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inquiryName PEt3/Triethylphosphine CAS NO. 554-70-1 Molecular Formula C6H15P Molecular Weight 118.16 EINECS 209-068-8
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inquiryTriethylphosphine Basic information Product Name: Triethylphosphine Synonyms: AURORA KA-1111;CYTOP(R) 320;(C2H5)3P;Phosphorus triethyl;tl409;triethylphosphane;Triethyl-phosphane;triethyl-phosphin CAS: 554-70-1 MF: C6H15P MW: 118.16 EI
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Conditions | Yield |
---|---|
In dichloromethane mixing of the Mo compd. with the free phosphine (molar ratio 4.5:1) in CH2Cl2;; | A 100% B n/a |
In toluene mixing of the Mo compd. with the free phosphine (molar ratio 2.1:1) in toluene;; | A 100% B n/a |
Conditions | Yield |
---|---|
With phosphan; zinc(II) oxide In acetone at 0℃; for 12h; Solvent; Reagent/catalyst; Temperature; Irradiation; | 96% |
Conditions | Yield |
---|---|
With phenylsilane; C28H16F24O8S2Si In (2)H8-toluene at 100℃; for 48h; Inert atmosphere; | 91% |
With aluminium hydride In 1,2-dimethoxyethane at 0 - 65℃; for 12h; Inert atmosphere; Schlenk technique; | 70% |
With chromium |
ethylmagnesium bromide
cis-2,10-dimethyl-<1,2,3>benzothiadiphospholo<2,3-b><1,2,3>benzothiadiphosphole
A
triethylphosphine
B
4-methyl-2-[(5-methyl-2-sulfanylphenyl)phosphanyl]benzenethiol
Conditions | Yield |
---|---|
In tetrahydrofuran | A n/a B 90% |
sodium tetrahydroborate
cis,trans-dicarbonylbis(triethylphosphine)(dithioformate-κ2-S)manganese
B
triethylphosphine
Conditions | Yield |
---|---|
In ethanol; dichloromethane Addn. of a NaBH4 soln. (EtOH) to a stirred soln. of Mn-complex in CH2Cl2 under N2, stirring (1.5 h), colour turns from deep blue to bright red.; Evapn. of solvent in vac., pumping for 1 h to eleminate the free phosphine, extg. of red solid (hexane), filtn., addn. of EtOH, slow evapn. in vac., elem. anal.; | A 90% B n/a |
Conditions | Yield |
---|---|
Stage #1: chloroethane With magnesium; methyl iodide In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; ethyl acetate at 40 - 50℃; for 2.5h; Inert atmosphere; Stage #2: With phosphorus trichloride In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; ethyl acetate at 5℃; for 4h; Concentration; Temperature; Inert atmosphere; | 89.9% |
trans-platinum(triethylphosphine)2(chloro)2
B
(Et3P)2Pt{η2-(PSiMe3)2}
C
Tris(trimethylsilyl)phosphane
D
triethylphosphine
Conditions | Yield |
---|---|
In toluene under protective gas; 8.8 mmol of the Li salt in toluene added to 4 mmol of the Pt complex in toluene at -20°C; mixt. warmed to 20°C and stirred for 2 d; filtration; filtrate evapd. in vac.; fractionated crystn.; | A 12% B 7% C n/a D n/a |
diethyl ether
triphenylmethyl sodium
tetraethylphosphonium iodide
A
triphenylmethane
B
triethylphosphine
Conditions | Yield |
---|---|
With phosphonium iodide at 160℃; entsteht das Hydrojodid; |
ethanol
sodium ethanolate
A
styrene
B
triethylphosphine oxide
C
1-butylbenzene
D
triethylphosphine
Conditions | Yield |
---|---|
beim anschliessenden Erhitzen unter Stickstoff; |
ethanol
sodium ethanolate
A
1,1-Diphenylethylene
B
triethylphosphine oxide
C
1,1-diphenylbutane
D
triethylphosphine
Conditions | Yield |
---|---|
beim anschliessenden Erhitzen in einer Stickstoff-Atmosphaere unter vermindertem Druck; |
Conditions | Yield |
---|---|
With phosphonium iodide at 180℃; entsteht das Hydrojodid; |
dichlorotriethylphosphorane
triethylphosphine
Conditions | Yield |
---|---|
With sodium amalgam; ethanol |
fluoren-9-ylidene-triethylphosphoranylidene-hydrazine
A
di-fluoren-9-ylidene-hydrazine
B
triethylphosphine
Conditions | Yield |
---|---|
at 200 - 210℃; im Vakuum; |
Conditions | Yield |
---|---|
With diethyl ether |
Conditions | Yield |
---|---|
With diethyl ether; phosphorus tribromide das Reaktionsprodukt wird im Kohlendioxydstrom destilliert; | |
With phosphorus trichloride at -20℃; |
Conditions | Yield |
---|---|
With tetraphosphorus trisulfide; diethyl ether |
Conditions | Yield |
---|---|
With diethyl ether; phosphorus trichloride entsteht eine Verbindung mit Zinkchlorid; |
Conditions | Yield |
---|---|
With phosphorus trichloride und Behandeln des Reaktionsprodukts mit wss.NaOH; |
Conditions | Yield |
---|---|
With phosphorus trichloride |
triethyl-phenylthiocarbamoyl-phosphonium betaine
A
phenyl isothiocyanate
B
triethylphosphine
Conditions | Yield |
---|---|
beim Erhitzen; |
triethyl-diphenylacetyl-phosphonium betaine
A
diphenyl ketene
B
triethylphosphine
Conditions | Yield |
---|---|
at 100℃; |
tetraethylphosphonium; tetraethylphosphonium acetate
A
methane
B
triethylphosphine oxide
C
butanone
D
triethylphosphine
Conditions | Yield |
---|---|
beim Erhitzen; Produkt 5: Aethylen, Produkt 6: CO2; |
triethylbenzyl phosphonium chloride
A
benzyl chloride
B
triethylphosphine
Conditions | Yield |
---|---|
at 340℃; |
A
ethane
B
triethylphosphine oxide
C
ethylbenzene
D
triethylphosphine
Conditions | Yield |
---|---|
bei der Destillation; Produkt 5: Styrol; |
A
ethene
B
triethylphosphine oxide
C
pentan-3-one
D
triethylphosphine
Conditions | Yield |
---|---|
at 200 - 230℃; Produkt 5: CO2, Produkt 6: CO; |
A
ethane
B
triethylphosphine oxide
C
ethylbenzene
D
triethylphosphine
Conditions | Yield |
---|---|
bei der Destillation; Produkt 5: Styrol; |
Conditions | Yield |
---|---|
at 350 - 380℃; |
Conditions | Yield |
---|---|
With sodium phosphide |
ethene
methyl iodide
A
tetraethylphosphonium iodide
B
triethylphosphine
Conditions | Yield |
---|---|
With phosphorous; cyclohexane at 250℃; under 661957 Torr; unter Einleiten von Wasserstoff; |
triethylphosphine
Conditions | Yield |
---|---|
With iodine In diethyl ether at 20℃; for 48h; Addition; | 100% |
Conditions | Yield |
---|---|
In pentane at 0℃; Addition; | 100% |
Conditions | Yield |
---|---|
With pyridine In toluene at 85℃; for 21h; | 100% |
Conditions | Yield |
---|---|
In toluene at 20℃; | 100% |
1,1,2,2-tetrachloro-1,2-bis(t-butylamido)1,2-bis(t-butylamine)ditungsten(III)(3W-W)
triethylphosphine
1,1,2,2-tetrachloro-1,2-bis(t-butylamido)1,2-bis(triethylphsphine)-ditungsten(III)(3W-W)
Conditions | Yield |
---|---|
In pentane under dry N2; addn. of phosphine to W-complex in n-pentane, stirring (10 min); solvent removal (vac.); | 100% |
(bicyclo[2.2.1]hepta-2,5-diene)tetracarbonylmolybdenum(0)
triethylphosphine
cis-{molybdenum(0)(carbonyl)4(P(ethyl)3)2}
B
bicyclo[2.2.1]hepta-2,5-diene
Conditions | Yield |
---|---|
In tetrahydrofuran under argon; reaction in a calorimeter; | A 100% B n/a |
triethylphosphine
Conditions | Yield |
---|---|
In benzene (under N2 or Ar) addn. of P-compd. to Pt-complex in benzene at room temp., standing overnight (ambient temp.); solvent removal (vac.); elem. anal.; | 100% |
Conditions | Yield |
---|---|
In dichloromethane The soln. of reagents in CH2Cl2 was stirred for 10 min at 25°C (N2 atm.);; hexane was added, concd., filtered, washed with Et2O-hexane, recrystd. from CH2Cl2-hexane;; | 100% |
Conditions | Yield |
---|---|
In dichloromethane byproducts: P(C6H5)3; mixing of the Mo compd. with the free phosphine (molar ratio 2.5:1) in CH2Cl2;; | 100% |
Conditions | Yield |
---|---|
In dichloromethane-d2 PEt3 is added to Fe-Au-compd. in CD2Cl2 in a NMR-tube; monitored by (31)P-NMR-spectroscopy; | 100% |
Conditions | Yield |
---|---|
In toluene mixing of the Mo compd. with the free phosphine (molar ratio 2.0:1) in toluene;; | A 100% B n/a |
Conditions | Yield |
---|---|
In toluene PEt3 was added to a soln. of (Cu(OSiPh3))4*toluene in toluene (molar ratio 1.38:0.17) under Argon and the mixt. stirred for 16 h;; the solvent was evapd. in vac. and the resulting oil kept in a dynamic vac. at ca. 60°C for 4 h for slow solidification; elem. anal.;; | 100% |
(PEt3)2Pt(2,2'-biphenyl)
hydrogen
triethylphosphine
trans-(PEt3)2Pt(α-biphenyl)H
Conditions | Yield |
---|---|
In benzene-d6 H2-atmosphere (1 atm); stirring (80°C, 12 h); evapn.; | 100% |
5,10,15-tris(pentafluorophenyl)corrole manganese(V) (N-mesityl)
triethylphosphine
manganeser(III) 5,10,15-tris(pentafluorophenyl)corrole NPEt3(mesityl)
Conditions | Yield |
---|---|
In toluene Irradiation (UV/VIS); (Ar), at 85°C for 21 h; | 100% |
5,10,15-tris(pentafluorophenyl)corrole manganese(V) (N-2,4,6-trichlorophenyl)
triethylphosphine
manganese(III) 5,10,15-tris(pentafluorophenyl)corrple NPEt3(2,4,6-trichlorophenyl)
Conditions | Yield |
---|---|
In toluene Irradiation (UV/VIS); (Ar), at 20°C for < 1 min; | 100% |
Conditions | Yield |
---|---|
In hexane (N2); standard Schlenk technique; hexane and PEt3 were added via syringeto mixt. of Ru complex and ligand; mixt. was stirred at room temp. for 20 h; volatiles evapd. with oil diffusion pump; crystd. from hexane at -30°C; recrystd. (pentane); | 100% |
(η(3)-pentadienyl)Ir(PEt3)2
triethylphosphine
((1,4,5-η)pentadienyl)Ir(PEt3)3
Conditions | Yield |
---|---|
In benzene-d6 N2-atmosphere, NMR tube; detd. by NMR spectroscopy; | 100% |
triethylphosphine
Conditions | Yield |
---|---|
In not given | 100% |
triethylphosphine
triethylphosphane hydrobromide
Conditions | Yield |
---|---|
With hydrogen bromide In water at 0 - 20℃; Inert atmosphere; | 100% |
With hydrogen bromide In water at 0 - 20℃; Inert atmosphere; | 97% |
With hydrogen bromide |
Conditions | Yield |
---|---|
In hexane for 0.166667h; Inert atmosphere; Glovebox; | 100% |
Conditions | Yield |
---|---|
In benzene-d6 at 20℃; for 0.0833333h; Inert atmosphere; Schlenk technique; | 100% |
bis(1,5-cyclooctadiene)nickel (0)
3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)naphthalen-2-yl trifluoromethanesulfonate
lithium bromide
triethylphosphine
Conditions | Yield |
---|---|
In tetrahydrofuran; hexane at 20℃; for 1h; Inert atmosphere; | 100% |
triethylphosphine
(triethylphosphine)chlorogold(I)
Conditions | Yield |
---|---|
Stage #1: gold(III) tetrachloride trihydrate With 2,2'-thiobis-ethanol In water Stage #2: triethylphosphine In ethanol; water at 0 - 20℃; for 2h; | 100% |
triethylphosphine
triethyldifluorophosphorane
Conditions | Yield |
---|---|
With xenon fluoride In dichloromethane at 20℃; for 1h; Inert atmosphere; | 99% |
With 1-pentanamine hydrofluoride; N,N,N,N-tetraethylammonium tetrafluoroborate In acetonitrile anodic oxidation; | 80% |
(i) sulfur, benzene, (ii) SbF3; Multistep reaction; |
toluene-4-sulfonic acid
acetone
triethylphosphine
Toluene-4-sulfonatetriethyl-(1-hydroxy-1-methyl-ethyl)-phosphonium;
Conditions | Yield |
---|---|
1) -78 deg C, 4h, 2) RT; | 99% |
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 0.833333h; Inert atmosphere; | 99% |
In dichloromethane at 25℃; for 24h; Inert atmosphere; | 98.4% |
In diethyl ether Ambient temperature; |
[Co2Rh2(CO)12]
bis(triphenylphosphine)iminium chloride
triethylphosphine
A
[bis(triphenylphospine)nitrogen(1+)][Co(CO)4]
trans-ClRh(CO)(PEt3)2
Conditions | Yield |
---|---|
In dichloromethane N2-atmosphere; addn. of (PPN)Cl to Co/Rh complex, then addn. of 2 equivs. PEt3; solvent removal (vac.), hexane addn., filtration, washing (hexane); | A 98.3% B 99% |
triethylphosphine
Conditions | Yield |
---|---|
In further solvent(s) Schlenk flask; in aniline, flask was sealed and heated at 50°C with stirring for 2 d; mixt. was filtered, layered with MeCN, ppt. was filtered off, washed with Et2O; NMR; | 99% |
triethylphosphine
Conditions | Yield |
---|---|
In acetonitrile byproducts: P(C6H5)3; under N2; monitored by (1)H-NMR; | 99% |
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