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Cas:23683-68-3
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inquiry3-BroMoperylene Basic information Product Name: 3-BroMoperylene Synonyms: 3-BroMoperylene CAS: 23683-68-3 MF:
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inquiry3-BroMoperylene CAS:23683-68-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedi
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiry1, High quality with competitive price:2, Fast and safe delivery3.Excellent pre-sales and after-sales service4. Well-trained and professional technologist and sales with rich experience in the field for 5-10 yearsAppearance:see detailed specification
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Our Company main product 一:suzuki reaction customization 二:Boronic acid derivative ①:phenylboronic acid derivative ②:Phenylboronic acid pinacol ester derivative ③:Potassium phenyltrifluoroborate derivative ④:Phenylboronic acid MIDA ester derivative
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3-bromoperylene CAS NO.23683-68-3 Application:3-bromoperylene CAS NO.23683-68-3
3-BROMOPERYLENEAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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3-bromoperylene CAS NO.23683-68-3Appearance:off-white fine crystalline powder Storage:Dry and ventilated Package:Standard or as customer's require Application:intermediates Transportation:Delivery by EMS, DHL, FEDEX, UPS, TNT
Cas:23683-68-3
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inquiry3-bromoperylene CAS NO.23683-68-3Appearance:off-white fine crystalline powder Storage:Dry and ventilated Package:Standard or as customer's require Application:intermediates Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small am
Cas:23683-68-3
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inquirygood quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:100mg Application:Pharma;Industry;Agricultural;chemical reaserch Transportation:by express or by sea Port:Any po
PERYLENE
3-bromoperylene
Conditions | Yield |
---|---|
With N-Bromosuccinimide In tetrahydrofuran at 20℃; for 40h; Schlenk technique; Inert atmosphere; | 100% |
With N-Bromosuccinimide In tetrahydrofuran at 20℃; for 24h; | 95% |
With N-Bromosuccinimide In N,N-dimethyl-formamide at 20℃; Inert atmosphere; | 94% |
3-bromoperylene
Conditions | Yield |
---|---|
With N-Bromosuccinimide In dichloromethane at 20℃; | 100% |
3-bromoperylene
Conditions | Yield |
---|---|
With N-Bromosuccinimide In dichloromethane at 20℃; | 100% |
PERYLENE
A
3,10-Dibromoperylene
B
3,9-dibromoperylene
C
3-bromoperylene
Conditions | Yield |
---|---|
With N-Bromosuccinimide In N,N-dimethyl-formamide at 20℃; | A n/a B 90% C n/a |
With N-Bromosuccinimide In dichloromethane at 20℃; for 2h; | A n/a B n/a C 30% |
With N-Bromosuccinimide In dichloromethane at 20℃; for 2h; Yields of byproduct given. Title compound not separated from byproducts; |
Triisopropyl borate
3-bromoperylene
water
(perylene-3-yl)boronic acid
Conditions | Yield |
---|---|
Stage #1: 3-bromoperylene With n-butyllithium In tetrahydrofuran for 0.25h; Cooling; Stage #2: Triisopropyl borate In tetrahydrofuran Stage #3: water In tetrahydrofuran | 100% |
Conditions | Yield |
---|---|
With piperidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 80℃; for 14h; Alkylation; Hagihara coupling; | 98% |
With piperidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 80℃; for 14h; Yield given; | |
With tris-(dibenzylideneacetone)dipalladium(0); copper(l) iodide; triphenylphosphine Schlenk technique; Inert atmosphere; |
3-bromoperylene
trimethylsilylacetylene
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine In N,N-dimethyl-formamide at 85℃; Inert atmosphere; | 97% |
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); N-ethyl-N,N-diisopropylamine In dichloromethane at 60℃; for 24h; Inert atmosphere; Schlenk technique; | 62% |
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine In N,N-dimethyl-formamide at 80℃; for 24h; Inert atmosphere; | 183 mg |
With piperidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 60 - 70℃; for 2h; Sonogashira Cross-Coupling; |
1,2,4,5-Tetrafluorobenzene
3-bromoperylene
3-(2,3,5,6-tetrafluorophenyl)perylene
iodine
3-(2,3,5,6-tetrafluoro-4-iodophenyl)perylene
Conditions | Yield |
---|---|
Stage #1: 1,2,4,5-Tetrafluorobenzene; 3-bromoperylene; 3-(2,3,5,6-tetrafluorophenyl)perylene With n-butyllithium In tetrahydrofuran; hexane at -60℃; for 2h; Schlenk technique; Inert atmosphere; Stage #2: iodine at -78℃; for 3h; Schlenk technique; Inert atmosphere; | 94% |
1,2,4,5-Tetrafluorobenzene
3-bromoperylene
3-(2,3,5,6-tetrafluorophenyl)perylene
bromine
C26H11BrF4
Conditions | Yield |
---|---|
Stage #1: 1,2,4,5-Tetrafluorobenzene; 3-bromoperylene; 3-(2,3,5,6-tetrafluorophenyl)perylene With n-butyllithium In tetrahydrofuran; hexane at -60℃; for 2h; Schlenk technique; Inert atmosphere; Stage #2: bromine at -78℃; for 3h; Schlenk technique; Inert atmosphere; | 93% |
3-bromoperylene
bis(pinacol)diborane
4,4,5,5-tetramethyl-2-((perylene-3-yl)phenyl)-1,3,2-dioxaborolan
Conditions | Yield |
---|---|
With potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride In 1,4-dioxane at 70℃; for 15h; | 91% |
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate In 1,4-dioxane at 80℃; for 19h; Inert atmosphere; | 62% |
With potassium acetate In 1,4-dioxane at 80℃; for 48h; Reagent/catalyst; Temperature; Inert atmosphere; | 52.4% |
Conditions | Yield |
---|---|
In toluene at 70℃; for 2h; Glovebox; | 90% |
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine In tetrahydrofuran at 70℃; for 8h; Inert atmosphere; | 88.9% |
With piperidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 70℃; for 2h; | 80% |
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; palladium diacetate In o-xylene at 120℃; for 3h; Time; | 88.12% |
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; triphenylphosphine In water; toluene at 80 - 110℃; for 15h; Suzuki Coupling; Inert atmosphere; | 88% |
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; toluene at 110℃; for 24h; Suzuki coupling; | 64% |
tetrakis(triethylphosphine)platinum(0)
3-bromoperylene
trans-platinum(triethylphosphine)2(3-perylenyl)(bromo)
Conditions | Yield |
---|---|
In toluene under N2; ligand added to soln. of Pt complex in toluene; stirred for 12h; solvent removed in vac.; washed with pentane; recrystd. from CH2Cl2-MeOH; dried in vac.; elem. anal.; | 87% |
3-bromoperylene
4-(diphenylamino)phenyl boronic acid
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water at 70℃; for 24h; Suzuki-Miyaura Coupling; Inert atmosphere; | 86% |
Conditions | Yield |
---|---|
With piperidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 60℃; for 0.5h; Inert atmosphere; | 82% |
3-bromoperylene
4-methyl-1-naphthylboronic acid
3-(4-methylnaphthalen-1-yl)perylene
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; triphenylphosphine In water; toluene at 80 - 110℃; Suzuki Coupling; Inert atmosphere; | 81% |
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In 1,2-dimethoxyethane; water for 11h; Inert atmosphere; Reflux; | 79% |
(2R,3S,5R)-2-(4,4′-dimethoxytrityloxymethyl)-5-ethynyl-3-hydroxytetrahydrofuran
3-bromoperylene
(2R,3S,5R)-3-hydroxy-2-(4,4'-dimethoxytrityloxymethyl)-5-(3-perylenylethynyl)tetrahydrofuran
Conditions | Yield |
---|---|
With diisopropylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 60℃; Sonogashira coupling reaction; | 78% |
Conditions | Yield |
---|---|
With piperidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 60℃; for 0.5h; Inert atmosphere; | 77% |
Conditions | Yield |
---|---|
Stage #1: 3-bromoperylene With n-butyllithium In tetrahydrofuran; hexane at -80℃; for 1h; Stage #2: C10H20O3 In tetrahydrofuran; hexane at 20℃; | 77% |
3-bromoperylene
Conditions | Yield |
---|---|
Stage #1: 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-fluoronaphthalene; 3-bromoperylene In ethanol; toluene at 95℃; for 0.333333h; Inert atmosphere; Schlenk technique; Stage #2: With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 100℃; for 20h; Suzuki Coupling; Inert atmosphere; Schlenk technique; | 75% |
3-bromoperylene
4,4,5,5-tetramethyl-2-(3-methylnaphthalen-1-yl)-1,3,2-dioxaborolane
3-(3-methylnaphthalen-1-yl)perylene
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; triphenylphosphine In water; toluene at 80 - 110℃; Suzuki Coupling; Inert atmosphere; | 72% |
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene for 8h; Suzuki Coupling; Inert atmosphere; Reflux; | 72% |
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 80℃; for 8h; Inert atmosphere; | 72% |
With palladium diacetate; potassium carbonate; triphenylphosphine In ethanol; water; toluene for 8h; Suzuki-Miyaura Coupling; Inert atmosphere; Reflux; | 47% |
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 90℃; for 8h; Inert atmosphere; |
3-bromoperylene
2-(biphenyl-4-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In 1,4-dioxane; water at 85℃; for 3h; Suzuki Coupling; | 72% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate In toluene at 110℃; Inert atmosphere; | 72% |
3-bromoperylene
4-methoxyphenylphenylperylenylphosphine oxide
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; 1,3-bis-(diphenylphosphino)propane; palladium diacetate In dimethyl sulfoxide at 150℃; | 70% |
Conditions | Yield |
---|---|
With potassium acetate; palladium diacetate In N,N-dimethyl acetamide at 150℃; for 48h; Schlenk technique; Inert atmosphere; | 70% |
Conditions | Yield |
---|---|
Stage #1: 3-bromoperylene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.333333h; Inert atmosphere; Stage #2: dimethylmonochlorosilane In tetrahydrofuran; hexane at -78 - 20℃; for 0.5h; Inert atmosphere; | 69% |
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