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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

Lincomycin Manufacturer/High quality/Best price/In stock

Cas:154-21-2

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Sinoway Industrial Co., Ltd.

Why is SINOWAY: 1) Specialized in pharmaceutical and healthcare industrial for 34 years. 2) ISO 9001:2015 & SGS audited supplier . 3) Accept various payment terms : T.T 30-60 days. 4) We have warehouse in USA with quickly shipment . 5) We c

99% up GMP DMF Lincomycin A 154-21-2

Cas:154-21-2

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Wuhan Fortuna Chemical Co.,Ltd

Unique advantages Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White powder Storage:Cool dry place Package:1kg/foill bag;25kg/drum Application:as medic

Lincomycin Cas 154-21-2

Cas:154-21-2

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Xi'an Quanao Biotech Co., Ltd.

Xi’an Quanao Biotech Co., Ltd. with 18 years experience in plant extract filed. Product grade: Medicine, Health care product, Cosmetics, Food, Beverage, Feed. Hot selling market: Europe, North America, South America, Middle East, Asia Pacifi

China Supplier Lincomycin powder price CAS :154-21-2

Cas:154-21-2

Min.Order:1 Kilogram

FOB Price: $19.0 / 32.0

Type:Manufacturers

inquiry

Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

Factory Price API 99% Lincomycin 154-21-2 GMP Manufacturer

Cas:154-21-2

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

inquiry

COLORCOM LTD.

Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on

Lincomycin

Cas:154-21-2

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

CAS 154-21-2 Lincomycin hydrochloride

Cas:154-21-2

Min.Order:1 Kilogram

FOB Price: $3.0 / 10.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Factory direct supply CAS 154-21-2 with best quality

Cas:154-21-2

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Henan Sinotech Import&Export Corporation

Product Name: Lincomycin Synonyms: Lincolnensin Hydrochloride CAS: 154-21-2 MF: C18H34N2O6S MW: 406.54 Appearance:White powder Storage:Store in cool and dry place, away from sun ligh

Lincomycin CAS:154-21-2

Cas:154-21-2

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese

Lincomycin

Cas:154-21-2

Min.Order:1 Kilogram

FOB Price: $86.0 / 100.0

Type:Trading Company

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Afine Chemicals Limited

Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter

Lincomycin

Cas:154-21-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

Lincomycin

Cas:154-21-2

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Lincomycin

Cas:154-21-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Lingrui Chemical Co.,Ltd.

Our advantages: 1, High quality with competitive price: 1) Standard:BP/USP/EP/Enterprise standard 2) All Purity≥99% 3) We are manufacturer and can provide high quality products with factory price. 2, Fast and safe delivery 1) Parcel can be

Manufacturer/High quality Lincomycin 154-21-2

Cas:154-21-2

Min.Order:1 Gram

Negotiable

Type:Other

inquiry

DB BIOTECH CO., LTD

Q1: Are you a manufacturer?Answer: Yes, we are factory founded on 2002. Q2: How to contact with us?Click "contact supplier" And then send us message the product you interest in, you will get reply within 12 hours. Q3:Which kind of payment terms do yo

High quality lincomycin powder with factory price

Cas:154-21-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

TaiChem Taizhou Limited

Established in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site

Lincomycin

Cas:154-21-2

Min.Order:10 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

High purity Lincomycin

Cas:154-21-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

Lincomycin

Cas:154-21-2

Min.Order:1 Milligram

Negotiable

Type:Trading Company

inquiry

Hangzhou Think Chemical Co. Ltd

HANGZHOU THINK CHEMICAL CO., LTD. (THINKCHEM) is an integrative corporation of trade, research and contract manufacture. With about ten years of business experiences on the marketing & distribution, thinkchem specializes in exp

Good quality Lincomycin HCl

Cas:154-21-2

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

Hangzhou Huarong Pharm Co., Ltd.

Hangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu

Lincomycin Hcl

Cas:154-21-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hangzhou Zhongqi chem Co.,Ltd.

Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and h

Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

Lincomycin

Cas:154-21-2

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

SAGECHEM LIMITED

SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe

SAGECHEM/Lincomycin

Cas:154-21-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Senova Technology Company Limited

LINCOMYCIN is very strong of Senova Tech and we have GMP workshop with storng production capacity to meet customers demand worldwide. Specification is as below, Appearance: white to almost white crystalline powder PH: 3-5 Water b

Lincomycin

Cas:154-21-2

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

lincomycin

Cas:154-21-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

Lincomycin

Cas:154-21-2

Min.Order:0

Negotiable

Type:Other

inquiry

Wuxi TAA Chemical Industry Co.,LTD.

1.A strong technical force and advanced processing equipments. The quality of the products has been strictly inspected and all kinds of index have reached or exceeded domestic and international standards.2. Now we have established long-term stable re

Lincomycin; CAS 154-21-2

Cas:154-21-2

Min.Order:0

Negotiable

Type:Other

inquiry

GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier

Lincomycin

Cas:154-21-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

C34H61N3O9SSi3

C34H61N3O9SSi3

lincomycin
154-21-2

lincomycin

Conditions
ConditionsYield
With potassium carbonate In methanol at 130℃; for 20h;98.4%
C26H46N5O8S(1+)

C26H46N5O8S(1+)

lincomycin
154-21-2

lincomycin

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: Microbiological reaction
2: Microbiological reaction
3: aq. buffer / 30 °C / Microbiological reaction
View Scheme
C34H60N4O18S

C34H60N4O18S

lincomycin
154-21-2

lincomycin

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Microbiological reaction
2: aq. buffer / 30 °C / Microbiological reaction
View Scheme
C22H39N3O9S

C22H39N3O9S

lincomycin
154-21-2

lincomycin

Conditions
ConditionsYield
In aq. buffer at 30℃; Microbiological reaction;
C20H37N3O8S

C20H37N3O8S

lincomycin
154-21-2

lincomycin

Conditions
ConditionsYield
With pyridoxal 5'-phosphate; LmbF enzyme; S-methyltransferase LmbG; S-adenosyl-L-methionine In aq. phosphate buffer at 30℃; for 2h; pH=7.5; Enzymatic reaction;
lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

lincomycin
154-21-2

lincomycin

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: pyridine / 8 h / 2 - 20 °C
2: acetic acid / methanol / 18 h / 30 °C
3: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 20 h / 30 °C
4: potassium carbonate / methanol / 20 h / 130 °C
View Scheme
C30H66N2O6SSi4

C30H66N2O6SSi4

lincomycin
154-21-2

lincomycin

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: acetic acid / methanol / 18 h / 30 °C
2: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 20 h / 30 °C
3: potassium carbonate / methanol / 20 h / 130 °C
View Scheme
2,3,4-tris-O-(trimethylsilyl)lincomycin
25420-97-7

2,3,4-tris-O-(trimethylsilyl)lincomycin

lincomycin
154-21-2

lincomycin

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 20 h / 30 °C
2: potassium carbonate / methanol / 20 h / 130 °C
View Scheme
acetic anhydride
108-24-7

acetic anhydride

lincomycin
154-21-2

lincomycin

(2R,3S,4S,5R,6R)-2-((1R,2R)-2-acetoxy-1-((2S,4R)-1-methyl-4-propylpyrrolidine-2-carboxamido)propyl)-6-(methylthio)tetrahydro-2H-pyran-3,4,5-triyl triacetate
168399-17-5

(2R,3S,4S,5R,6R)-2-((1R,2R)-2-acetoxy-1-((2S,4R)-1-methyl-4-propylpyrrolidine-2-carboxamido)propyl)-6-(methylthio)tetrahydro-2H-pyran-3,4,5-triyl triacetate

Conditions
ConditionsYield
With pyridine at 20℃; for 38h; Acetylation;98.8%
chloro-trimethyl-silane
75-77-4

chloro-trimethyl-silane

lincomycin
154-21-2

lincomycin

C30H66N2O6SSi4

C30H66N2O6SSi4

Conditions
ConditionsYield
With pyridine; 1,1,1,3,3,3-hexamethyl-disilazane at 0 - 20℃; for 2h;91%
chloro-trimethyl-silane
75-77-4

chloro-trimethyl-silane

lincomycin
154-21-2

lincomycin

2,3,4-tris-O-(trimethylsilyl)lincomycin
25420-97-7

2,3,4-tris-O-(trimethylsilyl)lincomycin

Conditions
ConditionsYield
Stage #1: chloro-trimethyl-silane; lincomycin With pyridine; 1,1,1,3,3,3-hexamethyl-disilazane at 20℃; for 2h; Ice cooling;
Stage #2: With water; acetic acid In methanol at 20℃; for 16h;
Stage #3: With sodium hydrogencarbonate In methanol; water
91%
Stage #1: chloro-trimethyl-silane; lincomycin With pyridine; 1,1,1,3,3,3-hexamethyl-disilazane at 20℃; for 2h;
Stage #2: With acetic acid In methanol at 20℃; for 16h;
91%
With pyridine; 1,1,1,3,3,3-hexamethyl-disilazane
chloro-trimethyl-silane
75-77-4

chloro-trimethyl-silane

1,1,1,3,3,3-hexamethyl-disilazane
999-97-3

1,1,1,3,3,3-hexamethyl-disilazane

lincomycin
154-21-2

lincomycin

2,3,4-tris-O-(trimethylsilyl)lincomycin
25420-97-7

2,3,4-tris-O-(trimethylsilyl)lincomycin

Conditions
ConditionsYield
Stage #1: chloro-trimethyl-silane; 1,1,1,3,3,3-hexamethyl-disilazane; lincomycin With pyridine at 20℃; Cooling with ice;
Stage #2: With acetic acid In methanol; water at 20℃; for 16h;
Stage #3: With sodium hydrogencarbonate In methanol; water
91%
lincomycin
154-21-2

lincomycin

A

lincomycin (S)-sulfoxide

lincomycin (S)-sulfoxide

B

lincomycin (R)-sulfoxide

lincomycin (R)-sulfoxide

Conditions
ConditionsYield
With 3,3-dimethyldioxirane In methanol at 20℃; for 84h; Oxidation;A 15%
B 28%
lincomycin
154-21-2

lincomycin

A

propyl-L-hygric acid
13380-36-4

propyl-L-hygric acid

B

α-methylthiolincosaminide
14810-93-6

α-methylthiolincosaminide

Conditions
ConditionsYield
With sodium hydroxide at 95 - 110℃; for 22h; Product distribution; other compounds, other products;
lincomycin
154-21-2

lincomycin

lincomycin-sulfone

lincomycin-sulfone

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 98.8 percent / pyridine / 38 h / 20 °C
2: 46.8 percent / N-methylmorpholine N-oxide / osmium tetroxide / tetrahydrofuran; 2-methyl-propan-2-ol / 68 h / 20 °C
3: 99 percent / sodium methoxide / methanol / pH 7 - 8
View Scheme
Multi-step reaction with 2 steps
1: 15 percent / dimethyldioxirane / methanol / 84 h / 20 °C
2: 64.7 percent / N-methylmorpholine N-oxide / osmium tetroxide / tetrahydrofuran; 2-methyl-propan-2-ol / 6.5 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: 28 percent / dimethyldioxirane / methanol / 84 h / 20 °C
2: 78.3 percent / N-methylmorpholine N-oxide / osmium tetroxide / tetrahydrofuran; 2-methyl-propan-2-ol / 6.5 h / 20 °C
View Scheme
lincomycin
154-21-2

lincomycin

Acetic acid (2R,3S,4S,5R,6R)-4,5-diacetoxy-2-{(1R,2R)-2-acetoxy-1-[((2S,4R)-1-methyl-4-propyl-pyrrolidine-2-carbonyl)-amino]-propyl}-6-methanesulfonyl-tetrahydro-pyran-3-yl ester

Acetic acid (2R,3S,4S,5R,6R)-4,5-diacetoxy-2-{(1R,2R)-2-acetoxy-1-[((2S,4R)-1-methyl-4-propyl-pyrrolidine-2-carbonyl)-amino]-propyl}-6-methanesulfonyl-tetrahydro-pyran-3-yl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 98.8 percent / pyridine / 38 h / 20 °C
2: 46.8 percent / N-methylmorpholine N-oxide / osmium tetroxide / tetrahydrofuran; 2-methyl-propan-2-ol / 68 h / 20 °C
View Scheme
lincomycin
154-21-2

lincomycin

A

Methyl 6-Amino-6,8-dideoxy-1-thio-D-erythro-α-D-galacto-octopyranoside
14810-93-6

Methyl 6-Amino-6,8-dideoxy-1-thio-D-erythro-α-D-galacto-octopyranoside

B

(2S,4R)-1-Methyl-4-propyl-pyrrolidine-2-carboxylic acid hydrazide
13380-37-5

(2S,4R)-1-Methyl-4-propyl-pyrrolidine-2-carboxylic acid hydrazide

Conditions
ConditionsYield
With hydrazine hydrate Reflux;
lincomycin
154-21-2

lincomycin

7(S)-7-deoxyl-7-(thiophen-2-ylthio)lincomycin

7(S)-7-deoxyl-7-(thiophen-2-ylthio)lincomycin

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: pyridine; 1,1,1,3,3,3-hexamethyl-disilazane / 2 h / 20 °C
1.2: 16 h / 20 °C
2.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran
2.2: 0.5 h / 20 °C
View Scheme
lincomycin
154-21-2

lincomycin

7(S)-7-deoxy-7-(thiazol-2-ylthio)lincomycin

7(S)-7-deoxy-7-(thiazol-2-ylthio)lincomycin

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: pyridine; 1,1,1,3,3,3-hexamethyl-disilazane / 2 h / 20 °C
1.2: 16 h / 20 °C
2.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran
2.2: 0.5 h / 20 °C
View Scheme
lincomycin
154-21-2

lincomycin

7(S)-7-deoxy-7-(1,3,4-thiadiazol-2-ylthio)lincomycin
1429341-38-7

7(S)-7-deoxy-7-(1,3,4-thiadiazol-2-ylthio)lincomycin

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: pyridine; 1,1,1,3,3,3-hexamethyl-disilazane / 2 h / 20 °C
1.2: 16 h / 20 °C
2.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran
2.2: 0.5 h / 20 °C
View Scheme
lincomycin
154-21-2

lincomycin

7(S)-7-(5-chlorobenzo[d]thiazol-2-ylthio)-7-deoxylincomycin
941590-01-8

7(S)-7-(5-chlorobenzo[d]thiazol-2-ylthio)-7-deoxylincomycin

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: pyridine; 1,1,1,3,3,3-hexamethyl-disilazane / 2 h / 20 °C
1.2: 16 h / 20 °C
2.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran
2.2: 0.5 h / 20 °C
View Scheme
lincomycin
154-21-2

lincomycin

7(S)-7-deoxyl-7-(thiazolo[5,4-c]pyridin-2-ylthio)lincomycin

7(S)-7-deoxyl-7-(thiazolo[5,4-c]pyridin-2-ylthio)lincomycin

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: pyridine; 1,1,1,3,3,3-hexamethyl-disilazane / 2 h / 20 °C
1.2: 16 h / 20 °C
2.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran
2.2: 0.5 h / 20 °C
View Scheme
lincomycin
154-21-2

lincomycin

7(S)-7-(6-cyanobenzo[d]thiazol-2-ylthio)-7-deoxylincomycin
941590-04-1

7(S)-7-(6-cyanobenzo[d]thiazol-2-ylthio)-7-deoxylincomycin

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: pyridine; 1,1,1,3,3,3-hexamethyl-disilazane / 2 h / 20 °C
1.2: 16 h / 20 °C
2.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran
2.2: 0.5 h / 20 °C
View Scheme
lincomycin
154-21-2

lincomycin

7(S)-7-deoxy-7-(6-nitrobenzo[d]thiazol-2-ylthio)lincomycin
941590-07-4

7(S)-7-deoxy-7-(6-nitrobenzo[d]thiazol-2-ylthio)lincomycin

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: pyridine; 1,1,1,3,3,3-hexamethyl-disilazane / 2 h / 20 °C
1.2: 16 h / 20 °C
2.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran
2.2: 0.5 h / 20 °C
View Scheme
lincomycin
154-21-2

lincomycin

7(S)-7-(6-aminobenzo[d]thiazol-2-ylthio)-7-deoxylincomycin
941585-06-4

7(S)-7-(6-aminobenzo[d]thiazol-2-ylthio)-7-deoxylincomycin

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: pyridine; 1,1,1,3,3,3-hexamethyl-disilazane / 2 h / 20 °C
1.2: 16 h / 20 °C
2.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran
2.2: 0.5 h / 20 °C
View Scheme
Multi-step reaction with 3 steps
1: pyridine; 1,1,1,3,3,3-hexamethyl-disilazane / 2 h / 0 - 20 °C
2: methanol; water; acetic acid / 16 h / 20 °C
3: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 16 h / 0 - 20 °C
View Scheme
lincomycin
154-21-2

lincomycin

7(S)-7-deoxy-7-(5-nitrobenzo[d]thiazol-2-ylthio)lincomycin
941590-03-0

7(S)-7-deoxy-7-(5-nitrobenzo[d]thiazol-2-ylthio)lincomycin

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: pyridine; 1,1,1,3,3,3-hexamethyl-disilazane / 2 h / 20 °C
1.2: 16 h / 20 °C
2.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran
2.2: 0.5 h / 20 °C
View Scheme
lincomycin
154-21-2

lincomycin

7(S)-7-deoxy-7-(2-nitrophenylthio)lincomycin
941588-55-2

7(S)-7-deoxy-7-(2-nitrophenylthio)lincomycin

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: pyridine; 1,1,1,3,3,3-hexamethyl-disilazane / 2 h / 20 °C
1.2: 16 h / 20 °C
2.1: diethylazodicarboxylate; tributylphosphine / tetrahydrofuran / 0 - 20 °C
2.2: 20 °C
View Scheme
lincomycin
154-21-2

lincomycin

7(S)-7-deoxy-7-(3-nitrophenylthio)lincomycin
941587-70-8

7(S)-7-deoxy-7-(3-nitrophenylthio)lincomycin

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: pyridine; 1,1,1,3,3,3-hexamethyl-disilazane / 2 h / 20 °C
1.2: 16 h / 20 °C
2.1: diethylazodicarboxylate; tributylphosphine / tetrahydrofuran / 0 - 20 °C
2.2: 20 °C
View Scheme
lincomycin
154-21-2

lincomycin

7(S)-7-deoxy-7-(4-nitrophenylthio)lincomycin
941587-69-5

7(S)-7-deoxy-7-(4-nitrophenylthio)lincomycin

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: pyridine; 1,1,1,3,3,3-hexamethyl-disilazane / 2 h / 20 °C
1.2: 16 h / 20 °C
2.1: diethylazodicarboxylate; tributylphosphine / tetrahydrofuran / 0 - 20 °C
2.2: 20 °C
View Scheme
lincomycin
154-21-2

lincomycin

7(S)-7-(5-amino-1,3,4-thiadiazol-2-ylthio)-7-deoxylincomycin
941586-01-2

7(S)-7-(5-amino-1,3,4-thiadiazol-2-ylthio)-7-deoxylincomycin

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: pyridine; 1,1,1,3,3,3-hexamethyl-disilazane / 2 h / 20 °C
1.2: 16 h / 20 °C
2.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 17 h / 0 - 20 °C
3.1: trifluoroacetic acid / water / 1 h / 20 °C
View Scheme
lincomycin
154-21-2

lincomycin

7(S)-7-deoxy-7-(5-methylamino-1,3,4-thiadiazol-2-ylthio)lincomycin
941586-02-3

7(S)-7-deoxy-7-(5-methylamino-1,3,4-thiadiazol-2-ylthio)lincomycin

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: pyridine; 1,1,1,3,3,3-hexamethyl-disilazane / 2 h / 20 °C
1.2: 16 h / 20 °C
2.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 0 - 20 °C
3.1: trifluoroacetic acid / water / 20 °C
View Scheme
lincomycin
154-21-2

lincomycin

7(S)-7-deoxy-7-(5-(4-(difluoromethylthio)phenylamino)-1,3,4-thiadiazol-2-ylthio)lincomycin
941586-41-0

7(S)-7-deoxy-7-(5-(4-(difluoromethylthio)phenylamino)-1,3,4-thiadiazol-2-ylthio)lincomycin

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: pyridine; 1,1,1,3,3,3-hexamethyl-disilazane / 2 h / 20 °C
1.2: 16 h / 20 °C
2.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran
2.2: 0.5 h / 20 °C
View Scheme

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