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Luyunjia Chemistry Xiamen Limited

Quick Details CAS No.: 859-18-7 Other Names: Lincocin Hydrochloride MF: C18H35ClN2O6S EINECS No.: 212-726-7 Place of Origin: Jiangsu, China (Mainland) Type: Antibiotic and Antimicrobial Agents Grade Standard: Medicine Grade Brand Name:

lower price Lincomycin hydrochloride 859-18-7

Cas:859-18-7

Min.Order:1 Kilogram

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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

Lincomycin hydrochloride Manufacturer/High quality/Best price/In stock

Cas:859-18-7

Min.Order:1 Kilogram

FOB Price: $3.0

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Hangzhou Dingyan Chem Co., Ltd

Items Standard Result Characters A white or almost white, crystalliine powder Dissolves in water and methanol,slightly Soluble in ethanol..

High purity Various Specifications Lincocin Hydrochloride CAS:859-18-7

Cas:859-18-7

Min.Order:1 Gram

FOB Price: $100.0 / 500.0

Type:Manufacturers

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality Lincomycin Hydrochloride Bp/Ep supplier in China

Cas:859-18-7

Min.Order:1 Metric Ton

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Wuhan Fortuna Chemical Co.,Ltd

Unique advantages for Lincomycin hydrochloride Cas859-18-7 Guaranteed the purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White or almost white,crystalline powder Storage:Store in 2-8℃

Hot sale Lincomycin hydrochloride Cas859-18-7 with high quality and factory price

Cas:859-18-7

Min.Order:1 Kilogram

FOB Price: $68.0 / 70.0

Type:Trading Company

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Hangzhou JINLAN Pharm-Drugs Technology Co., Ltd

We can provide GMP validation service that complies with SFDA, FDA, WHO and EU EMPA.Excellent registration team could help us easlily to register our products in different countries.If you and your customer are interested in some products or need C

Lincomycin hydrochloride manufacturer with low price

Cas:859-18-7

Min.Order:1 Gram

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Type:Manufacturers

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Hangzhou Think Chemical Co. Ltd

HANGZHOU THINK CHEMICAL CO., LTD. (THINKCHEM) is an integrative corporation of trade, research and contract manufacture. With about ten years of business experiences on the marketing & distribution, thinkchem specializes in exp

Lincomycin hydrochloride CAS:859-18-7 factory manufacture

Cas:859-18-7

Min.Order:1 Kilogram

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Type:Other

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

Large Stock 99.0% Lincocin Hydrochloride 859-18-7 Producer

Cas:859-18-7

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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Xi`an Eastling Biotech Co., Ltd.

Lincocin Hydrochloride CAS: 859-18-7 Molecular Formula: C18H35ClN2O6S Home Product Category Inorganic chemical engineering inorganic salt 859-18-7 859-18-7 - Names and Identifiers Name Lincocin Hydrochloride Synonyms

Factory high quality Lincomycin HCl

Cas:859-18-7

Min.Order:1 Gram

FOB Price: $159.0 / 170.0

Type:Lab/Research institutions

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Shandong Jiulong Hisince Pharmaceutical Co.,Ltd.

Lincomycin Hydrochloride 1.Full experience of large numbers containers loading in Chinese sea port 2.Fast shipment by reputed shipping line 3.Pac

lincomycin hydrochloride

Cas:859-18-7

Min.Order:25 Kilogram

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Type:Manufacturers

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COLORCOM LTD.

Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on

Lincomycin Hydrochloride

Cas:859-18-7

Min.Order:1 Metric Ton

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Type:Manufacturers

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Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

Lincomycin hydrochloride

Cas:859-18-7

Min.Order:1 Kilogram

FOB Price: $3.0 / 10.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Pharmaceutical Grade CAS 859-18-7 with competitive price

Cas:859-18-7

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Lincomycin Hydrochloride 99%

Cas:859-18-7

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

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LIDE PHARMACEUTICALS LIMITED

Advantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&amp

Lincomycin hydrochloride/ LIDE PHARMA- Factory supply / Best price

Cas:859-18-7

Min.Order:0

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Antimex Chemical Limied

Lincomycin Hydrochloride 859-18-7 98%MIN supplier Name Lincomycin hydrochloride EINECS212-726-7 CAS No.859-18-7 Density==PSA147.79000 LogP0.27380 SolubilitySoluble in water. Melting Point156-158 °C FormulaC18H34N2O6S.HCl Boiling Point6

Lincomycin Hydrochloride 859-18-7 98%MIN supplier

Cas:859-18-7

Min.Order:1 Gram

FOB Price: $15.0

Type:Lab/Research institutions

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Henan Sinotech Import&Export Corporation

Name: Lincocin Hydrochloride Synonyms: Lincomycin Hcl CAS: 859-18-7 MF: C18H35ClN2O6S Appearance:White powder Storage:Store in cool and dry place, away from sun light. Package:25kg/drum Application:APIs Transportation:By sea or by air Port:Qingd

Lincocin Hydrochloride

Cas:859-18-7

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

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Hefei TNJ chemical industry co.,ltd

1. We are one of the domestic largest manufacturers of API; 2. We are always supplier of products with higher quality and at more competitive price; 3. We are supplier of safe and ecofriendly products ; 4. We provide stable supply

Lincomycin hydrochloride, CAS 859-18-7

Cas:859-18-7

Min.Order:25 Kilogram

Negotiable

Type:Trading Company

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Hubei Langyou International Trading Co., Ltd

Advantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best s

99% Ketotifen Fumarate CAS 859-18-7 With Factory Price

Cas:859-18-7

Min.Order:10 Gram

Negotiable

Type:Other

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HANWAYS CHEMPHARM CO.,LIMITED

Hanways chempharm is a specialized company concentrating on the R&D, production, marketing and technical service of APIs and pharmaceutical intermediates. The marketing department is located in Wuhan. We have two GMP facilities in Hubei Pr

Antibiotic Raw Powder Lincomycin Hydrochloride Lincomycin HCl CAS 859-18-7

Cas:859-18-7

Min.Order:1 Kilogram

FOB Price: $200.0 / 400.0

Type:Trading Company

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Shanghai Upbio Tech Co.,Ltd

1,In No Less five years exporting experience. 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Onchem specialized in APIs, chemical inte

high quality Lincomycin Hydrochloride 99%

Cas:859-18-7

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Lab/Research institutions

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Xi'an Faithful Biotech Co., Ltd.

We are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery

Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present

Veterinary medicine raw material 99% Lincomycin Hcl powder 859-18-7

Cas:859-18-7

Min.Order:1 Kilogram

FOB Price: $75.0 / 80.0

Type:Trading Company

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Qingdao Beluga Import and Export Co., LTD

Lincomycin hydrochloride CAS:859-18-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic in

Lincomycin hydrochloride CAS:859-18-7

Cas:859-18-7

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shanghai Terui OP New Material Technology Co., Ltd.

We have overseas warehouses in California, New Laredo Mexico, Vancouver Canada, Amsterdam Netherlands, and Melbourne Australia. Overseas warehouses can provide some of the best-selling products. We look forward to the cooperation of local powerful

Chinese suppliers CAS 859-18-7 Lincomycin hydrochloride

Cas:859-18-7

Min.Order:0 Metric Ton

Negotiable

Type:Trading Company

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Lincomycin hydrochloride

Cas:859-18-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Leader Biochemical Group

About Product Details

China Biggest Factory Manufacturer Supply Lincomycin hydrochloride CAS 859-18-7

Cas:859-18-7

Min.Order:500 Kilogram

FOB Price: $1.0 / 2.0

Type:Lab/Research institutions

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Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s

LINCOMYCIN HYDROCHLORIDE

Cas:859-18-7

Min.Order:1 Kilogram

FOB Price: $400.0 / 500.0

Type:Lab/Research institutions

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Lonwin Chemical Group Limited

Lincomycin CAS: 859-18-7 Specification Item Standard Identification A.H-NMR:Comply with the structure B.LC-MS:Comply with the structure C.The IR spectrum of sampl

Factory supply Lincomycin

Cas:859-18-7

Min.Order:1 Kilogram

FOB Price: $100.0 / 150.0

Type:Other

inquiry

Synthetic route

lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

(1S,2S,4R)-1-Methyl-1-oxy-4-propyl-pyrrolidine-2-carboxylic acid [(1R,2R)-2-hydroxy-1-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-methanesulfonyl-tetrahydro-pyran-2-yl)-propyl]-amide

(1S,2S,4R)-1-Methyl-1-oxy-4-propyl-pyrrolidine-2-carboxylic acid [(1R,2R)-2-hydroxy-1-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-methanesulfonyl-tetrahydro-pyran-2-yl)-propyl]-amide

Conditions
ConditionsYield
With ammonium hydroxide; dihydrogen peroxide; acetonitrile In water at 20℃; for 0.333333h; pH=10.8;95%
chloro-trimethyl-silane
75-77-4

chloro-trimethyl-silane

lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

1,1,1,3,3,3-hexamethyl-disilazane
999-97-3

1,1,1,3,3,3-hexamethyl-disilazane

C30H66N2O6SSi4

C30H66N2O6SSi4

Conditions
ConditionsYield
With pyridine at 2 - 20℃; for 8h;89%
lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

clindamycin hydrochloride monohydrate

clindamycin hydrochloride monohydrate

Conditions
ConditionsYield
In water86%
lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

A

(1S,2S,4R)-1-Methyl-1-oxy-4-propyl-pyrrolidine-2-carboxylic acid [(1R,2R)-2-hydroxy-1-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-methanesulfinyl-tetrahydro-pyran-2-yl)-propyl]-amide

(1S,2S,4R)-1-Methyl-1-oxy-4-propyl-pyrrolidine-2-carboxylic acid [(1R,2R)-2-hydroxy-1-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-methanesulfinyl-tetrahydro-pyran-2-yl)-propyl]-amide

B

(1S,2S,4R)-1-Methyl-1-oxy-4-propyl-pyrrolidine-2-carboxylic acid [(1R,2R)-2-hydroxy-1-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-methanesulfonyl-tetrahydro-pyran-2-yl)-propyl]-amide

(1S,2S,4R)-1-Methyl-1-oxy-4-propyl-pyrrolidine-2-carboxylic acid [(1R,2R)-2-hydroxy-1-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-methanesulfonyl-tetrahydro-pyran-2-yl)-propyl]-amide

Conditions
ConditionsYield
With ammonium hydroxide; dihydrogen peroxide In water at 20℃; for 12h; pH=10.8;A 66%
B 30%
lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

Methyl 6-Amino-6,8-dideoxy-1-thio-D-erythro-α-D-galacto-octopyranoside
14810-93-6

Methyl 6-Amino-6,8-dideoxy-1-thio-D-erythro-α-D-galacto-octopyranoside

Conditions
ConditionsYield
With hydrazine hydrate at 120℃; for 24h;59%
lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

A

(1R,2S,4R)-1-Methyl-1-oxy-4-propyl-pyrrolidine-2-carboxylic acid [(1R,2R)-2-hydroxy-1-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-methanesulfonyl-tetrahydro-pyran-2-yl)-propyl]-amide

(1R,2S,4R)-1-Methyl-1-oxy-4-propyl-pyrrolidine-2-carboxylic acid [(1R,2R)-2-hydroxy-1-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-methanesulfonyl-tetrahydro-pyran-2-yl)-propyl]-amide

B

(1S,2S,4R)-1-Methyl-1-oxy-4-propyl-pyrrolidine-2-carboxylic acid [(1R,2R)-2-hydroxy-1-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-methanesulfonyl-tetrahydro-pyran-2-yl)-propyl]-amide

(1S,2S,4R)-1-Methyl-1-oxy-4-propyl-pyrrolidine-2-carboxylic acid [(1R,2R)-2-hydroxy-1-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-methanesulfonyl-tetrahydro-pyran-2-yl)-propyl]-amide

Conditions
ConditionsYield
With sodium hydroxide; dihydrogen peroxide In water at 20℃; for 12h; pH=9.75;A 47%
B 50%
D-Mannose
530-26-7

D-Mannose

lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

(2S,4R)-1-Methyl-4-propyl-pyrrolidine-2-carboxylic acid [(1R,2R)-2-((2S,3S,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-1-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-methylsulfanyl-tetrahydro-pyran-2-yl)-propyl]-amide

(2S,4R)-1-Methyl-4-propyl-pyrrolidine-2-carboxylic acid [(1R,2R)-2-((2S,3S,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-1-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-methylsulfanyl-tetrahydro-pyran-2-yl)-propyl]-amide

Conditions
ConditionsYield
With α-mannosidase In various solvent(s) at 48℃; pH=5.0; Enzymatic reaction;2.4%
lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

C26H50N2O6S

C26H50N2O6S

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: hydrazine hydrate / 24 h / 120 °C
2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 20 °C
3: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
View Scheme
lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

C31H58N2O8S

C31H58N2O8S

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: hydrazine hydrate / 24 h / 120 °C
2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 20 °C
View Scheme
lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

C9H18ClNO4S

C9H18ClNO4S

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: hydrazine hydrate / 24 h / 120 °C
2: triphenylphosphine; tetrachloromethane / acetonitrile / 3 h / Reflux
View Scheme
lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

C26H39ClN2O5S

C26H39ClN2O5S

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: hydrazine hydrate / 24 h / 120 °C
2.1: triphenylphosphine; tetrachloromethane / acetonitrile / 3 h / Reflux
3.1: triethylamine; isobutyl chloroformate / acetonitrile / 1 h / 10 °C
3.2: 18 h / 20 °C
View Scheme
lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

C21H31ClN2O5S

C21H31ClN2O5S

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: hydrazine hydrate / 24 h / 120 °C
2: triphenylphosphine; tetrachloromethane / acetonitrile / 3 h / Reflux
3: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 3.5 h / 20 °C
4: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
View Scheme
lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

C26H39ClN2O7S

C26H39ClN2O7S

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: hydrazine hydrate / 24 h / 120 °C
2: triphenylphosphine; tetrachloromethane / acetonitrile / 3 h / Reflux
3: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 3.5 h / 20 °C
View Scheme
lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

C20H30ClN3O5S

C20H30ClN3O5S

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: hydrazine hydrate / 24 h / 120 °C
2: triphenylphosphine; tetrachloromethane / acetonitrile / 3 h / Reflux
3: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 20 °C
4: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
View Scheme
lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

C25H38ClN3O7S

C25H38ClN3O7S

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: hydrazine hydrate / 24 h / 120 °C
2: triphenylphosphine; tetrachloromethane / acetonitrile / 3 h / Reflux
3: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 20 °C
View Scheme
lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

C23H36N2O6S

C23H36N2O6S

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: hydrazine hydrate / 24 h / 120 °C
2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 20 °C
3: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
View Scheme
lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

C28H44N2O8S

C28H44N2O8S

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: hydrazine hydrate / 24 h / 120 °C
2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 20 °C
View Scheme
lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

C23H42N2O6S

C23H42N2O6S

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: hydrazine hydrate / 24 h / 120 °C
2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 20 °C
3: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
View Scheme
lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

C28H50N2O8S

C28H50N2O8S

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: hydrazine hydrate / 24 h / 120 °C
2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 20 °C
View Scheme
lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

clindamycin phosphate
24729-96-2

clindamycin phosphate

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: phosgene / chloroform; N,N-dimethyl-formamide / 2 h / 5 - 71 °C / Large scale
1.2: 10 °C / Alkaline conditions; Large scale
2.1: toluene-4-sulfonic acid / acetone / 6 h / 35 °C / Large scale
3.1: triethylamine; trichlorophosphate; 1H-imidazole / acetone / 4 h / 22 °C / Large scale
3.2: 30 °C / Large scale
View Scheme
lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

Conditions
ConditionsYield
Stage #1: lincomycin hydrochloride With phosgene In chloroform; N,N-dimethyl-formamide at 5 - 71℃; for 2h; Large scale;
Stage #2: at 10℃; Temperature; Reagent/catalyst; Alkaline conditions; Large scale;
With bis(trichloromethyl) carbonate; ester of 3,5-di-tert-butyl-4-hydroxyphenylpropionic acid and pentaerythritol In chloroform; 1,2-dichloro-ethane; N,N-dimethyl-formamide at 12 - 62℃; for 13h; Temperature; Large scale;
lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

C21H37ClN2O5S

C21H37ClN2O5S

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: phosgene / chloroform; N,N-dimethyl-formamide / 2 h / 5 - 71 °C / Large scale
1.2: 10 °C / Alkaline conditions; Large scale
2.1: toluene-4-sulfonic acid / acetone / 6 h / 35 °C / Large scale
View Scheme
lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

7-epiclindamycin hydrochloride

7-epiclindamycin hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1: pyridine / 8 h / 2 - 20 °C
2: acetic acid / methanol / 18 h / 30 °C
3: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 20 h / 30 °C
4: potassium carbonate / methanol / 20 h / 130 °C
5: hydrogenchloride
6: bis(trichloromethyl) carbonate / N,N-dimethyl-formamide; chloroform / 23 h / 5 - 60 °C
View Scheme
lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

C18H34N2O6S*ClH

C18H34N2O6S*ClH

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: pyridine / 8 h / 2 - 20 °C
2: acetic acid / methanol / 18 h / 30 °C
3: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 20 h / 30 °C
4: potassium carbonate / methanol / 20 h / 130 °C
5: hydrogenchloride
View Scheme
lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

2,3,4-tris-O-(trimethylsilyl)lincomycin
25420-97-7

2,3,4-tris-O-(trimethylsilyl)lincomycin

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: pyridine / 8 h / 2 - 20 °C
2: acetic acid / methanol / 18 h / 30 °C
View Scheme
lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

C34H61N3O9SSi3

C34H61N3O9SSi3

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: pyridine / 8 h / 2 - 20 °C
2: acetic acid / methanol / 18 h / 30 °C
3: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 20 h / 30 °C
View Scheme
lincomycin hydrochloride
859-18-7

lincomycin hydrochloride

lincomycin
154-21-2

lincomycin

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: pyridine / 8 h / 2 - 20 °C
2: acetic acid / methanol / 18 h / 30 °C
3: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 20 h / 30 °C
4: potassium carbonate / methanol / 20 h / 130 °C
View Scheme

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