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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

Lithium triethylborohydride Manufacturer/High quality/Best price/In stock

Cas:22560-16-3

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality Lithium triethylborohydride supplier in China

Cas:22560-16-3

Min.Order:0 Metric Ton

Negotiable

Type:Manufacturers

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Lithium triethylhydroborate

Cas:22560-16-3

Min.Order:1

Negotiable

Type:Other

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Lithium triethylborohydride

Cas:22560-16-3

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

Lithium triethylborohydride CAS 22560-16-3

Cas:22560-16-3

Min.Order:1 Gram

FOB Price: $6.0 / 9.0

Type:Trading Company

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Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

C6H16BLi LITHIUM TRIETHYLBOROHYDRIDE 22560-16-3

Cas:22560-16-3

Min.Order:1 Metric Ton

Negotiable

Type:Lab/Research institutions

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

New production CAS 22560-16-3 with best price

Cas:22560-16-3

Min.Order:10 Gram

FOB Price: $146.0 / 176.0

Type:Trading Company

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Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages High purity, all above 98.5%, no impurities after dissolution We will test each batch to ensure quality OEM and private brand services designed for free Various cap colors available We can also provide MT1 peptide powd

LITHIUM TRIETHYLBOROHYDRIDE CAS22560-16-3

Cas:22560-16-3

Min.Order:1 Kilogram

FOB Price: $5.0 / 10.0

Type:Trading Company

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Borate(1-),triethylhydro-, lithium (1:1), (T-4)- 22560-16-3

Cas:22560-16-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese

Agrochemical Intermediates, LITHIUM TRIETHYLBOROHYDRIDE CAS:22560-16-3

Cas:22560-16-3

Min.Order:1 Kilogram

FOB Price: $168.0 / 172.0

Type:Trading Company

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:22560-16-3

Cas:22560-16-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

Lithium triethylborohydride

Cas:22560-16-3

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Lithium triethylborohydride

Cas:22560-16-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Jinan Finer Chemical Co., Ltd

Name Lithium triethylborohydride Cas 22560-16-3 Appearance: cololess liquid Assay: 1 mol Capacity:200MT/year Application: Reducing agent Min.package: 1gram Standard: enterprise Brand: Finerchem Molecular Formula C6H15B.Li

Lithium triethylborohydride

Cas:22560-16-3

Min.Order:1 Gram

FOB Price: $52.0

Type:Lab/Research institutions

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Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

Lithium triethylborohydride

Cas:22560-16-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Shanghai Minstar Chemical Co., Ltd

LITHIUM TRIETHYLBOROHYDRIDE Basic information Product Name: LITHIUM TRIETHYLBOROHYDRIDE Synonyms: lithiumtriethylborohydride,calselect lt,;lithiumtriethylborohydride,calselect lt,intetrahydrofuran;Lithium triethylborohydrideLithium triethylhyd

LITHIUM TRIETHYLBOROHYDRIDE

Cas:22560-16-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

Lithium triethylborohydride

Cas:22560-16-3

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

LITHIUM TRIETHYLBOROHYDRIDE

Cas:22560-16-3

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

Lithium triethylborohydride

Cas:22560-16-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

Lithium triethylborohydride

Cas:22560-16-3

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

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Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

LITHIUMTRIETHYLBOROHYDRIDE

Cas:22560-16-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

Cas no.22560-16-3 98% Lithium Triethylborohydride

Cas:22560-16-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

Lithium triethylborohydride

Cas:22560-16-3

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

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Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

Lithium triethylborohydride

Cas:22560-16-3

Min.Order:0

Negotiable

Type:Other

inquiry

GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier

Lithium triethylborohydride

Cas:22560-16-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

JINHUA HUAYI CHEMICAL CO., LTD.

Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands

Lithium Triethylborohydride

Cas:22560-16-3

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Dingyan Chem Co., Ltd

high purity, manufacturer Application:Intermediate

Lithium triethylborohydride in THF

Cas:22560-16-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Shanghai Acmec Biochemical Technology Co., Ltd.

Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea

Acmec Lithium triethylborohydride 500ml

Cas:22560-16-3

Min.Order:1 bottle

Negotiable

Type:Lab/Research institutions

inquiry

Aecochem Corp.

Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS

Lithium triethylborohydride

Cas:22560-16-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

LithiuM triethylborohydride

Cas:22560-16-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

triethyl borane
97-94-9

triethyl borane

lithium hydride

lithium hydride

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

Conditions
ConditionsYield
in an autoclave near 200°C;
in an autoclave near 200°C;
In tetrahydrofuran
triethyl borane
97-94-9

triethyl borane

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

Conditions
ConditionsYield
With n-butyllithium In tetrahydrofuran; pentane byproducts: isobutylene; (N2); to stirred soln. of boranederiv. in THF was dropwise added pentane soln. of LiBu at -78°C, then mixt. was allowed to warm up to room temp.; not isolated, detected by (11)B-NMR;>99
triethyl borane
97-94-9

triethyl borane

lithium tri-t-butoxyaluminum hydride

lithium tri-t-butoxyaluminum hydride

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

Conditions
ConditionsYield
In tetrahydrofuran byproducts: Al{OC(CH3)3}; active intermediate;
In tetrahydrofuran byproducts: Al{OC(CH3)3}; active intermediate;
sodium triethylborohydride

sodium triethylborohydride

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
2: tetrahydrofuran
View Scheme
Multi-step reaction with 2 steps
2: tetrahydrofuran
View Scheme
{CH3N(PF2)2}3Co2(CO)2
64799-21-9

{CH3N(PF2)2}3Co2(CO)2

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

{{CH3N(PF2)2}3Co2(CO)(CHO)}(1-)

{{CH3N(PF2)2}3Co2(CO)(CHO)}(1-)

Conditions
ConditionsYield
In tetrahydrofuran reduction with excess LiEt3BH at -78°C; not isolated; various yields for various conditions.;100%
(η(6)-3-ethylanisole)tricarbonylchromium
88729-81-1

(η(6)-3-ethylanisole)tricarbonylchromium

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

(ethylbenzene)tricarbonylchromium
12203-31-5

(ethylbenzene)tricarbonylchromium

Conditions
ConditionsYield
With chlorhydric or trifluoroacetic acid In tetrahydrofuran N2-atmosphere; refluxing (2 h), acid addn.; extg. (Et2O), washing (satd. Na2CO3 soln., brine), drying (Na2SO4), filtering, evapn. (reduced pressure), recrystn. (hexane / Me2CO);100%
tris(triphenylphosphine)ruthenium(II) chloride
15529-49-4, 41756-81-4

tris(triphenylphosphine)ruthenium(II) chloride

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

hydridochlorotris(triphenylphosphine)ruthenium(II)
55102-19-7

hydridochlorotris(triphenylphosphine)ruthenium(II)

Conditions
ConditionsYield
In tetrahydrofuran IR;100%
In tetrahydrofuran; toluene (N2); stirred at room temp. for 30 min; concd.; ethanol added; cooled to -20°C; filtered; washed (ethanol and petroleum ether); dried in vacuo; NMR;>99
bis(1'-mesitylthiolatoferrocenyl)disulfane
326887-77-8

bis(1'-mesitylthiolatoferrocenyl)disulfane

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

lithium 1'-(mesitylthio)ferrocene-1-thiolate

lithium 1'-(mesitylthio)ferrocene-1-thiolate

Conditions
ConditionsYield
In tetrahydrofuran mixed, stirred for 1,5 h; not isolated;100%
(η(5):η(5)-(C5H3CO2Me)2)Mo2(CO)6
184488-45-7, 184243-69-4

(η(5):η(5)-(C5H3CO2Me)2)Mo2(CO)6

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

Li2(trans-1,1'-[η5:η5-(C5H3CO2Me)2]Mo2(CO)6)

Li2(trans-1,1'-[η5:η5-(C5H3CO2Me)2]Mo2(CO)6)

Conditions
ConditionsYield
In tetrahydrofuran byproducts: Et3B; 0°C; evapn. (vac.);100%
(CH3C(CH2P(C6H5)2)3)Re(CO)2(1+)*BF4(1-)=[(CH3C(CH2P(C6H5)2)3)Re(CO)2]BF4
166989-37-3

(CH3C(CH2P(C6H5)2)3)Re(CO)2(1+)*BF4(1-)=[(CH3C(CH2P(C6H5)2)3)Re(CO)2]BF4

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

(CH3C(CH2P(C6H5)2)3)Re(CO)2(H)
166989-33-9

(CH3C(CH2P(C6H5)2)3)Re(CO)2(H)

Conditions
ConditionsYield
In tetrahydrofuran; tetrahydrofuran-d8 N2-atmosphere; detd. by NMR spectroscopy;100%
tricarbonyl[η(6)-2-chloro(trimethylsilyl)benzene]chromium

tricarbonyl[η(6)-2-chloro(trimethylsilyl)benzene]chromium

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

tricarbonyl[η(6)-4-deuterio(trimethylsilyl)benzene]chromium
138496-16-9

tricarbonyl[η(6)-4-deuterio(trimethylsilyl)benzene]chromium

Conditions
ConditionsYield
With CF3COOH In tetrahydrofuran N2-atmosphere; stirring (-78°C, 50 min), CF3COOH addn.;100%
C41H49Cl2FeNOP2

C41H49Cl2FeNOP2

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

C41H50ClFeNOP2

C41H50ClFeNOP2

Conditions
ConditionsYield
In tetrahydrofuran at -30 - 28℃; Schlenk technique; Inert atmosphere; Glovebox;100%
C29H37Cl2FeNOP2

C29H37Cl2FeNOP2

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

C29H38ClFeNOP2

C29H38ClFeNOP2

Conditions
ConditionsYield
In tetrahydrofuran at -30 - 28℃; Schlenk technique; Inert atmosphere; Glovebox;100%
C26H39Cl2FeNOP2

C26H39Cl2FeNOP2

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

C26H40ClFeNOP2

C26H40ClFeNOP2

Conditions
ConditionsYield
In tetrahydrofuran at -30 - 28℃; Schlenk technique; Inert atmosphere; Glovebox;100%
[bis(2-diphenylphosphinophenyl)amide]PdCl

[bis(2-diphenylphosphinophenyl)amide]PdCl

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

C36H29NP2Pd

C36H29NP2Pd

Conditions
ConditionsYield
In tetrahydrofuran; benzene-d6 for 0.166667h; Inert atmosphere;100%
nido-NB10H13

nido-NB10H13

N,N,N,N,-tetramethylethylenediamine
110-18-9

N,N,N,N,-tetramethylethylenediamine

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

Li(1+)*2(CH3)2N(CH2)2N(CH3)2*{NB10H12}(1-)={Li((CH3)2N(CH2)2N(CH3)2)2}{NB10H12}

Li(1+)*2(CH3)2N(CH2)2N(CH3)2*{NB10H12}(1-)={Li((CH3)2N(CH2)2N(CH3)2)2}{NB10H12}

Conditions
ConditionsYield
In tetrahydrofuran byproducts: B(C2H5)3, H2; addn. of Li(BHEt3) in THF to soln. of the borane at -78°C, stirred for 5 min at room temp., volatiles removed in vac., addn. of THF, addn. of tmeda;; concentrated, washed three times with pentane, dried;;99%
6-azido-8,9:9,10-di-μ-hydro-1,2,3,4,5,7,7,8,9,10-decahydro-5,6-μ-amino-nido-decaborane

6-azido-8,9:9,10-di-μ-hydro-1,2,3,4,5,7,7,8,9,10-decahydro-5,6-μ-amino-nido-decaborane

N,N,N,N,-tetramethylethylenediamine
110-18-9

N,N,N,N,-tetramethylethylenediamine

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

Li(tmeda)2(1+)-{9-azido-3,4:3,8-di-μ-hydro-undecahydro-2-aza-1,5-didebor-closo-tridecaborate(1-)}

Li(tmeda)2(1+)-{9-azido-3,4:3,8-di-μ-hydro-undecahydro-2-aza-1,5-didebor-closo-tridecaborate(1-)}

Conditions
ConditionsYield
In tetrahydrofuran; dichloromethane addn. of LiBHEt3 in THF to B-compd. in THF (0°C), stirring (15 min, room temp.), removal of volatiles (vac.), dissolution (CH2Cl2), addn. of org. compd. in CH2Cl2; reprecipitated with CH2Cl2, layered with hexane;99%
Ir(CF3)Cl(CH3CN)(CO)[P(C6H5)3]2(1+)*SbF6(1-)=[Ir(CF3)Cl(CH3CN)(CO)(P(C6H5)3)2](SbF6)
105250-39-3

Ir(CF3)Cl(CH3CN)(CO)[P(C6H5)3]2(1+)*SbF6(1-)=[Ir(CF3)Cl(CH3CN)(CO)(P(C6H5)3)2](SbF6)

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

Ir(CF3)HCl(CO)[P(C6H5)3]2
131100-72-6, 105250-42-8

Ir(CF3)HCl(CO)[P(C6H5)3]2

Conditions
ConditionsYield
In tetrahydrofuran addn. of 1 equiv. LiEt3BH in THF to stirred soln. of Ir-complex in THF (under N2); addn. of n-hexane, evapn. (reduced pressure), grey solid dissolved in CH2Cl2, filtered, crystn. (CH2Cl2/EtOH), elem. anal.;99%
tetrachlorosilane
10026-04-7, 53609-55-5

tetrachlorosilane

(μ-dithio)bis(tricarbonyliron)
14243-23-3

(μ-dithio)bis(tricarbonyliron)

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

Si[S2Fe2(CO)6]2
71592-21-7

Si[S2Fe2(CO)6]2

Conditions
ConditionsYield
In tetrahydrofuran under N2, to the stirred soln. of 2.91 mmol Fe compd. in THF cooled to -78°C was added LiEt3BH in THF in small portions, to this was added SiCl4 over 3 min at -78°C, mixt. was warmed to room temp.; volatiles were removed in vac., solid extd. 4 times with CH2Cl2, filtered under N2 through a Celite pad supporteed on a fritted funnel, solventremoved in vac., recrystd. from CH2Cl2, elem. anal.;99%
[(CpCr(CO)2)2(μ,η(2)-P2)]

[(CpCr(CO)2)2(μ,η(2)-P2)]

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

[(CpCr(CO)2)2(μ-PH2)(μ-H)]
239134-51-1

[(CpCr(CO)2)2(μ-PH2)(μ-H)]

Conditions
ConditionsYield
In tetrahydrofuran Ar-atmosphere; excess hydride;99%
Fe2(CO)6(μ-SNMe)
88253-22-9

Fe2(CO)6(μ-SNMe)

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

trifluoroacetic acid
76-05-1

trifluoroacetic acid

Fe2(CO)6(μ-NHMe)(μ-SH)

Fe2(CO)6(μ-NHMe)(μ-SH)

Conditions
ConditionsYield
In tetrahydrofuran byproducts: Et2BO2CCF3, C2H6, CF3COO(1-); Ar-atmosphere; addn. of 2 equiv. of B-compd. to Fe-complex soln. at -78°C, addn. of excess CF3COOH, warming to room temp.; solvent removal (vac.), extn. into hexane, evapn.;99%
1-(tert-butyldimethylsilyl)-2-chloro-1,2-dihydro-1,2-azaborinine
1138164-75-6

1-(tert-butyldimethylsilyl)-2-chloro-1,2-dihydro-1,2-azaborinine

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

C4H4B(H)N(tert-butyldimethylsilyl)
1138164-76-7

C4H4B(H)N(tert-butyldimethylsilyl)

Conditions
ConditionsYield
In not given99%
tetrahydrofuran
109-99-9

tetrahydrofuran

C38H41ClIrOP*0.5CH2Cl2

C38H41ClIrOP*0.5CH2Cl2

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

C50H67IrLiO4P

C50H67IrLiO4P

Conditions
ConditionsYield
at -230℃; for 0.166667h; Inert atmosphere;99%
lithium triethylborohydride
22560-16-3

lithium triethylborohydride

17O-water
13968-48-4

17O-water

Li(17)OH

Li(17)OH

Conditions
ConditionsYield
In tetrahydrofuran byproducts: B(C2H5)3, H2; stirring stoich. amt. of H2(17)O and B-compd. in THF for 0.5 h at ca -5°C, then allowed to warm to room temp., stirred for 1 h, then under N2, solvent removed, solid heated to 100°C for 1 h, then at 250°C for 24 h at 1E-3 torr;98%
{manganese(carbonyl)5(COPh)}

{manganese(carbonyl)5(COPh)}

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

Li(1+)*Mn(CO)4(CHO)(COC6H5)(1-)=Li[Mn(CO)4(CHO)(COC6H5)]

Li(1+)*Mn(CO)4(CHO)(COC6H5)(1-)=Li[Mn(CO)4(CHO)(COC6H5)]

Conditions
ConditionsYield
With 1,2,4,5-tetrachlorobenzene In tetrahydrofuran byproducts: (C2H5)3B; NMR tube was dried at 110°C for 30 min, rinsed with Li(C2H5)3BH and THF, flushed with N2, sealed, a soln. of Mn-complex and 1,2,4,5-tetrachlorobenzene in THF was syringed, cooled to -50°C, a soln. of Li(C2H5)3BH in THF was added; monitored by NMR (1)H;98%
(μ-dithio)bis(tricarbonyliron)
14243-23-3

(μ-dithio)bis(tricarbonyliron)

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

dichlorodimethylgermanium
1529-48-2

dichlorodimethylgermanium

((CH3)2GeS2)Fe2(CO)6
74438-41-8

((CH3)2GeS2)Fe2(CO)6

Conditions
ConditionsYield
In tetrahydrofuran under N2, to the stirred soln. of 2.91 mmol Fe compd. in THF cooled to -78°C was added LiEt3BH in THF in portions, to this was added Me2GeCl2 at -78°C, warmed to room temp.; solvent evapd., chromy. (silicic acid-CH2Cl2), recrystd. from pentane, elem. anal.;98%
Fe(η3:η2-indenide)(1,2-bis(diethylphosphino)ethane)Br

Fe(η3:η2-indenide)(1,2-bis(diethylphosphino)ethane)Br

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

Fe(η3:η2-indenide)(1,2-bis(diethylphosphino)ethane)H

Fe(η3:η2-indenide)(1,2-bis(diethylphosphino)ethane)H

Conditions
ConditionsYield
In tetrahydrofuran at -78 - 20℃; for 2h; Schlenk technique; Inert atmosphere;98%
Pd(Cl)N(C6H4P(CH(CH3)2)2)2
779333-78-7

Pd(Cl)N(C6H4P(CH(CH3)2)2)2

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

C24H37NP2Pd

C24H37NP2Pd

Conditions
ConditionsYield
In tetrahydrofuran at -35 - 20℃; for 1h; Inert atmosphere;98%
(4,5-bis(diisopropylphosphino)-2,7,9,9-tetramethyl-9H-acridin-10-ide)NiCl

(4,5-bis(diisopropylphosphino)-2,7,9,9-tetramethyl-9H-acridin-10-ide)NiCl

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

(4,5-bis(diisopropylphosphino)-2,7,9,9-tetramethyl-9H-acridin-10-ide)NiH

(4,5-bis(diisopropylphosphino)-2,7,9,9-tetramethyl-9H-acridin-10-ide)NiH

Conditions
ConditionsYield
In tetrahydrofuran; benzene for 10h; Inert atmosphere;97.1%
lithium triethylborohydride
22560-16-3

lithium triethylborohydride

Li{(η5-cyclohexadienyl)tricarbonylchromium}

Li{(η5-cyclohexadienyl)tricarbonylchromium}

Conditions
ConditionsYield
In tetrahydrofuran N2-atmosphere;97%
Fe(η-C5H5)(CO)2(COMe)

Fe(η-C5H5)(CO)2(COMe)

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

Li(1+)*Fe(C5H5)(CO)(CHO)(COCH3)(1-)=Li[Fe(C5H5)(CO)(CHO)(COCH3)]

Li(1+)*Fe(C5H5)(CO)(CHO)(COCH3)(1-)=Li[Fe(C5H5)(CO)(CHO)(COCH3)]

Conditions
ConditionsYield
With 1,2,4,5-tetrachlorobenzene In tetrahydrofuran byproducts: (C2H5)3B; NMR tube was dried at 110°C for 30 min, rinsed with Li(C2H5)3BH and THF, flushed with N2, sealed, a soln. of Fe-complex and 1,2,4,5-tetrachlorobenzene in THF was syringed, cooled to -50°C, a soln. of Li(C2H5)3BH in THF was added; monitored by NMR (1)H;97%
(μ-dithio)bis(tricarbonyliron)
14243-23-3

(μ-dithio)bis(tricarbonyliron)

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

ethyl iodide
75-03-6

ethyl iodide

Fe2(CO)6(μ-SEt)2

Fe2(CO)6(μ-SEt)2

Conditions
ConditionsYield
In tetrahydrofuran under N2, to the stirred soln. of 2.91 mmol Fe compd. in THF cooled to -78°C was added LiEt3BH in THF in small portions, to this was added EtI, mixt. stirred for 1 h; solvent evapd., chromy. (silicic acid-10% CH2Cl2/pentane) (a,e isomer/e,e isomer: 2.7);96%
{RuCl2(H2C(C3H3N2)2)(C8H12)}
152391-10-1

{RuCl2(H2C(C3H3N2)2)(C8H12)}

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

{RuCl(H)(H2C(C3H3N2)2)(C8H12)}
152391-12-3

{RuCl(H)(H2C(C3H3N2)2)(C8H12)}

Conditions
ConditionsYield
In tetrahydrofuran (N2; Schlenk-tube technique); a soln. of LiB(C2H5)3H in THF is added to a THF soln. of Ru complex at -78°C; stirring; allowing to warm to room temp. for 1h; pptn.;; filtration; washing with diethyl ether; elem. anal.;;96%
[Fe(η(5)-C5H5)(CO)2(C(O)-p-C6H4OMe)]

[Fe(η(5)-C5H5)(CO)2(C(O)-p-C6H4OMe)]

lithium triethylborohydride
22560-16-3

lithium triethylborohydride

Li(1+)*Fe(C5H5)(CO)(CHO)(COC6H4OCH3)(1-)=Li[Fe(C5H5)(CO)(CHO)(COC6H4OCH3)]

Li(1+)*Fe(C5H5)(CO)(CHO)(COC6H4OCH3)(1-)=Li[Fe(C5H5)(CO)(CHO)(COC6H4OCH3)]

Conditions
ConditionsYield
With 1,2,4,5-tetrachlorobenzene In tetrahydrofuran NMR tube was dried at 110°C for 30 min, rinsed with Li(C2H5)3BH and THF, flushed with N2, sealed, a soln. of Fe-complex and 1,2,4,5-tetrachlorobenzene in THF was syringed, cooled to -50°C, a soln. of Li(C2H5)3BH in THF was added; monitored by NMR (1)H;96%

Raw Materials

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