 °C View Scheme |
Conditions | Yield |
---|---|
In tetrahydrofuran |
Conditions | Yield |
---|---|
With potassium dihydrogenphosphate; recombinant E.coli phosphopentomutase; recombinant E.coli purine nucleoside phosphorylase; recombinant E.coli ribokinase; potassium chloride; ATP; manganese(ll) chloride In aq. buffer at 50℃; for 0.5h; pH=7.5; Enzymatic reaction; | 90 %Chromat. |
O6-(benzotriazol-1-yl)-2-chloro-9-[2,3,5-tri-O-(t-butyldimethylsilyl)-β-D-ribofuranosyl]purine
2-Chloroadenosine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: ammonium hydroxide / 1.5 h / 20 °C 2: potassium fluoride / methanol / 24 h / 80 °C View Scheme |
O6-(benzotriazol-1H-yl)-2',3',5'-tri-O-(tert-butyldimethylsilyl)guanosine
2-Chloroadenosine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: tert.-butylnitrite; chloro-trimethyl-silane / dichloromethane / 1 h / 0 °C 2: ammonium hydroxide / 1.5 h / 20 °C 3: potassium fluoride / methanol / 24 h / 80 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: tin(IV) chloride / nitromethane / 3 h / 20 °C / Cooling with ice 2: sodium methylate; methanol / 1 h / Reflux View Scheme |
1-β-D-ribofuranosyl-1H-benzotriazole
2-Chloroadenosine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: tin(IV) chloride / nitromethane / 3 h / 20 °C / Cooling with ice 2: sodium methylate; methanol / 1 h / Reflux View Scheme |
2,6-dichloropurine riboside
2-Chloroadenosine
Conditions | Yield |
---|---|
With ammonia In methanol at 80℃; for 7h; High pressure; | |
at 20℃; for 24h; | 4.5 g |
1,2,3,5-tetraacetylribose
2-Chloroadenosine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: tin(IV) chloride / 0.25 h / 90 - 120 °C 2: ammonia / methanol / 24 h / 100 °C / Autoclave 3: 24 h / 20 °C View Scheme |
Conditions | Yield |
---|---|
With E-purine nucleoside phosphorylase-0002 In aq. buffer at 40℃; for 0.3h; pH=9; Equilibrium constant; Reagent/catalyst; Temperature; pH-value; Enzymatic reaction; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: E-pyrimidine nucleoside phosphorylase-0002; potassium dihydrogenphosphate / aq. buffer / 0.2 h / 40 °C / pH 9 / Enzymatic reaction 2: E-purine nucleoside phosphorylase-0002 / aq. buffer / 0.3 h / 40 °C / pH 9 / Enzymatic reaction View Scheme |
2-Chloroadenosine
2,2-dimethoxy-propane
((3aR,4R,6R,6aR)-6-(6-amino-2-chloro-9H-purin-9-yl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methanol
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid at 20℃; Cycloaddition; | 100% |
With perchloric acid In water at 20℃; for 8h; Reagent/catalyst; Inert atmosphere; | 88% |
With toluene-4-sulfonic acid In acetone at 45℃; | 85% |
chlorodiethylisopropylsilane
2-Chloroadenosine
2-chloro-2',3',5'-tri-O-(isopropyldiethylsilyl)adenosine
Conditions | Yield |
---|---|
With 1H-imidazole In tetrahydrofuran; DMF (N,N-dimethyl-formamide) at 20℃; for 18h; | 100% |
Conditions | Yield |
---|---|
With hydrogen sulfide; acetic acid In N-methyl-acetamide; water | 100% |
Conditions | Yield |
---|---|
With uridine phosphorylase; disodium hydrogen arsenate heptahydrate; Escherichia coli purine nucleoside phosphorylase for 48h; Enzymatic reaction; | 99% |
2-Chloroadenosine
2-hydrazinoadenosine
Conditions | Yield |
---|---|
With hydrazine hydrate at 20℃; for 4h; | 97% |
With hydrazine hydrate In water at 45 - 50℃; Temperature; | 87% |
With hydrazine at 40 - 55℃; for 2h; Product distribution / selectivity; | 81.4% |
2-Chloroadenosine
trimethyl orthoformate
2-chloro-2′,3′-O-methoxymethylideneadenosine
Conditions | Yield |
---|---|
Stage #1: 2-Chloroadenosine; trimethyl orthoformate With toluene-4-sulfonic acid at 20℃; Stage #2: at 20℃; for 3h; | 96% |
With toluene-4-sulfonic acid In N,N-dimethyl-formamide at 20℃; for 24h; | 81% |
With toluene-4-sulfonic acid at 20℃; |
acetic anhydride
2-Chloroadenosine
2',3',5'-tri-O-acetyl-2-chloroadenosine
Conditions | Yield |
---|---|
With dmap; triethylamine In acetonitrile at 50℃; | 94% |
N-BOC-1,2-diaminoethane
2-Chloroadenosine
tert-butyl (2-((6-amino-9-((2R,3R,4S,5R)-3,4-dihydroxy-5-(hydroxymethyl)tetrahydrofuran-2-yl)-9H-purin-2-yl)amino)ethyl)carbamate
Conditions | Yield |
---|---|
at 150℃; for 2h; Inert atmosphere; Neat (no solvent); | 91.4% |
2-Chloroadenosine
acetone
((3aR,4R,6R,6aR)-6-(6-amino-2-chloro-9H-purin-9-yl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methanol
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid at 20℃; Inert atmosphere; | 90% |
With toluene-4-sulfonic acid at 20℃; for 22h; Cooling with ice; Inert atmosphere; | 83% |
With toluene-4-sulfonic acid at 20℃; for 22h; Cooling with ice; | 83% |
2-Chloroadenosine
mercaptoacetic acid
2-(6-amino-9-((2R,3R,4S,5R)-3,4-dihydroxy-5-(hydroxymethyl)tetrahydrofuran-2-yl)-9H-purin-2-ylthio)acetic acid
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide | 90% |
2-Chloroadenosine
toluene-4-sulfonic acid
((3aR,4R,6R,6aR)-6-(6-amino-2-chloro-9H-purin-9-yl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methanol
Conditions | Yield |
---|---|
In acetone at 20℃; for 4h; Inert atmosphere; | 90% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide | 85% |
3,3,3-trifluoro-propane-1-thiol
2-Chloroadenosine
2-[(3,3,3-trifluoropropyl)thio]adenosine
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide for 5h; Reagent/catalyst; Solvent; Reflux; | 85% |
Conditions | Yield |
---|---|
With triethylamine In ethanol; water | 85% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide | 80% |
p-Aminophenethylamine
2-Chloroadenosine
2-[2-(4-aminophenyl)ethylamino]adenosine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine at 140℃; for 4h; Substitution; | 79% |
Conditions | Yield |
---|---|
With potassium tert-butylate; palladium diacetate; triphenylphosphine; potassium thioacetate In dimethyl sulfoxide at 120℃; Inert atmosphere; | 77% |
2-Chloroadenosine
Conditions | Yield |
---|---|
With N,N,N,N,N,N-hexamethylphosphoric triamide; thionyl chloride at 20℃; Inert atmosphere; | 76% |
Conditions | Yield |
---|---|
In ethanol; water at 100℃; for 132h; Sealed tube; | 75% |
1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane
2-Chloroadenosine
(6aR,8R,9R,9aS)-8-(6-amino-2-chloro-9H-purin-9-yl)-2,2,4,4-tetraisopropyltetrahydro-6H-furo[3,2-f][1,3,5,2,4]trioxadisilocin-9-ol
Conditions | Yield |
---|---|
With 1H-imidazole In tetrahydrofuran; DMF (N,N-dimethyl-formamide) at 20℃; for 24h; | 72% |
With pyridine for 1h; Ambient temperature; | 69% |
In pyridine at 20℃; |
2-Chloroadenosine
2-hydroxyethanethiol
S-(2-hydroxy-ethyl)-2-thio-isoguanosine
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide | 72% |
2-(aminoethyl)pyridine
2-Chloroadenosine
2-[2-(pyridin-2-yl)ethylamino]-adenosine
Conditions | Yield |
---|---|
at 140℃; for 4h; | 71% |
2-cyclohexylethylamine
2-Chloroadenosine
2-[(2-Cyclohexylethyl)amino]adenosine
Conditions | Yield |
---|---|
at 140℃; for 4h; | 71% |
isopropyldimethylsilyl chloride
2-Chloroadenosine
2-chloro-2',3',5'-tri-O-(isopropyldimethylsilyl)adenosine
Conditions | Yield |
---|---|
With 1H-imidazole In tetrahydrofuran; DMF (N,N-dimethyl-formamide) at 20℃; for 18h; | 70% |
4,4'-dimethoxytrityl chloride
2-Chloroadenosine
2-Chloro-5'-O-(4,4'-dimethoxytrityl)adenosine
Conditions | Yield |
---|---|
With pyridine for 24h; Ambient temperature; | 69% |
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