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3,9-dibromoPeryleneAppearance:white crystalline powder Storage:Shading, sealed, dry place. Package:aluminous bag Application:API Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport to airport) or by sea L
PERYLENE
3,9-dibromoperylene
Conditions | Yield |
---|---|
With bromine In acetic acid at 50℃; for 5h; | 94% |
With N-Bromosuccinimide In tetrahydrofuran Inert atmosphere; | 91% |
With bromine In tetrachloromethane at 110℃; for 12h; | 63% |
PERYLENE
A
3,10-Dibromoperylene
B
3,9-dibromoperylene
C
3-bromoperylene
Conditions | Yield |
---|---|
With N-Bromosuccinimide In N,N-dimethyl-formamide at 20℃; | A n/a B 90% C n/a |
With N-Bromosuccinimide In dichloromethane at 20℃; for 2h; | A n/a B n/a C 30% |
With N-Bromosuccinimide In dichloromethane at 20℃; for 2h; Yields of byproduct given. Title compound not separated from byproducts; |
Conditions | Yield |
---|---|
With bromine In benzene at 40℃; Inert atmosphere; | A 23% B 29% |
With bromine | |
With bromine In benzene at 35℃; for 1.16667h; Inert atmosphere; Overall yield = 26 %; Overall yield = 2.1 g; |
perylene-3,9-(SO3H)2
3,9-dibromoperylene
Conditions | Yield |
---|---|
With sulfuric acid; bromine; acetic acid |
PERYLENE
benzene
A
3,10-Dibromoperylene
B
3,9-dibromoperylene
Conditions | Yield |
---|---|
bei der Bromierung; |
Conditions | Yield |
---|---|
Bromierung; |
Conditions | Yield |
---|---|
at 90℃; Bromierung; |
PERYLENE
bromine
A
3,10-Dibromoperylene
B
3,9-dibromoperylene
sulfuric acid
perylene-3,9-(SO3H)2
bromine
acetic acid
3,9-dibromoperylene
Conditions | Yield |
---|---|
Stage #1: 3,9-dibromoperylene With n-butyllithium In tetrahydrofuran for 0.25h; Stage #2: Triisopropyl borate In tetrahydrofuran | 100% |
3,9-dibromoperylene
di-p-tolylamine
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate In 1,2-dimethoxyethane; toluene at 110℃; Buchwald-Hartwig Coupling; Inert atmosphere; | 83% |
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; potassium tert-butylate; palladium diacetate In toluene at 88℃; for 14h; | 82% |
3,9-dibromoperylene
bis(4-methoxyphenyl)amine
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate In 1,2-dimethoxyethane; toluene at 110℃; Buchwald-Hartwig Coupling; Inert atmosphere; | 81% |
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In water; toluene at 70℃; for 11h; Inert atmosphere; | 80.56% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate In 1,2-dimethoxyethane; toluene at 110℃; Buchwald-Hartwig Coupling; Inert atmosphere; | 79% |
3,9-dibromoperylene
trimethylsilylacetylene
Conditions | Yield |
---|---|
With piperidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 60 - 70℃; for 2h; Sonogashira Cross-Coupling; | 78% |
3,9-dibromoperylene
bis-(4-fluoro-phenyl)-amine
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate In 1,2-dimethoxyethane; toluene at 110℃; Buchwald-Hartwig Coupling; Inert atmosphere; | 78% |
Conditions | Yield |
---|---|
With potassium carbonate; triphenylphosphine; palladium dichloride In ethanol; water; toluene for 4h; Inert atmosphere; Reflux; | 75.26% |
Conditions | Yield |
---|---|
With potassium carbonate; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran; water for 12h; Heating / reflux; | 75% |
Conditions | Yield |
---|---|
With piperidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 60 - 70℃; for 2h; Sonogashira Cross-Coupling; | 70% |
3,10-Dibromoperylene
3,9-dibromoperylene
2,7-dibromo-9,9-dioctylfluorene
poly-2,7-(9,9-dioctylfluorene)-co-(perylene), Mn = 47930 g/mol, D = 4.1; monomer(s): 3,9-dibromoperylene 1,5 mol%; 3,10-dibromoperylene, 1.5 mol%; 2,7-dibromo-9,9-dioctylfluorene
Conditions | Yield |
---|---|
Stage #1: 3,10-Dibromoperylene; 3,9-dibromoperylene; 2,7-dibromo-9,9-dioctylfluorene With [2,2]bipyridinyl; cyclooctadiene; bis(1,5-cyclooctadiene)nickel (0) In N,N-dimethyl-formamide; toluene at 85℃; for 24h; Yamamoto polymerization; Stage #2: With bromobenzene In N,N-dimethyl-formamide; toluene Further stages.; | 69% |
3,10-Dibromoperylene
3,9-dibromoperylene
2,7-dibromo-9,9-dioctylfluorene
N,N'-bis(4'-bromophenyl)-1,6,7,12-tetra[4-(1,1,3,3-tetramethylbutyl)phenoxy]perylene-3,4,9,10-tetracarboxdiimide
poly-2,7-(9,9-dioctylfluorene)-co-(perylene)-co-[1,6,7,12-tetra(4-tert-octyl)-phenoxy-bis-N,N'-bisphenylperylene-3,4,9,10-dicarboximide], Mn = 46650, D = 7.7; monomer(s): 3,9-dibromoperylene 1,5 mol%; 3,10-dibromoperylene, 1.5 mol%;
Conditions | Yield |
---|---|
Stage #1: 3,10-Dibromoperylene; 3,9-dibromoperylene; 2,7-dibromo-9,9-dioctylfluorene; N,N'-bis(4'-bromophenyl)-1,6,7,12-tetra[4-(1,1,3,3-tetramethylbutyl)phenoxy]perylene-3,4,9,10-tetracarboxdiimide With [2,2]bipyridinyl; bis(1,5-cyclooctadiene)nickel (0); 1,5-cis,cis-cyclooctadiene In N,N-dimethyl-formamide; toluene at 85℃; for 24h; Yamamoto polymerization; Stage #2: With bromobenzene In N,N-dimethyl-formamide; toluene Further stages.; | 67% |
3,9-dibromoperylene
4,4’-dicyanodipehnylamine
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate In 1,2-dimethoxyethane; toluene at 110℃; Buchwald-Hartwig Coupling; Inert atmosphere; | 60% |
3,9-dibromoperylene
4-methoxyphenylboronic acid
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In water; toluene at 100℃; for 8h; Suzuki-Miyaura Coupling; | 57% |
Conditions | Yield |
---|---|
Stage #1: 3,10-Dibromoperylene; 3,9-dibromoperylene; C63H92BNO4 With tetrakis(triphenylphosphine) palladium(0); water; potassium carbonate In ethanol; toluene at 90℃; for 4h; Suzuki Coupling; Inert atmosphere; Stage #2: With iron(III) chloride In nitromethane; dichloromethane at 20℃; for 2h; | 55% |
3,9-dibromoperylene
bis(pinacol)diborane
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); potassium acetate; XPhos In 1,4 dimethylcyclohexane for 12h; Reflux; | 50.83% |
With tris-(dibenzylideneacetone)dipalladium(0); potassium acetate; XPhos In 1,4-dioxane for 12h; Reflux; | 50.83% |
Conditions | Yield |
---|---|
Stage #1: allyl alcohol With 9-bora-bicyclo[3.3.1]nonane In tetrahydrofuran for 18h; Suzuki Coupling; Inert atmosphere; Cooling; Reflux; Stage #2: 3,9-dibromoperylene With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate Suzuki Coupling; Inert atmosphere; Reflux; | 41% |
Conditions | Yield |
---|---|
With piperidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 60 - 70℃; for 6h; Sonogashira Cross-Coupling; | 38% |
5-Hexen-1-ol
3,9-dibromoperylene
Conditions | Yield |
---|---|
Stage #1: 5-Hexen-1-ol With 9-bora-bicyclo[3.3.1]nonane In tetrahydrofuran for 18h; Suzuki Coupling; Inert atmosphere; Cooling; Reflux; Stage #2: 3,9-dibromoperylene With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate Suzuki Coupling; Inert atmosphere; Reflux; | 30% |
3,9-dibromoperylene
1,2-bis(4-butylphenyl)ethyne
A
1,2,7,8-tetrakis(4-n-butylphenyl)dicyclopenta[cd,lm]perylene
B
1,2,8,9,10,11-hexakis(4-n-butylphenyl)benzo[b]cyclopenta[lm]perylene
Conditions | Yield |
---|---|
With triethylamine; tris-(o-tolyl)phosphine; bis(dibenzylideneacetone)-palladium(0) In toluene; acetonitrile at 111℃; for 16h; Inert atmosphere; | A 18% B n/a |
3,9-dibromoperylene
diphenyl acetylene
A
7-(1,2-diphenylvinyl)-1,2-diphenylcyclopenta[cd]perylene
B
1,2,7,8-tetraphenylbiscyclopenta[cd,lm]perylene
Conditions | Yield |
---|---|
With triethylamine; tris-(o-tolyl)phosphine; bis(dibenzylideneacetone)-palladium(0) In toluene; acetonitrile at 111℃; for 16h; Inert atmosphere; | A n/a B 17% |
3,9-dibromoperylene
perylene-3,9-dione
3,9-dibromoperylene
3,9-dibromo-4,10-dinitro-perylene
Conditions | Yield |
---|---|
With sulfuric acid; acetic acid; potassium nitrate |
Conditions | Yield |
---|---|
With aluminium trichloride at 150 - 170℃; |
3,9-dibromoperylene
benzoyl chloride
3,9-dibenzoyl-4,10-dibromo-perylene
Conditions | Yield |
---|---|
With carbon disulfide; aluminium trichloride |
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