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Cas:15763-11-8
Min.Order:5 Kiloliter
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Type:Manufacturers
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Min.Order:1 Kilogram
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Min.Order:10 Milligram
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2-Chloroadenosine
2-hydrazinoadenosine
Conditions | Yield |
---|---|
With hydrazine hydrate at 20℃; for 4h; | 97% |
With hydrazine hydrate In water at 45 - 50℃; Temperature; | 87% |
With hydrazine at 40 - 55℃; for 2h; Product distribution / selectivity; | 81.4% |
2',3',5'-tri-O-acetyl-2-chloroadenosine
2-hydrazinoadenosine
Conditions | Yield |
---|---|
With hydrazine hydrate In methanol at 80 - 90℃; for 5h; Solvent; | 97% |
With hydrazine hydrate | 90% |
2-fluoroadenosine
2-hydrazinoadenosine
Conditions | Yield |
---|---|
With hydrazine hydrate In ethanol at 20℃; for 17h; Reflux; | 94% |
6-amino-2-chloro-9-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-9H-purine
2-hydrazinoadenosine
Conditions | Yield |
---|---|
With hydrazine hydrate In methanol at 80 - 90℃; for 5h; Solvent; | 94% |
2-iodoadenosine
2-hydrazinoadenosine
Conditions | Yield |
---|---|
With hydrazine hydrate In ethanol at 40 - 45℃; for 2h; | 88% |
With hydrazine hydrate In isopropyl alcohol at 80℃; | 82% |
With hydrazine hydrate In ethanol for 24h; Reflux; | |
With hydrazine hydrate In ethanol at 40 - 45℃; for 2h; | 66 g |
2-chloro-6-methoxy-purine riboside
2-hydrazinoadenosine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: methanol; NH3 2: N2H4 View Scheme |
G
2-hydrazinoadenosine
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: dmap; N,N-dimethyl-ethanamine / acetonitrile / 1 h / 20 °C 2: tetraethylammonium chloride; N,N-dimethyl-aniline; trichlorophosphate / 100 °C 3: benzyltriethylammonium nitrite; acetyl chloride / dichloromethane / 1 h / 0 °C / Inert atmosphere; Cooling with ice 4: ammonia / ethanol / 72 h / 20 °C 5: hydrazine hydrate / 10 h / 20 °C View Scheme | |
Multi-step reaction with 5 steps 1: N,N-dimethyl-ethanamine; dmap / acetonitrile 2: tetraethylammonium chloride; trichlorophosphate; N,N-dimethyl-aniline / Inert atmosphere 3: benzyltriethylammonium nitrite; acetyl chloride / dichloromethane / Inert atmosphere; Cooling with ice 4: ammonia; ethanol / 20 °C 5: hydrazine hydrate / 4 h / 20 °C View Scheme |
2',3',5'-tri-O-acetyl-guanosine
2-hydrazinoadenosine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: tetraethylammonium chloride; N,N-dimethyl-aniline; trichlorophosphate / 100 °C 2: benzyltriethylammonium nitrite; acetyl chloride / dichloromethane / 1 h / 0 °C / Inert atmosphere; Cooling with ice 3: ammonia / ethanol / 72 h / 20 °C 4: hydrazine hydrate / 10 h / 20 °C View Scheme | |
Multi-step reaction with 4 steps 1: tetraethylammonium chloride; trichlorophosphate; N,N-dimethyl-aniline / Inert atmosphere 2: benzyltriethylammonium nitrite; acetyl chloride / dichloromethane / Inert atmosphere; Cooling with ice 3: ammonia; ethanol / 20 °C 4: hydrazine hydrate / 4 h / 20 °C View Scheme |
2-amino-6-chloro-9-(2,3,5-tri-O-acetyl-β-D-ribofuranosyl)purine
2-hydrazinoadenosine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: benzyltriethylammonium nitrite; acetyl chloride / dichloromethane / 1 h / 0 °C / Inert atmosphere; Cooling with ice 2: ammonia / ethanol / 72 h / 20 °C 3: hydrazine hydrate / 10 h / 20 °C View Scheme | |
Multi-step reaction with 3 steps 1: benzyltriethylammonium nitrite; acetyl chloride / dichloromethane / Inert atmosphere; Cooling with ice 2: ammonia; ethanol / 20 °C 3: hydrazine hydrate / 4 h / 20 °C View Scheme |
(2R,3R,4R,5R)-4-(acetyloxy)-2-[(acetyloxy)methyl]-5-(2,6-dichloro-9H-purin-9-yl)tetrahydro-3-furanyl acetate
2-hydrazinoadenosine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: ammonia / ethanol / 72 h / 20 °C 2: hydrazine hydrate / 10 h / 20 °C View Scheme | |
Multi-step reaction with 3 steps 1: ammonia / methanol / 24 h / 100 °C / Autoclave 2: 24 h / 20 °C 3: hydrazine hydrate / water / 4 h / 50 °C View Scheme | |
Multi-step reaction with 2 steps 1: ammonia; ethanol / 20 °C 2: hydrazine hydrate / 4 h / 20 °C View Scheme |
2,6-dichloropurine riboside
2-hydrazinoadenosine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: ammonia / methanol / 7 h / 80 °C / High pressure 2: hydrazine hydrate / 10 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: 24 h / 20 °C 2: hydrazine hydrate / water / 4 h / 50 °C View Scheme |
1,2,3,5-tetraacetylribose
2-hydrazinoadenosine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: tin(IV) chloride / 0.25 h / 90 - 120 °C 2: ammonia / methanol / 24 h / 100 °C / Autoclave 3: 24 h / 20 °C 4: hydrazine hydrate / water / 4 h / 50 °C View Scheme |
2,6 dichloropurine
2-hydrazinoadenosine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: tin(IV) chloride / 0.25 h / 90 - 120 °C 2: ammonia / methanol / 24 h / 100 °C / Autoclave 3: 24 h / 20 °C 4: hydrazine hydrate / water / 4 h / 50 °C View Scheme |
Conditions | Yield |
---|---|
With polyethylene glycol-600 In water at 45 - 55℃; | 98.12% |
In water at 30 - 50℃; Temperature; | 95% |
With acetic acid In methanol at 80℃; for 3h; | 91% |
2-hydrazinoadenosine
2-(4-methoxycarbonylpyrazol-1-yl)adenosine
Conditions | Yield |
---|---|
Stage #1: 2-hydrazinoadenosine With acetic acid In methanol; water for 0.0833333h; Stage #2: sodium 2-(dimethoxymethyl)-3-methoxy-3-oxoprop-1-en-1-olate at 50 - 55℃; for 2.08333h; Reagent/catalyst; Concentration; Temperature; Solvent; | 95% |
Stage #1: 2-hydrazinoadenosine With acetic acid In methanol; water for 0.0833333h; Stage #2: sodium 2-(dimethoxymethyl)-3-methoxy-3-oxoprop-1-en-1-olate In methanol; water at 50 - 55℃; for 2h; Reagent/catalyst; Solvent; Temperature; Time; | 95% |
3-cyclohexylpropanal
2-hydrazinoadenosine
Conditions | Yield |
---|---|
In methanol | 92% |
2-hydrazinoadenosine
acetaldehyde
Conditions | Yield |
---|---|
In methanol | 92% |
Conditions | Yield |
---|---|
In methanol at 80℃; for 3h; | 92% |
Conditions | Yield |
---|---|
In methanol Heating; | 91% |
3,3-diethoxy-2-methoxycarbonylpropen-1-ol sodium salt
2-hydrazinoadenosine
2-(4-methoxycarbonylpyrazol-1-yl)adenosine
Conditions | Yield |
---|---|
Stage #1: 2-hydrazinoadenosine With acetic acid In water for 0.0833333h; Stage #2: 3,3-diethoxy-2-methoxycarbonylpropen-1-ol sodium salt In 1,2-dimethoxyethane; water at 55 - 60℃; for 3h; | 91% |
Conditions | Yield |
---|---|
In methanol Heating; | 89% |
2-hydrazinoadenosine
acetophenone
Conditions | Yield |
---|---|
In methanol Heating; | 89% |
2-hydrazinoadenosine
propionaldehyde
Conditions | Yield |
---|---|
In methanol | 88% |
2-chloro-3-carbaldehydepyridine
2-hydrazinoadenosine
Conditions | Yield |
---|---|
In methanol at 80℃; for 0.5h; | 86% |
pyridine-2-carbaldehyde
2-hydrazinoadenosine
Conditions | Yield |
---|---|
In methanol Heating; | 85% |
4-chlorobenzaldehyde
2-hydrazinoadenosine
Conditions | Yield |
---|---|
In methanol Heating; | 85% |
Conditions | Yield |
---|---|
With acetic acid In water for 1h; Ambient temperature; | 85% |
Conditions | Yield |
---|---|
In methanol for 1.33333h; Ambient temperature; | 85% |
3-thiophene carboxaldehyde
2-hydrazinoadenosine
Conditions | Yield |
---|---|
In methanol Heating; | 84% |
2-hydrazinoadenosine
(E)-t-butyl 4-formylcinnamate
Conditions | Yield |
---|---|
In methanol Heating; | 83% |
3-pyridinecarboxaldehyde
2-hydrazinoadenosine
Conditions | Yield |
---|---|
In methanol Heating; | 82% |
thiophene-2-carbaldehyde
2-hydrazinoadenosine
Conditions | Yield |
---|---|
In methanol Heating; | 81% |
2-Acetylthiophene
2-hydrazinoadenosine
Conditions | Yield |
---|---|
In methanol Heating; | 81% |
2-hydrazinoadenosine
1-(4-formylphenyl)-1H-imidazole
Conditions | Yield |
---|---|
In methanol at 80℃; for 0.5h; | 81% |
2-hydrazinoadenosine
m-tolyl aldehyde
Conditions | Yield |
---|---|
In methanol Heating; | 79% |
2-hydrazinoadenosine
adenosine
Conditions | Yield |
---|---|
With water; oxygen; copper(II) sulfate at 80℃; for 6h; Green chemistry; | 79% |
With potassium trimethylsilonate In water at 70℃; for 48h; Temperature; Green chemistry; | 89 %Spectr. |
2-chloro-benzaldehyde
2-hydrazinoadenosine
Conditions | Yield |
---|---|
In methanol Heating; | 78% |
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