Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:1486-28-8
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryHebei yanxi chemical co. LTD. has expanded a compositive entity from initially only as a small manufacturer. The company dedicated to the development, production and marketing of chemicals. After many years of efforts, we have established stable
Cas:1486-28-8
Min.Order:1 Metric Ton
FOB Price: $1.0 / 2.0
Type:Manufacturers
inquiryQingdao Greenchem international Trading Co.,Ltd. is the commercial company which is invested by BeiJing Greenchem Technology Co.,Ltd. in Qingdao. It takes charge of export and production promotion, as well as imports and selling relevant production
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:1486-28-8
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.
Cas:1486-28-8
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:1486-28-8
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryProduct Name: METHYLDIPHENYLPHOSPHINE Synonyms: METHYLDIPHENYLPHOSPHINE;DIPHENYLMETHYLPHOSPHINE;Methyldiphenylphsphine;Methyldiphenylphosphine,99%;Diphenylphosphinomethane;Methyldiphenylphosphine, 99% 25GR;Methyldiphenylphosphine, 99% 5GR;98% (
Cas:1486-28-8
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
Cas:1486-28-8
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryMETHYLDIPHENYLPHOSPHINECAS: 1486-28-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic in
Cas:1486-28-8
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:1486-28-8
Min.Order:4 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Superior quality moderate price & quick delivery Appearance: Colorless to light yellow liquiD Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:
Cas:1486-28-8
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providing h
SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe
Cas:1486-28-8
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryHigh quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:1486-28-8
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryHunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as:
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier
Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
Cas:1486-28-8
Min.Order:1 bottle
Negotiable
Type:Lab/Research institutions
inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
MethyldiphenylphosphineAppearance:detailed see specifications Storage:Keep away of light, cool place Package:25kg/drum;200kg/drum Application:It is an important raw material and intermediate used in Organic Synthesis, Pharmaceuticals, Agrochemicals a
good quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:25kg,50kg,180kg,200kg,250kg,1000kg,customization Application:Pharma;Industry;Agricultural;chemical reaserch Tran
We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as primary a
Methyldiphenylphosphine cas 1486-28-8Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
good quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:1g Application:Pharma;Industry;Agricultural;chemical reaserch Transportation:by express or by sea Port:Any port
The factory supplies Application:manufacturing supplies
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Conditions | Yield |
---|---|
In toluene mixing of the Mo compd. with the free phosphine (molar ratio 2.1:1) in toluene;; | A 100% B n/a |
Conditions | Yield |
---|---|
In toluene mixing of the Mo compd. with the free phosphine (molar ratio 2.0:1) in toluene;; | A 100% B n/a |
Conditions | Yield |
---|---|
In toluene mixing of the Mo compd. with the free phosphine (molar ratio 2.0:1) in toluene;; | A 100% B n/a |
Conditions | Yield |
---|---|
In dichloromethane mixing of the Mo compd. with the free phosphine (molar ratio 1.1:1) inCH2Cl2;; | A 100% B n/a |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride; cerium(III) chloride In tetrahydrofuran at 40℃; for 0.5h; | 98% |
With aluminium hydride*tetrahydrofuran In tetrahydrofuran for 0.5h; Heating; | 96% |
Stage #1: diphenyl(methyl)phosphine oxide With trityl tetrakis(pentafluorophenyl)borate In (2)H8-toluene at 20℃; Glovebox; Inert atmosphere; Stage #2: With phenylsilane In (2)H8-toluene at 80℃; for 1.5h; Glovebox; Inert atmosphere; Sealed tube; | 93% |
Diphenylphosphonigsaeure-trimethylsilylester
methyllithium
diphenyl(methyl)phosphine
Conditions | Yield |
---|---|
In tetrahydrofuran at 0 - 25℃; for 2h; | 96% |
Conditions | Yield |
---|---|
Stage #1: Ph2PCH2NHPh With methyllithium In toluene at -78 - 20℃; Inert atmosphere; Stage #2: methyl iodide In toluene at -78℃; Inert atmosphere; | 95% |
n-butyl magnesium bromide
methylmagnesium bromide
cis-2,10-dimethyl-<1,2,3>benzothiadiphospholo<2,3-b><1,2,3>benzothiadiphosphole
A
dibutyl-methyl-phosphine
B
n-Butyl-methyl-phenyl-phosphin
C
diphenyl(methyl)phosphine
D
4-methyl-2-[(5-methyl-2-sulfanylphenyl)phosphanyl]benzenethiol
Conditions | Yield |
---|---|
Stage #1: n-butyl magnesium bromide; cis-2,10-dimethyl-<1,2,3>benzothiadiphospholo<2,3-b><1,2,3>benzothiadiphosphole; phenylmagnesium bromide In tetrahydrofuran for 0.0833333h; Stage #2: methylmagnesium bromide In tetrahydrofuran Title compound not separated from byproducts; | A n/a B n/a C n/a D 90% |
methylmagnesium bromide
ethylmagnesium bromide
cis-2,10-dimethyl-<1,2,3>benzothiadiphospholo<2,3-b><1,2,3>benzothiadiphosphole
A
diethylmethylphosphine
B
ethylmethylphenylphosphine
C
diphenyl(methyl)phosphine
D
4-methyl-2-[(5-methyl-2-sulfanylphenyl)phosphanyl]benzenethiol
Conditions | Yield |
---|---|
Stage #1: ethylmagnesium bromide; cis-2,10-dimethyl-<1,2,3>benzothiadiphospholo<2,3-b><1,2,3>benzothiadiphosphole; phenylmagnesium bromide In tetrahydrofuran for 0.0833333h; Stage #2: methylmagnesium bromide In tetrahydrofuran Title compound not separated from byproducts; | A n/a B n/a C n/a D 90% |
Conditions | Yield |
---|---|
Stage #1: Ph2PCH2NH(t-Bu) With methyllithium In toluene at -78 - 20℃; Inert atmosphere; Stage #2: methyl iodide In toluene at -78℃; Inert atmosphere; | 89% |
trimethylsulphonium iodide
(trimethylsilyl)diphenylphosphine
diphenyl(methyl)phosphine
Conditions | Yield |
---|---|
Stage #1: trimethylsulphonium iodide With n-butyllithium In tetrahydrofuran; hexane at -70℃; for 0.166667h; Stage #2: (trimethylsilyl)diphenylphosphine In tetrahydrofuran; hexane at -70 - 20℃; for 0.5h; | 88% |
phenylsilane
Methylenetriphenylphosphorane
B
diphenyl(methyl)phosphine
Conditions | Yield |
---|---|
With bis(trimethylsilyl)amide yttrium(III) In benzene-d6 at 25℃; for 0.5h; Catalytic behavior; Reagent/catalyst; | A 88% B n/a |
Conditions | Yield |
---|---|
With 15-crown-5 In tetrahydrofuran at 25℃; for 6h; Inert atmosphere; | 88% |
1-methoxy-2-trimethylsilylethyne
(trimethylsilyl)diphenylphosphine
A
bis(trimethylsilyl)ketene
B
diphenyl(methyl)phosphine
Conditions | Yield |
---|---|
In acetonitrile for 48h; Ambient temperature; | A 65% B 82% |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride; water In 1,4-dioxane for 0.25h; Heating; | 79% |
With tetrakis(triphenylphosphine) palladium(0); hydrogen; triethylamine In 1,4-dioxane at 130℃; under 76000 Torr; Product distribution; other quaternary phosphonium salts; |
6,6'-dimethyl fulvene
(lithiomethyl)diphenylphosphane
A
lithium (1-methylethenyl)cyclopentadiene
B
dilithium salt of 2,4-bis(1,3-cyclopentadienyl)-4-methyl-1-pentene
C
dilithium salt of 6-(1,3-cyclopentadienyl)-6,8,8-trimethylbicyclo<3.3.0>octa-1,3-diene
D
lithium <1,1-dimethyl-2-(diphenylphosphino)ethyl>cyclopentadienide
E
diphenyl(methyl)phosphine
Conditions | Yield |
---|---|
In Petroleum ether at 27℃; for 168h; Product distribution; | A 5% B 30% C 25% D 12% E 78% |
6,6'-dimethyl fulvene
(lithiomethyl)diphenylphosphane
A
dilithium salt of 2,4-bis(1,3-cyclopentadienyl)-4-methyl-1-pentene
B
dilithium salt of 6-(1,3-cyclopentadienyl)-6,8,8-trimethylbicyclo<3.3.0>octa-1,3-diene
C
lithium <1,1-dimethyl-2-(diphenylphosphino)ethyl>cyclopentadienide
D
diphenyl(methyl)phosphine
Conditions | Yield |
---|---|
In Petroleum ether at 27℃; for 168h; | A n/a B n/a C 12% D 78% |
N-phenyl methyldiphenyl-λ5-phosphazene
diphenyl(methyl)phosphine
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran for 6h; Ambient temperature; | 78% |
phenylsilane
Methylenetriphenylphosphorane
A
Diphenyl-phenylsilanylmethyl-phosphane
C
diphenyl(methyl)phosphine
Conditions | Yield |
---|---|
With C31H52N2PSi4Y In benzene-d6 at 25℃; for 3.5h; | A n/a B 77% C n/a |
[Li(THF)1.5][(CO)4W(μ-PPh2)2Os(CO)2(CHO)(PMePh2)]
Li[(CO)4W(μ-PPh2)2Os(H)(CO)2(PMePh2)]
Li[(CO)4W(μ-PPh2)2Os(H)(CO)3]
C
diphenyl(methyl)phosphine
Conditions | Yield |
---|---|
In dimethylsulfoxide-d6 under N2, soln. of educt in (CD3)2SO heated at 100°C for 11 h; identified by NMR; | A 25% B 75% C n/a |
Conditions | Yield |
---|---|
Stage #1: triphenylphosphine In tetrahydrofuran at 20℃; Inert atmosphere; Stage #2: methyl iodide In tetrahydrofuran for 0.166667h; Inert atmosphere; | 75% |
methyl magnesium iodide
chloro-diphenylphosphine
diphenyl(methyl)phosphine
Conditions | Yield |
---|---|
In diethyl ether at -35℃; Inert atmosphere; | 74% |
methyl(phenyl)(trimethylsilyl)phosphine
chlorobenzene
diphenyl(methyl)phosphine
Conditions | Yield |
---|---|
With bis(triphenylphosphine)nickel(II) chloride; potassium tert-butylate In 1,4-dioxane at 90℃; for 12h; Inert atmosphere; | 69% |
Conditions | Yield |
---|---|
In pentane at -30 - 20℃; for 16h; | 60% |
Conditions | Yield |
---|---|
With CO In tetrahydrofuran treatment with CO; addn. of pentane; | A 60% B n/a |
borane-THF
diphenyl(methyl)phosphine oxide
A
diphenyl(methyl)phosphine
B
diphenylmethylphosphine-borane complex
Conditions | Yield |
---|---|
With titanium(IV) isopropylate In tetrahydrofuran; toluene at 80℃; for 24h; Schlenk technique; Inert atmosphere; | A 57% B 20% |
With titanium(IV) isopropylate In tetrahydrofuran; toluene at 80℃; for 24h; Schlenk technique; Inert atmosphere; | A 40% B 45% |
5-lithiomethyl-5H-dibenzophosphole
A
5-methyl-5H-dibenzophosphole
B
diphenyl(methyl)phosphine
C
benzene
Conditions | Yield |
---|---|
by hydrolysis; | A 43% B 10% C n/a |
2-dimethylsilyl-1-diphenylphosphinoethane
B
diphenyl(methyl)phosphine
Conditions | Yield |
---|---|
In diethyl ether byproducts: CH4; (N2), dried solvents, -40°C, dropwise addn. of educts, 4 h, evapn. in vac. (same temp.), addn. of petroleum ether yield yellow pptn., cooled down to -78°C; filtration ppt., washing (pentane), dried (high vac.), elem. anal.; | A 42% B n/a |
[{((2,6-dimethylphenyl)NC(methyl))2CH}AlH2]
Methylenetriphenylphosphorane
B
diphenyl(methyl)phosphine
Conditions | Yield |
---|---|
In benzene at 60℃; for 2h; Glovebox; Heating; | A 21% B n/a |
diethyl ether
sodium methylate
chloro-diphenylphosphine
A
diphenyl(methyl)phosphine
B
diphenyl(methyl)phosphine oxide
Conditions | Yield |
---|---|
With polymeric complex of oxodiperoxochromium(VI) compound and pyrazine (Pyz-CrO5)n In dichloromethane for 0.1h; Ambient temperature; | 100% |
With dihydrogen peroxide In dichloromethane; water at 20℃; for 3h; Glovebox; Inert atmosphere; | 100% |
With α-azohydroperoxides In benzene-d6 at 32℃; | 95% |
Phenyl azide
diphenyl(methyl)phosphine
N-phenyl methyldiphenyl-λ5-phosphazene
Conditions | Yield |
---|---|
In dichloromethane at 25℃; for 4h; Staudinger reaction; | 100% |
diphenyl(methyl)phosphine
Conditions | Yield |
---|---|
With borane-THF In tetrahydrofuran at -78 - 20℃; | 100% |
With dimethylsulfide borane complex In tetrahydrofuran at 25℃; for 1h; | 91% |
With dimethylsulfide borane complex complexation; |
diphenyl(methyl)phosphine
Conditions | Yield |
---|---|
With iodine In diethyl ether at 20℃; for 48h; Addition; | 100% |
Conditions | Yield |
---|---|
In pentane at 0℃; Addition; | 100% |
(bicyclo[2.2.1]hepta-2,5-diene)tetracarbonylmolybdenum(0)
diphenyl(methyl)phosphine
cis-{molybdenum(0)(carbonyl)4(P(phenyl)2(methyl))2}
B
bicyclo[2.2.1]hepta-2,5-diene
Conditions | Yield |
---|---|
In tetrahydrofuran reaction in a calorimeter under argon; | A 100% B n/a |
diphenyl(methyl)phosphine
Conditions | Yield |
---|---|
With PMePh2 In dichloromethane; dichloromethane-d2 shaken for 1 min; evapn., not isolated, identified by NMR-spectroscopy;; | 100% |
diphenyl(methyl)phosphine
Conditions | Yield |
---|---|
In dichloromethane N2 atmosphere; addn. of phosphine to Rh complex, stirring (30 min., room temp.); evapn. (vac.), recrystn. (CH2Cl2/hexane); elem. anal.; | 100% |
diphenyl(methyl)phosphine
Conditions | Yield |
---|---|
In dichloromethane N2 atmosphere; addn. of phosphine to Rh complex, stirring (30 min., room temp.); evapn. (vac.), recrystn. (CH2Cl2/hexane); | 100% |
Conditions | Yield |
---|---|
In chloroform-d1 byproducts: CO; (N2); stirring at ambiente temp.; react. followed by (1)H NMR; completed after 20 h; evapn. to dryness; recrystn. from pure hexane; elem. anal.; (31)P-, (1)H-, (13)C-NMR; IR; | 100% |
diphenyl(methyl)phosphine
Conditions | Yield |
---|---|
In not given | 100% |
(Z)-methyl 2-azido-3-phenylacrylate
diphenyl(methyl)phosphine
3-methoxycarbonyl-1-methyl-1,1,4-triphenyl-2-aza-1λ5-phosphabuta-1,3-diene
Conditions | Yield |
---|---|
In diethyl ether Ambient temperature; | 99% |
Conditions | Yield |
---|---|
In not given Re-complex reacted with ligand according to Chatt, J; Leigh, G. J; Mingos, D. M. P.; Paske, R. J. J. Chem. Soc. A 1968, 2636; | 99% |
diphenyl(methyl)phosphine
diphenylmethylphosphine-borane complex
Conditions | Yield |
---|---|
In tetrahydrofuran under N2, Schlenk techniques; soln. of P compd. (1.35 mmol) added to soln. of B compd. (1.30 mmol) at -78°C with stirring, warmed to roomtemp. overnight; evapd.; | 99% |
diphenyl(methyl)phosphine
[((diphenylmethylphosphane)2Pd)2(P2C(=N(iPr)2))](BF4)
Conditions | Yield |
---|---|
In dichloromethane 4 equivs. of phosphine, stirring for 30 min at room temp.; evapn., washing (MePh, ether); NMR spectroscopy; | 99% |
diphenyl(methyl)phosphine
Conditions | Yield |
---|---|
In toluene (Ar); std. Schlenk technique; soln. of P ligand in toluene was added dropwise to stirred soln. of Rh complex in toluene; soln. was stirred at room temp. for 20 h; solvent removed (vac.); | 99% |
o-Ph2PC6H4CH2OCH2C5H4N-2
diphenyl(methyl)phosphine
mer-[(Ph2PC6H4CHOCH2C5H4N-κ(3)P,C,N)Ir(H)(Cl)(PMePh2)]
Conditions | Yield |
---|---|
In toluene (Ar); std. Schlenk technique; soln. of P ligand in toluene was added dropwise to stirred soln. of Ir complex (0.5 equiv.) and P-N ligand (1 equiv.) in toluene; soln. was stirred at room temp. for 12 h; solvent removed (vac.); | 99% |
dichloromethane
water
diphenyl(methyl)phosphine
cobalt(II) chloride
zinc
B
cobalt
C
zinc(II) chloride
Conditions | Yield |
---|---|
In dichloromethane | A n/a B 99% C n/a D n/a |
diphenyl(methyl)phosphine
bis(methyldiphenylphosphine)nickel(II) chloride
Conditions | Yield |
---|---|
In ethanol at 80℃; for 0.5h; Sealed tube; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
In chloroform Inert atmosphere; | 99% |
diphenyl(methyl)phosphine
azidoformiate de methyle
P,P-diphenyl-P-(methyl)(N-methoxycabonyl)phosphazene
Conditions | Yield |
---|---|
In diethyl ether Staudinger reaction; | 98% |
N-[5-(bromomethyl)-4-(4-fluorophenyl)-6-(propan-2-yl)pyrimidin-2-yl]-N-methylmethanesulfonamide
diphenyl(methyl)phosphine
Conditions | Yield |
---|---|
In tetrahydrofuran at 50℃; for 0.25h; | 98% |
iron pentacarbonyl
diphenyl(methyl)phosphine
Fe(CO)4PPh2Me
Conditions | Yield |
---|---|
cyclopentadienyl iron(II) dicarbonyl dimer In toluene to boiling soln. of Fe(CO)5 and catalyst added ligand, heated for 1.75 h; evapd. in vac., chromd., recrystd.; | 98% |
[(η(5)-C5H4Me)Fe(CO)2]2 In toluene to boiling soln. of Fe(CO)5 and catalyst added ligand, heated for 1.25 h; evapd. in vac., chromd., recrystd.; | 98% |
cobalt(II) chloride dihydrate In toluene ligand and catalyst added to toluene, stirred soln. brought to reflux, Fe(CO)5 added to this soln., reflux continued for 1 h under N2; catalyst and excess ligand removed by chromy., solvent and excess Fe(CO)5 removed by evapn.; | 98% |
pentamethylcyclopentadienyliron(III) dicarbonyl dimer In toluene to boiling soln. of Fe(CO)5 and catalyst added ligand, heated for 1.25 h; evapd. in vac., chromd., recrystd.; | 96% |
cobalt(II)-iodide * 4 H2O In toluene ligand and catalyst added to toluene, stirred soln. brought to reflux, Fe(CO)5 added to this soln., reflux continued for 1.5 h under N2; catalyst and excess ligand removed by chromy., solvent and excess Fe(CO)5 removed by evapn.; | 78% |
diphenyl(methyl)phosphine
Conditions | Yield |
---|---|
In pentane; benzene react. of Pd complex with phosphine in benzene and addn. of pentane; | 98% |
In benzene addn. of pentane; cooling to -30°C; decanting; | 90% |
thallium(I) tetrafluoroborate
diphenyl(methyl)phosphine
Conditions | Yield |
---|---|
In tetrahydrofuran TlBF4 is added to a soln. of the starting complex and the phosphine in THF, stirred overnight; cooled to -40°C, filtered, the filtrate is evapd. to dryness, elem. anal.; | 98% |
About|Contact|Cas|Product Name|Molecular|Country|Encyclopedia
Message|New Cas|MSDS|Service|Advertisement|CAS DataBase|Article Data|Manufacturers | Chemical Catalog
©2008 LookChem.com,License: ICP
NO.:Zhejiang16009103
complaints:service@lookchem.com Desktop View