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Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

High Quality 99% 56752-35-3 3,9-Dibromoperylene Manufacturer

Cas:56752-35-3

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Perylene, 3,9-dibromo- 56752-35-3

Cas:56752-35-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

3,9-Dibromoperylene CAS:56752-35-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic inter

3,9-Dibromoperylene CAS:56752-35-3

Cas:56752-35-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Perylene, 3,9-dibromo-

Cas:56752-35-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Perylene, 3,9-dibromo-

Cas:56752-35-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

3,9-dibromoPerylene

Cas:56752-35-3

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Triumph International Development Limilted

Appearance:off-white to white solid Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for Synthesis API and Research Transportation:By Sea/Air/Courier Port:Qingdao

3,9-dibromoperylene 56752-35-3

Cas:56752-35-3

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

3,9-Dibromoperylene

Cas:56752-35-3

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

3,9-dibromoPerylene

Cas:56752-35-3

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

3,9-dibromoPerylene

Cas:56752-35-3

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

3,9-dibromoPerylene

Cas:56752-35-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

3,9-dibromoPerylene

Cas:56752-35-3

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

SAGECHEM LIMITED

SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in

SAGECHEM/ 3,9-Dibromoperylene /Manufacturer in China

Cas:56752-35-3

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

3,9-Dibromoperylene

Cas:56752-35-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

3,9-dibromoPerylene

Cas:56752-35-3

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

Hebei Mojin Biotechnology Co.,Ltd

1, High quality with competitive price:2, Fast and safe delivery3.Excellent pre-sales and after-sales service4. Well-trained and professional technologist and sales with rich experience in the field for 5-10 yearsAppearance:see detailed specification

3,9-dibromoperylene

Cas:56752-35-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

3,9-dibromoPerylene

Cas:56752-35-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates

3,9-dibromoperylene

Cas:56752-35-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Wuxi TAA Chemical Industry Co.,LTD.

1.A strong technical force and advanced processing equipments. The quality of the products has been strictly inspected and all kinds of index have reached or exceeded domestic and international standards.2. Now we have established long-term stable re

Perylene, 3,9-dibromo-

Cas:56752-35-3

Min.Order:0

Negotiable

Type:Other

inquiry

Henan Tianfu Chemical Co., Ltd.

1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.

Perylene, 3,9-dibromo-

Cas:56752-35-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Xian Changyue Biological Technology Co., Ltd.

best seller Application:API

3,9-Dibromoperylene

Cas:56752-35-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

Perylene, 3,9-dibromo-

Cas:56752-35-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hubei Langyou International Trading Co., Ltd

3,9-dibromoPerylene Application:3,9-dibromoPerylene

3,9-dibromoPerylene

Cas:56752-35-3

Min.Order:0

Negotiable

Type:Other

inquiry

DB BIOTECH CO., LTD

best seller Application:API

3,9-Dibromoperylene

Cas:56752-35-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Wuhan ZeShanCheng Biomedical Technology Co., Ltd.

1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highl

Perylene, 3,9-dibromo-

Cas:56752-35-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

3,9-Dibromoperylene

Cas:56752-35-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou ZeErRui Chemical Co., Ltd.

Hangzhou ZeErRui Chemical Co., Ltd. is focused on customization, research and development and production of APIs and advanced intermediates, which can effectively compensate for the deficiencies of traditional CRO and CMO. Priority of high-tech barri

3,9-dibromoPerylene

Cas:56752-35-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Newgreat Chemical Co., Ltd

Wuhan Xinweiye Chemical Co., Ltd. is mainly engaged in the process development and production of customized synthesis and pharmaceutical intermediates. We have professional researchers in organic synthesis, analytical chemistry and production process

3,9-dibromoPerylene

Cas:56752-35-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers2. Produce products of different specifications and sizes according to your requirements.3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures sta

3,9-Dibromoperylene

Cas:56752-35-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hunan Longxianng Runhui Trading Co.,Ltd

3,9-dibromoPeryleneAppearance:white crystalline powder Storage:Shading, sealed, dry place. Package:aluminous bag Application:API Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport to airport) or by sea L

3,9-dibromoPerylene

Cas:56752-35-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

PERYLENE
198-55-0

PERYLENE

3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

Conditions
ConditionsYield
With bromine In acetic acid at 50℃; for 5h;94%
With N-Bromosuccinimide In tetrahydrofuran Inert atmosphere;91%
With bromine In tetrachloromethane at 110℃; for 12h;63%
PERYLENE
198-55-0

PERYLENE

A

3,10-Dibromoperylene
85514-20-1

3,10-Dibromoperylene

B

3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

C

3-bromoperylene
23683-68-3

3-bromoperylene

Conditions
ConditionsYield
With N-Bromosuccinimide In N,N-dimethyl-formamide at 20℃;A n/a
B 90%
C n/a
With N-Bromosuccinimide In dichloromethane at 20℃; for 2h;A n/a
B n/a
C 30%
With N-Bromosuccinimide In dichloromethane at 20℃; for 2h; Yields of byproduct given. Title compound not separated from byproducts;
PERYLENE
198-55-0

PERYLENE

A

3,10-Dibromoperylene
85514-20-1

3,10-Dibromoperylene

B

3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

Conditions
ConditionsYield
With bromine In benzene at 40℃; Inert atmosphere;A 23%
B 29%
With bromine
With bromine In benzene at 35℃; for 1.16667h; Inert atmosphere; Overall yield = 26 %; Overall yield = 2.1 g;
perylene-3,9-(SO3H)2
71506-23-5

perylene-3,9-(SO3H)2

3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

Conditions
ConditionsYield
With sulfuric acid; bromine; acetic acid
PERYLENE
198-55-0

PERYLENE

benzene
71-43-2

benzene

A

3,10-Dibromoperylene
85514-20-1

3,10-Dibromoperylene

B

3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

C

3,4,9-tribromo-perylene

3,4,9-tribromo-perylene

Conditions
ConditionsYield
bei der Bromierung;
PERYLENE
198-55-0

PERYLENE

aluminium bromide
7727-15-3

aluminium bromide

nitrobenzene
98-95-3

nitrobenzene

3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

Conditions
ConditionsYield
Bromierung;
PERYLENE
198-55-0

PERYLENE

dihydrogen peroxide
7722-84-1

dihydrogen peroxide

acetic acid
64-19-7

acetic acid

sodium bromide

sodium bromide

3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

Conditions
ConditionsYield
at 90℃; Bromierung;
PERYLENE
198-55-0

PERYLENE

bromine
7726-95-6

bromine

A

3,10-Dibromoperylene
85514-20-1

3,10-Dibromoperylene

B

3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

sulfuric acid
7664-93-9

sulfuric acid

perylene-3,9-(SO3H)2
71506-23-5

perylene-3,9-(SO3H)2

bromine
7726-95-6

bromine

acetic acid
64-19-7

acetic acid

3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

Triisopropyl borate
5419-55-6

Triisopropyl borate

3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

perylene-3,9-diboronic acid

perylene-3,9-diboronic acid

Conditions
ConditionsYield
Stage #1: 3,9-dibromoperylene With n-butyllithium In tetrahydrofuran for 0.25h;
Stage #2: Triisopropyl borate In tetrahydrofuran
100%
3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

di-p-tolylamine
620-93-9

di-p-tolylamine

3,9-bis(N,N-bis(4-methylphenyl)amino)perylene

3,9-bis(N,N-bis(4-methylphenyl)amino)perylene

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate In 1,2-dimethoxyethane; toluene at 110℃; Buchwald-Hartwig Coupling; Inert atmosphere;83%
3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

C24H13NO2

C24H13NO2

C68H34N2O4

C68H34N2O4

Conditions
ConditionsYield
With tri-tert-butyl phosphine; potassium tert-butylate; palladium diacetate In toluene at 88℃; for 14h;82%
3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

bis(4-methoxyphenyl)amine
101-70-2

bis(4-methoxyphenyl)amine

3,9-bis(N,N-bis(4-methoxyphenyl)amino)perylene

3,9-bis(N,N-bis(4-methoxyphenyl)amino)perylene

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate In 1,2-dimethoxyethane; toluene at 110℃; Buchwald-Hartwig Coupling; Inert atmosphere;81%
3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

phenylboronic acid
98-80-6

phenylboronic acid

C26H15Br

C26H15Br

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In water; toluene at 70℃; for 11h; Inert atmosphere;80.56%
3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

diphenylamine
122-39-4

diphenylamine

3,9-bis(N,N-diphenylamino)perylene

3,9-bis(N,N-diphenylamino)perylene

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate In 1,2-dimethoxyethane; toluene at 110℃; Buchwald-Hartwig Coupling; Inert atmosphere;79%
3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

trimethylsilylacetylene
1066-54-2

trimethylsilylacetylene

3,9-bis(trimethylsilylethynyl)perylene

3,9-bis(trimethylsilylethynyl)perylene

Conditions
ConditionsYield
With piperidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 60 - 70℃; for 2h; Sonogashira Cross-Coupling;78%
3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

bis-(4-fluoro-phenyl)-amine
330-91-6

bis-(4-fluoro-phenyl)-amine

3,9-bis(N,N-bis(4-fluorophenyl)amino)perylene

3,9-bis(N,N-bis(4-fluorophenyl)amino)perylene

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate In 1,2-dimethoxyethane; toluene at 110℃; Buchwald-Hartwig Coupling; Inert atmosphere;78%
3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

(6-phenylpyridin-3-yl)boronic acid
155079-10-0

(6-phenylpyridin-3-yl)boronic acid

C42H26N2
1257879-55-2

C42H26N2

Conditions
ConditionsYield
With potassium carbonate; triphenylphosphine; palladium dichloride In ethanol; water; toluene for 4h; Inert atmosphere; Reflux;75.26%
3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

4-Chlorophenylboronic acid
1679-18-1

4-Chlorophenylboronic acid

C32H18Cl2
951039-41-1

C32H18Cl2

Conditions
ConditionsYield
With potassium carbonate; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran; water for 12h; Heating / reflux;75%
3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

4-tert-Butylphenylacetylene
772-38-3

4-tert-Butylphenylacetylene

C44H36

C44H36

Conditions
ConditionsYield
With piperidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 60 - 70℃; for 2h; Sonogashira Cross-Coupling;70%
3,10-Dibromoperylene
85514-20-1

3,10-Dibromoperylene

3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

2,7-dibromo-9,9-dioctylfluorene
198964-46-4

2,7-dibromo-9,9-dioctylfluorene

poly-2,7-(9,9-dioctylfluorene)-co-(perylene), Mn = 47930 g/mol, D = 4.1; monomer(s): 3,9-dibromoperylene 1,5 mol%; 3,10-dibromoperylene, 1.5 mol%; 2,7-dibromo-9,9-dioctylfluorene

poly-2,7-(9,9-dioctylfluorene)-co-(perylene), Mn = 47930 g/mol, D = 4.1; monomer(s): 3,9-dibromoperylene 1,5 mol%; 3,10-dibromoperylene, 1.5 mol%; 2,7-dibromo-9,9-dioctylfluorene

Conditions
ConditionsYield
Stage #1: 3,10-Dibromoperylene; 3,9-dibromoperylene; 2,7-dibromo-9,9-dioctylfluorene With [2,2]bipyridinyl; cyclooctadiene; bis(1,5-cyclooctadiene)nickel (0) In N,N-dimethyl-formamide; toluene at 85℃; for 24h; Yamamoto polymerization;
Stage #2: With bromobenzene In N,N-dimethyl-formamide; toluene Further stages.;
69%
3,10-Dibromoperylene
85514-20-1

3,10-Dibromoperylene

3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

2,7-dibromo-9,9-dioctylfluorene
198964-46-4

2,7-dibromo-9,9-dioctylfluorene

N,N'-bis(4'-bromophenyl)-1,6,7,12-tetra[4-(1,1,3,3-tetramethylbutyl)phenoxy]perylene-3,4,9,10-tetracarboxdiimide
344454-74-6

N,N'-bis(4'-bromophenyl)-1,6,7,12-tetra[4-(1,1,3,3-tetramethylbutyl)phenoxy]perylene-3,4,9,10-tetracarboxdiimide

poly-2,7-(9,9-dioctylfluorene)-co-(perylene)-co-[1,6,7,12-tetra(4-tert-octyl)-phenoxy-bis-N,N'-bisphenylperylene-3,4,9,10-dicarboximide], Mn = 46650, D = 7.7; monomer(s): 3,9-dibromoperylene 1,5 mol%; 3,10-dibromoperylene, 1.5 mol%;

poly-2,7-(9,9-dioctylfluorene)-co-(perylene)-co-[1,6,7,12-tetra(4-tert-octyl)-phenoxy-bis-N,N'-bisphenylperylene-3,4,9,10-dicarboximide], Mn = 46650, D = 7.7; monomer(s): 3,9-dibromoperylene 1,5 mol%; 3,10-dibromoperylene, 1.5 mol%;

Conditions
ConditionsYield
Stage #1: 3,10-Dibromoperylene; 3,9-dibromoperylene; 2,7-dibromo-9,9-dioctylfluorene; N,N'-bis(4'-bromophenyl)-1,6,7,12-tetra[4-(1,1,3,3-tetramethylbutyl)phenoxy]perylene-3,4,9,10-tetracarboxdiimide With [2,2]bipyridinyl; bis(1,5-cyclooctadiene)nickel (0); 1,5-cis,cis-cyclooctadiene In N,N-dimethyl-formamide; toluene at 85℃; for 24h; Yamamoto polymerization;
Stage #2: With bromobenzene In N,N-dimethyl-formamide; toluene Further stages.;
67%
3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

4,4’-dicyanodipehnylamine
36602-05-8

4,4’-dicyanodipehnylamine

3,9-bis(N,N-bis(4-cyanophenyl)amino)perylene

3,9-bis(N,N-bis(4-cyanophenyl)amino)perylene

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate In 1,2-dimethoxyethane; toluene at 110℃; Buchwald-Hartwig Coupling; Inert atmosphere;60%
3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

4-methoxyphenylboronic acid
5720-07-0

4-methoxyphenylboronic acid

3,9-bis(4-methoxyphenyl)perylene

3,9-bis(4-methoxyphenyl)perylene

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In water; toluene at 100℃; for 8h; Suzuki-Miyaura Coupling;57%
3,10-Dibromoperylene
85514-20-1

3,10-Dibromoperylene

3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

C63H92BNO4

C63H92BNO4

C77H88BrNO2

C77H88BrNO2

Conditions
ConditionsYield
Stage #1: 3,10-Dibromoperylene; 3,9-dibromoperylene; C63H92BNO4 With tetrakis(triphenylphosphine) palladium(0); water; potassium carbonate In ethanol; toluene at 90℃; for 4h; Suzuki Coupling; Inert atmosphere;
Stage #2: With iron(III) chloride In nitromethane; dichloromethane at 20℃; for 2h;
55%
3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

bis(pinacol)diborane
73183-34-3

bis(pinacol)diborane

3,9-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)perylene

3,9-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)perylene

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); potassium acetate; XPhos In 1,4 dimethylcyclohexane for 12h; Reflux;50.83%
With tris-(dibenzylideneacetone)dipalladium(0); potassium acetate; XPhos In 1,4-dioxane for 12h; Reflux;50.83%
3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

allyl alcohol
107-18-6

allyl alcohol

C26H24O2

C26H24O2

Conditions
ConditionsYield
Stage #1: allyl alcohol With 9-bora-bicyclo[3.3.1]nonane In tetrahydrofuran for 18h; Suzuki Coupling; Inert atmosphere; Cooling; Reflux;
Stage #2: 3,9-dibromoperylene With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate Suzuki Coupling; Inert atmosphere; Reflux;
41%
3,6,9,12-tetraoxapentadec-14-yn-1-amine
1013921-36-2

3,6,9,12-tetraoxapentadec-14-yn-1-amine

3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

C42H50N2O8

C42H50N2O8

Conditions
ConditionsYield
With piperidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 60 - 70℃; for 6h; Sonogashira Cross-Coupling;38%
5-Hexen-1-ol
821-41-0

5-Hexen-1-ol

3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

6-[9-(6-Hydroxy-hexyl)-perylen-3-yl]-hexan-1-ol

6-[9-(6-Hydroxy-hexyl)-perylen-3-yl]-hexan-1-ol

Conditions
ConditionsYield
Stage #1: 5-Hexen-1-ol With 9-bora-bicyclo[3.3.1]nonane In tetrahydrofuran for 18h; Suzuki Coupling; Inert atmosphere; Cooling; Reflux;
Stage #2: 3,9-dibromoperylene With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate Suzuki Coupling; Inert atmosphere; Reflux;
30%
3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

1,2-bis(4-butylphenyl)ethyne
80221-11-0

1,2-bis(4-butylphenyl)ethyne

A

1,2,7,8-tetrakis(4-n-butylphenyl)dicyclopenta[cd,lm]perylene
1361026-35-8

1,2,7,8-tetrakis(4-n-butylphenyl)dicyclopenta[cd,lm]perylene

B

1,2,8,9,10,11-hexakis(4-n-butylphenyl)benzo[b]cyclopenta[lm]perylene
1361026-36-9

1,2,8,9,10,11-hexakis(4-n-butylphenyl)benzo[b]cyclopenta[lm]perylene

Conditions
ConditionsYield
With triethylamine; tris-(o-tolyl)phosphine; bis(dibenzylideneacetone)-palladium(0) In toluene; acetonitrile at 111℃; for 16h; Inert atmosphere;A 18%
B n/a
3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

diphenyl acetylene
501-65-5

diphenyl acetylene

A

7-(1,2-diphenylvinyl)-1,2-diphenylcyclopenta[cd]perylene
1361026-34-7

7-(1,2-diphenylvinyl)-1,2-diphenylcyclopenta[cd]perylene

B

1,2,7,8-tetraphenylbiscyclopenta[cd,lm]perylene
1361026-33-6

1,2,7,8-tetraphenylbiscyclopenta[cd,lm]perylene

Conditions
ConditionsYield
With triethylamine; tris-(o-tolyl)phosphine; bis(dibenzylideneacetone)-palladium(0) In toluene; acetonitrile at 111℃; for 16h; Inert atmosphere;A n/a
B 17%
3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

perylene-3,9-dione
5796-92-9

perylene-3,9-dione

3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

3,9-dibromo-4,10-dinitro-perylene
858857-30-4

3,9-dibromo-4,10-dinitro-perylene

Conditions
ConditionsYield
With sulfuric acid; acetic acid; potassium nitrate
3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

benzoyl chloride
98-88-4

benzoyl chloride

isoviolanthrone
128-64-3

isoviolanthrone

Conditions
ConditionsYield
With aluminium trichloride at 150 - 170℃;
3,9-dibromoperylene
56752-35-3

3,9-dibromoperylene

benzoyl chloride
98-88-4

benzoyl chloride

3,9-dibenzoyl-4,10-dibromo-perylene
856340-89-1

3,9-dibenzoyl-4,10-dibromo-perylene

Conditions
ConditionsYield
With carbon disulfide; aluminium trichloride

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