Factory supply cis-4-Methylcyclohexylamine CAS 2523-56-0 with fast delivery Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Foo
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inquiryCyclohexanamine,4-methyl-, cis- Application:Cyclohexanamine,4-methyl-, cis-
We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white crystals powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as
Supply top quality products with a reasonable price Application:api
Cyclohexanamine,4-methyl-, cis-Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:pharmaceutical intermediate Transportation:by air, by sea, by express
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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inquiry2523-56-0 Application:intermediate
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Min.Order:0
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Type:Lab/Research institutions
inquiryR & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
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inquirycis-4-methylcyclohexanamine
Conditions | Yield |
---|---|
With aminosulfonic acid; sodium hydroxide In acetonitrile at 20 - 25℃; for 16h; Inert atmosphere; | 90% |
cis-4-methylcyclohexanamine
Conditions | Yield |
---|---|
With aminosulfonic acid; potassium hydroxide In acetonitrile at 20 - 25℃; for 16h; Inert atmosphere; | 86.5% |
cis-4-methylcyclohexanamine
Conditions | Yield |
---|---|
With aminosulfonic acid; sodium hydroxide In tetrahydrofuran at 20 - 25℃; for 16h; Inert atmosphere; Large scale; | 85% |
cis-4-methylcyclohexanamine
Conditions | Yield |
---|---|
With aminosulfonic acid; lithium hydroxide In tetrahydrofuran at 20 - 25℃; for 16h; Inert atmosphere; | 81% |
p-toluidine
A
trans-4-methylcyclohexanamine
B
cis-4-methylcyclohexanamine
C
4,4'-dimethyldicyclohexylamine
Conditions | Yield |
---|---|
With hydrogen In tetrahydrofuran at 110℃; under 75007.5 Torr; for 3h; Kinetics; Reagent/catalyst; Temperature; Autoclave; | A 63.6% B 30.2% C n/a |
p-toluidine
A
trans-4-methylcyclohexanamine
B
cis-4-methylcyclohexanamine
Conditions | Yield |
---|---|
With hydrogenchloride; hydrogen; acetic acid; platinum at 25℃; under 2280 Torr; | |
With hydrogen; silica gel; rhodium In 2,2,4-trimethylpentane at 49.85℃; Product distribution; Further Variations:; Catalysts; | |
With hydrogen In 1,4-dioxane at 100℃; under 15001.5 Torr; for 3.33333h; Autoclave; | A n/a B n/a |
formamide
1-methylcyclohexan-4-one
A
trans-4-methylcyclohexanamine
B
cis-4-methylcyclohexanamine
Conditions | Yield |
---|---|
With formic acid anschliessendes Erhitzen mit wss.HCl; |
Conditions | Yield |
---|---|
With hydrogenchloride; acetic acid; platinum at 70 - 80℃; under 2280 Torr; anschliessend man verseift durch Erhitzen mit konz. Salzsaeure auf 130-140grad; |
trans-4-methylcyclohexyl p-toluenesulfonate
cis-4-methylcyclohexanamine
Conditions | Yield |
---|---|
(i) NaN3, (ii) H2, Pd-C, EtOH; Multistep reaction; | |
With ammonia | |
(i) NaN3, (ii) LiAlH4; Multistep reaction; |
1-methylcyclohexan-4-one
A
trans-4-methylcyclohexanamine
B
cis-4-methylcyclohexanamine
Conditions | Yield |
---|---|
Yield given. Multistep reaction. Yields of byproduct given; | |
With decane; (S)-1-phenyl-ethylamine; Chromobacterium violaceum amine transaminase A W60 C In tert-butyl methyl ether at 37℃; pH=8.2; Enzymatic reaction; stereoselective reaction; | A n/a B n/a |
With decane; (S)-1-phenyl-ethylamine; Vibrio fluvialis amine transaminase A In tert-butyl methyl ether at 37℃; pH=8.2; Catalytic behavior; Reagent/catalyst; Solvent; Enzymatic reaction; stereoselective reaction; | A n/a B n/a |
4-methylcyclohexanone oxime
cis-4-methylcyclohexanamine
Conditions | Yield |
---|---|
With hydrogen; platinum |
cis-4-methylcyclohexanamine
Conditions | Yield |
---|---|
With sodium amalgam; ethanol; acetic acid |
ethanol
4-methylcyclohexanone oxime
acetic acid
cis-4-methylcyclohexanamine
Conditions | Yield |
---|---|
With hydrogen; silica gel; rhodium In 2,2,4-trimethylpentane at 49.85℃; Activation energy; Further Variations:; Catalysts; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Py 2: liq. NH3 View Scheme |
cis-4-methylcyclohexylamine hydrochloride
cis-4-methylcyclohexanamine
Conditions | Yield |
---|---|
Stage #1: cis-4-methylcyclohexylamine hydrochloride With sodium hydrogencarbonate In water Stage #2: With hydrogenchloride In water at 20℃; Stage #3: With ammonia In methanol | 1.78 g |
1-methyl-4-nitrobenzene
A
trans-4-methylcyclohexanamine
B
cis-4-methylcyclohexanamine
Conditions | Yield |
---|---|
With hydrogen In tetrahydrofuran at 110℃; under 75007.5 Torr; for 3h; Kinetics; Autoclave; diastereoselective reaction; | A n/a B n/a |
Conditions | Yield |
---|---|
With methanol; 5% Rh/C; ammonia; hydrogen; isopropyl alcohol In Hexadecane at 140℃; under 12001.2 Torr; for 16h; Autoclave; | A n/a B n/a |
With alumina-supported nickel; ammonia; hydrogen In toluene at 160℃; for 6h; Time; High pressure; Overall yield = 96 percentChromat.; | A n/a B n/a |
2-(4-methylphenyl)-benzo-1,3-dioxa-2-borole
cis-4-methylcyclohexanamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: rhodium contaminated with carbon; hydrogen / ethyl acetate / 12 h / 70 °C / 11251.1 Torr 2: aminosulfonic acid; potassium hydroxide / acetonitrile / 16 h / 20 - 25 °C / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: rhodium contaminated with carbon; hydrogen / 80 °C / Autoclave; Large scale 2: aminosulfonic acid; sodium hydroxide / tetrahydrofuran / 16 h / 20 - 25 °C / Inert atmosphere; Large scale View Scheme |
p-tolylboronic pinacol ester
cis-4-methylcyclohexanamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: rhodium contaminated with carbon; hydrogen / ethyl acetate / 8 h / 60 °C / 15001.5 Torr 2: aminosulfonic acid; sodium hydroxide / acetonitrile / 16 h / 20 - 25 °C / Inert atmosphere View Scheme |
phthalic anhydride
cis-4-methylcyclohexanamine
cis-1-Methyl-4-phthalimidocyclohexan
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 150℃; | 80% |
cis-4-methylcyclohexanamine
benzoic acid
cis-4-benzamino-1-methyl-cyclohexane
Conditions | Yield |
---|---|
Stage #1: benzoic acid With N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In dichloromethane at 0℃; for 0.166667h; Stage #2: cis-4-methylcyclohexanamine With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; for 5h; | 80% |
cis-4-methylcyclohexanamine
3-chloroisoquinoline-7-carbaldehyde
3-((cis-4-methylcyclohexyl)amino)isoquinoline-7-carbaldehyde
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate; XPhos In N,N-dimethyl-formamide at 90℃; for 6h; Inert atmosphere; | 51% |
4,6-dichloro-1H-indole-2-carboxylic acid
cis-4-methylcyclohexanamine
4,6-dichloro-N-(cis-4-methylcyclohexyl)-1H-indole-2-carboxamide
Conditions | Yield |
---|---|
Stage #1: 4,6-dichloro-1H-indole-2-carboxylic acid With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; for 0.166667h; Stage #2: cis-4-methylcyclohexanamine In N,N-dimethyl-formamide at 20℃; for 16h; | 50% |
formaldehyd
formic acid
cis-4-methylcyclohexanamine
dimethyl-(cis-4-methyl-cyclohexyl)-amine
Conditions | Yield |
---|---|
With water |
Conditions | Yield |
---|---|
In 1,4-dioxane Heating; |
cis-4-methylcyclohexanamine
benzoyl chloride
cis-4-benzamino-1-methyl-cyclohexane
Conditions | Yield |
---|---|
With sodium hydroxide |
formaldehyd
cis-4-methylcyclohexanamine
dimethyl-(cis-4-methyl-cyclohexyl)-amine
Conditions | Yield |
---|---|
With formic acid |
Conditions | Yield |
---|---|
(i) ClCO2Et, Et3N, DMF, (ii) /BRN= 2203109/; Multistep reaction; |
cis-4-methylcyclohexanamine
cis-N-(4-Methylcyclohexyl)-3,3-diphenylpropylamin
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: (i) ClCO2Et, Et3N, DMF, (ii) /BRN= 2203109/ 2: LiAlH4 / tetrahydrofuran View Scheme |
cis-4-methylcyclohexanamine
3-chloroisoquinoline-7-carbaldehyde
4-chloro-3-((cis-4-methylcyclohexyl)amino)isoquinoline-7-carbaldehyde
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate; XPhos / N,N-dimethyl-formamide / 6 h / 90 °C / Inert atmosphere 2: N-chloro-succinimide; trifluoroacetic acid / acetonitrile / 16 h / 20 °C View Scheme |
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