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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

1-Phenazinecarboxylic acid

Cas:2538-68-3

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

1-Phenazinecarboxylic acid

Cas:2538-68-3

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufactu

PHENAZINE-1-CARBOXYLIC ACID CAS 2538-68-3

Cas:2538-68-3

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Wholesale price CAS 2538-68-3 with best price

Cas:2538-68-3

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Factory Supply High Quality CAS ?2538-68-3 ,1-Phenazinecarboxylic Acid

Cas:2538-68-3

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

1-Phenazinecarboxylic acid

Cas:2538-68-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

1-Phenazinecarboxylic acid

Cas:2538-68-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

1-Phenazinecarboxylic acid

Cas:2538-68-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

1-Phenazinecarboxylic Acid

Cas:2538-68-3

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

1-Phenazinecarboxylic Acid

Cas:2538-68-3

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

superior quality moderate price & quick delivery Appearance:Brown Solid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Tubermycin B (1-phe

1-Phenazinecarboxylic acid

Cas:2538-68-3

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Henan Tianfu Chemical Co., Ltd.

PHENAZINE-1-CARBOXYLIC ACID Basic information Product Name: PHENAZINE-1-CARBOXYLIC ACID Synonyms: PHENAZINE-1-CARBOXYLIC ACID;1-carboxylicacidphe

2538-68-3 C13H8N2O2 PHENAZINE-1-CARBOXYLIC ACID

Cas:2538-68-3

Min.Order:1 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Jiangsu Qianyu Molecular Technology Co., LTD.

Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

In Bulk SupplyPHENAZINE-1-CARBOXYLIC ACID

Cas:2538-68-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

1-Phenazinecarboxylic Acid

Cas:2538-68-3

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Hangzhou Huarong Pharm Co., Ltd.

We Huarong Pharm can provide Customized Synthesis & Process R&D & APIs and intermediates Production & Quality Research & Registration Application, especially our GMP validation service which complies with SFDA, FDA, WHO and EU EMPA. O

PHENAZINE-1-CARBOXYLIC ACID

Cas:2538-68-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

1-Phenazinecarboxylic Acid

Cas:2538-68-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

1-Phenazinecarboxylic Acid

Cas:2538-68-3

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Golden Pharma Co., Limited

GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation

PHENAZINE-1-CARBOXYLIC ACID

Cas:2538-68-3

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

1-Phenazinecarboxylic Acid

Cas:2538-68-3

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

Hebei Mojin Biotechnology Co.,Ltd

1, High quality with competitive price:2, Fast and safe delivery3.Excellent pre-sales and after-sales service4. Well-trained and professional technologist and sales with rich experience in the field for 5-10 yearsAppearance:see detailed specification

1-Phenazinecarboxylic acid

Cas:2538-68-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Suzhou Sibian Chemical Technology Co., Ltd

The process is mature and can be mass produced to 100 kg, with good quality and purity up to 99%.The product has a large stock and can be supplied stably. Package:bottle Application:Drug R&D Transportation:Sealed drying(25℃) Port:ShangHai

PHENAZINE-1-CARBOXYLIC ACID

Cas:2538-68-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

1-Phenazinecarboxylic Acid

Cas:2538-68-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Acmec Biochemical Technology Co., Ltd.

Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea

Acmec Phenazine-1-carboxylic acid 25mg

Cas:2538-68-3

Min.Order:1 bottle

Negotiable

Type:Lab/Research institutions

inquiry

Henan Allgreen Chemical Co.,Ltd

high qualityAppearance:white crystalline powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

1H-BENZOIMIDAZOL-5-YLAMINE

Cas:2538-68-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other Value-added customer services, for diversified range products of chemicals

PHENAZINE-1-CARBOXYLIC ACID

Cas:2538-68-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Xian Changyue Biological Technology Co., Ltd.

best seller Application:API

PHENAZINE-1-CARBOXYLIC ACID

Cas:2538-68-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Wuhan Circle Star Chem-medical Technology co.,Ltd.

1,we produce and sell good chemicals around the world.2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%.3,our staff consists of highly qualified in

PHENAZINE-1-CARBOXYLIC ACID

Cas:2538-68-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

phenazine-1-carboxylic acid

Cas:2538-68-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

We are a trading company aiming at providing high-quality services to customers. Established for many years, with good reputation in the industry Storage:Sealed and preserved Application:Fine chemical intermediates, used as the main raw material for

1-Phenazinecarboxylic Acid

Cas:2538-68-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hubei Langyou International Trading Co., Ltd

1-Phenazinecarboxylic Acid Application:1-Phenazinecarboxylic Acid

1-Phenazinecarboxylic Acid

Cas:2538-68-3

Min.Order:0

Negotiable

Type:Other

inquiry

Synthetic route

1-hydroxymethylphenazine
1082-79-7

1-hydroxymethylphenazine

tubermycin B
2538-68-3

tubermycin B

Conditions
ConditionsYield
With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); oxygen In acetonitrile at 80℃; for 10h; Reagent/catalyst; Green chemistry;98.2%
6-nitrodiphenylamine-2-carboxylic acid
54420-95-0

6-nitrodiphenylamine-2-carboxylic acid

tubermycin B
2538-68-3

tubermycin B

Conditions
ConditionsYield
With sodium tetrahydroborate; sodium ethanolate In ethanol for 1h; Heating;82%
With sodium tetrahydroborate; sodium hydroxide for 4h;79.4%
With sodium tetrahydroborate; sodium ethanolate In ethanol at 65℃; for 24h; Inert atmosphere;54%
N-(2-fluorophenyl)-3-nitroanthranilic acid
106976-05-0

N-(2-fluorophenyl)-3-nitroanthranilic acid

tubermycin B
2538-68-3

tubermycin B

Conditions
ConditionsYield
With sodium tetrahydroborate In ethanol for 1h; Heating;82%
1-cyanophenazine
411211-73-9

1-cyanophenazine

tubermycin B
2538-68-3

tubermycin B

Conditions
ConditionsYield
With sulfuric acid at 140℃; for 1h;75%
With potassium hydroxide
N-(2-methoxyphenyl)-3-nitroanthranilic acid
38120-51-3

N-(2-methoxyphenyl)-3-nitroanthranilic acid

A

tubermycin B
2538-68-3

tubermycin B

B

9-methoxyphenazine-1-carboxylic acid
23531-25-1

9-methoxyphenazine-1-carboxylic acid

Conditions
ConditionsYield
With sodium tetrahydroborate; sodium methylate In methanol Heating;A n/a
B 33%
anthranilic acid
118-92-3

anthranilic acid

nitrobenzene
98-95-3

nitrobenzene

tubermycin B
2538-68-3

tubermycin B

Conditions
ConditionsYield
With potassium hydroxide at 150 - 160℃;30%
With potassium hydroxide at 145 - 160℃;
2-((2-chlorophenyl)amino)-3-nitrobenzoic acid
38120-54-6

2-((2-chlorophenyl)amino)-3-nitrobenzoic acid

A

tubermycin B
2538-68-3

tubermycin B

B

9-chlorophenazine-1-carboxylic acid
103942-93-4

9-chlorophenazine-1-carboxylic acid

Conditions
ConditionsYield
With sodium hydroxide; sodium tetrahydroborateA n/a
B 21%
N-(2-phenoxyphenyl)-3-nitroanthranilic acid
103942-78-5

N-(2-phenoxyphenyl)-3-nitroanthranilic acid

A

tubermycin B
2538-68-3

tubermycin B

B

9-phenoxyphenazine-1-carboxylic acid
103942-79-6

9-phenoxyphenazine-1-carboxylic acid

Conditions
ConditionsYield
With sodium hydroxide; sodium tetrahydroborate for 48h; Reductive cyclization; Heating;A n/a
B 10%
1-methyl-phenazine
1016-59-7

1-methyl-phenazine

acetic anhydride
108-24-7

acetic anhydride

tubermycin B
2538-68-3

tubermycin B

Conditions
ConditionsYield
With chromium(VI) oxide; sulfuric acid; acetic acid
1-methyl-phenazine
1016-59-7

1-methyl-phenazine

acetic acid
64-19-7

acetic acid

tubermycin B
2538-68-3

tubermycin B

Conditions
ConditionsYield
With chromium(VI) oxide
phenazine-1-carboxamide
550-89-0

phenazine-1-carboxamide

tubermycin B
2538-68-3

tubermycin B

Conditions
ConditionsYield
With potassium hydroxide
With hydrogenchloride
With sulfuric acid
With water Acidic conditions;
2-bromo-3-nitro-benzoic acid
573-54-6

2-bromo-3-nitro-benzoic acid

tubermycin B
2538-68-3

tubermycin B

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 91 percent / N-ethylmorpholine / CuCl / various solvent(s) / 4 h / 80 °C
2: NaBH4; 2 N aq. NaOH / 48 h / Heating
View Scheme
Multi-step reaction with 2 steps
1: 79 percent / CuCl, Cu, N-ethylmorpholine / various solvent(s) / 15 h / 70 - 80 °C
2: NaBH4, NaOMe / methanol / Heating
View Scheme
Multi-step reaction with 2 steps
1: 78 percent / CuCl, Cu, N-ethylmorpholine / various solvent(s) / 15 h / 70 °C
2: 82 percent / NaBH4, NaOEt / ethanol / 1 h / Heating
View Scheme
2-phenoxyaniline
2688-84-8

2-phenoxyaniline

tubermycin B
2538-68-3

tubermycin B

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 91 percent / N-ethylmorpholine / CuCl / various solvent(s) / 4 h / 80 °C
2: NaBH4; 2 N aq. NaOH / 48 h / Heating
View Scheme
1-bromophenazine
3331-27-9

1-bromophenazine

tubermycin B
2538-68-3

tubermycin B

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 61 percent / dimethylsulfoxide / 3 h / 200 °C
2: 75 percent / aq. H2SO4 / 1 h / 140 °C
View Scheme
2-methoxy-phenylamine
90-04-0

2-methoxy-phenylamine

tubermycin B
2538-68-3

tubermycin B

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 79 percent / CuCl, Cu, N-ethylmorpholine / various solvent(s) / 15 h / 70 - 80 °C
2: NaBH4, NaOMe / methanol / Heating
View Scheme
aniline
62-53-3

aniline

ethane-α.β-bis-sulfonic acid chloride

ethane-α.β-bis-sulfonic acid chloride

tubermycin B
2538-68-3

tubermycin B

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 78 percent / CuCl, Cu, N-ethylmorpholine / various solvent(s) / 15 h / 70 °C
2: 82 percent / NaBH4, NaOEt / ethanol / 1 h / Heating
View Scheme
2-Chloroaniline
95-51-2

2-Chloroaniline

tubermycin B
2538-68-3

tubermycin B

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 58 percent / CuCl, Cu, N-ethylmorpholine / various solvent(s) / 15 h / 70 - 80 °C
2: NaBH4, 2N aq. NaOH
View Scheme
2-Fluoroaniline
348-54-9

2-Fluoroaniline

tubermycin B
2538-68-3

tubermycin B

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Cu, cuprous chloride, N-ethylmorpholine / various solvent(s) / 18 h / 70 °C
2: 82 percent / NaBH4 / ethanol / 1 h / Heating
View Scheme
1-methyl-1,2,3,4-tetrahydrophenazine
856342-39-7

1-methyl-1,2,3,4-tetrahydrophenazine

tubermycin B
2538-68-3

tubermycin B

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: iodine; acetic acid
2: CrO3
View Scheme
2,3-dinitro-benzonitrile
90325-27-2

2,3-dinitro-benzonitrile

tubermycin B
2538-68-3

tubermycin B

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: ethanol
2: iron (II)-oxalate dihydrate; lead / 260 °C
3: aq.-ethanolic KOH
View Scheme
3-nitro-2-(phenylamino)benzonitrile
411212-01-6

3-nitro-2-(phenylamino)benzonitrile

tubermycin B
2538-68-3

tubermycin B

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: iron (II)-oxalate dihydrate; lead / 260 °C
2: aq.-ethanolic KOH
View Scheme
aniline
62-53-3

aniline

tubermycin B
2538-68-3

tubermycin B

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: ethanol
2: iron (II)-oxalate dihydrate; lead / 260 °C
3: aq.-ethanolic KOH
View Scheme
Multi-step reaction with 2 steps
1: N-ethylmorpholine;; copper(l) chloride; copper / 16 h / 70 °C / Inert atmosphere
2: sodium tetrahydroborate; sodium ethanolate / ethanol / 24 h / 65 °C / Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1: N-ethylmorpholine;; 2.3-butanediol; copper(l) chloride; copper / 16 h / 70 °C / Inert atmosphere
2: sodium tetrahydroborate; sodium ethanolate / ethanol / 24 h / 65 °C / Inert atmosphere
View Scheme
1,2-diamino-benzene
95-54-5

1,2-diamino-benzene

tubermycin B
2538-68-3

tubermycin B

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: sodium acetate; acetic acid
2: iodine; acetic acid
3: CrO3
View Scheme
3-methyl-1,2-benzenediamine
2687-25-4

3-methyl-1,2-benzenediamine

tubermycin B
2538-68-3

tubermycin B

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: 10 h / 210 - 220 °C / Inert atmosphere
1.2: air / 3 h / 210 - 220 °C
2.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 4 h / Reflux
3.1: sodium carbonate / N,N-dimethyl-formamide; water / 2 h / 80 °C
4.1: 2,2'-azobis(isobutyronitrile); oxygen; N-Bromosuccinimide / acetonitrile / 10 h / 80 °C / Green chemistry
View Scheme
benzene-1,2-diol
120-80-9

benzene-1,2-diol

tubermycin B
2538-68-3

tubermycin B

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: 10 h / 210 - 220 °C / Inert atmosphere
1.2: air / 3 h / 210 - 220 °C
2.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 4 h / Reflux
3.1: sodium carbonate / N,N-dimethyl-formamide; water / 2 h / 80 °C
4.1: 2,2'-azobis(isobutyronitrile); oxygen; N-Bromosuccinimide / acetonitrile / 10 h / 80 °C / Green chemistry
View Scheme
1-methyl-phenazine
1016-59-7

1-methyl-phenazine

tubermycin B
2538-68-3

tubermycin B

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 4 h / Reflux
2: sodium carbonate / N,N-dimethyl-formamide; water / 2 h / 80 °C
3: 2,2'-azobis(isobutyronitrile); oxygen; N-Bromosuccinimide / acetonitrile / 10 h / 80 °C / Green chemistry
View Scheme
chorismic acid
617-12-9

chorismic acid

A

tubermycin B
2538-68-3

tubermycin B

B

phenazine-1,6-dicarboxylic acid
23462-25-1

phenazine-1,6-dicarboxylic acid

Conditions
ConditionsYield
With XpzABCDETF Enzymatic reaction;
tubermycin B
2538-68-3

tubermycin B

phenazine-1-carboxylic acid chloride

phenazine-1-carboxylic acid chloride

Conditions
ConditionsYield
With thionyl chloride98%
With thionyl chloride In toluene at 100℃; for 3h;97%
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 50℃; for 12h;92%
tubermycin B
2538-68-3

tubermycin B

1‑amino‑2‑(2,4‑difluorophenyl)‑3‑(1H‑1,2,4‑triazol‑1‑yl)propan‑2‑ol
126916-76-5

1‑amino‑2‑(2,4‑difluorophenyl)‑3‑(1H‑1,2,4‑triazol‑1‑yl)propan‑2‑ol

N-(2-(2,4-difluorophenyl)-2-hydroxy-3-(1H-1,2,4-triazol-1-yl)propyl)phenazine-1-carboxamide

N-(2-(2,4-difluorophenyl)-2-hydroxy-3-(1H-1,2,4-triazol-1-yl)propyl)phenazine-1-carboxamide

Conditions
ConditionsYield
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 0 - 25℃; for 10.5h; Inert atmosphere;96%
methanol
67-56-1

methanol

tubermycin B
2538-68-3

tubermycin B

phenazine-1-carboxylic acid methyl ester
3225-19-2

phenazine-1-carboxylic acid methyl ester

Conditions
ConditionsYield
With sulfuric acid86%
With sulfuric acid
Tetraethylene glycol
112-60-7

Tetraethylene glycol

tubermycin B
2538-68-3

tubermycin B

tetraethyleneglycol phenazine-1-carboxylate

tetraethyleneglycol phenazine-1-carboxylate

Conditions
ConditionsYield
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0℃; for 24h;86%
tubermycin B
2538-68-3

tubermycin B

phenazin-1-ylamine
2876-22-4

phenazin-1-ylamine

Conditions
ConditionsYield
Stage #1: tubermycin B With diphenyl phosphoryl azide; triethylamine In tetrahydrofuran at 20℃; for 3h; Inert atmosphere;
Stage #2: With water In tetrahydrofuran for 2h; Inert atmosphere; Reflux;
61%
Stage #1: tubermycin B With diphenyl phosphoryl azide; triethylamine In tetrahydrofuran at 20℃; for 3h; Inert atmosphere;
Stage #2: With water In tetrahydrofuran for 2h; Curtius Rearrangement; Reflux; Inert atmosphere;
61%
Stage #1: tubermycin B With diphenyl phosphoryl azide; triethylamine
Stage #2: With water
Stage #1: tubermycin B With diphenyl phosphoryl azide; triethylamine
Stage #2: With water
tubermycin B
2538-68-3

tubermycin B

phenazine-1-carboxylic acid 5-oxide
27210-90-8

phenazine-1-carboxylic acid 5-oxide

Conditions
ConditionsYield
With dihydrogen peroxide; acetic acid In water at 55℃; for 17h; Inert atmosphere;58%
With dihydrogen peroxide; acetic acid In water at 55℃; for 17h; Inert atmosphere;58%
With dihydrogen peroxide In acetic acid at 55 - 60℃; for 24h;38%
With dihydrogen peroxide; acetic acid
tubermycin B
2538-68-3

tubermycin B

4-phenyl-1-butylamine
13214-66-9

4-phenyl-1-butylamine

C23H21N3O

C23H21N3O

Conditions
ConditionsYield
Stage #1: tubermycin B; 4-phenyl-1-butylamine With tris(2,2,2-trifluoroethyl) borate In acetonitrile at 80℃; for 24h;
Stage #2: In dichloromethane; water; acetonitrile at 20℃; for 0.5h;
52.64%
With tris(2,2,2-trifluoroethyl) borate In acetonitrile at 80℃; for 24h;52.64%
tubermycin B
2538-68-3

tubermycin B

butan-1-ol
71-36-3

butan-1-ol

C17H16N2O2

C17H16N2O2

Conditions
ConditionsYield
Stage #1: tubermycin B With thionyl chloride In toluene at 80℃; for 2h;
Stage #2: butan-1-ol With triethylamine In dichloromethane at 20℃; for 12h;
52%
methanesulfonamide
3144-09-0

methanesulfonamide

tubermycin B
2538-68-3

tubermycin B

N-(methylsulfonyl)phenazine-1-carboxamide

N-(methylsulfonyl)phenazine-1-carboxamide

Conditions
ConditionsYield
Stage #1: tubermycin B With dmap; 1,1'-carbonyldiimidazole In dichloromethane; N,N-dimethyl-formamide at 70℃; for 2h; Inert atmosphere;
Stage #2: methanesulfonamide With triethylamine In dichloromethane; N,N-dimethyl-formamide at 70℃; for 48h; Inert atmosphere;
40%
2-(acetylamino)ethanethiol
1190-73-4

2-(acetylamino)ethanethiol

tubermycin B
2538-68-3

tubermycin B

A

C17H15N3O3S

C17H15N3O3S

B

C17H15N3O3S

C17H15N3O3S

C

C17H15N3O3S

C17H15N3O3S

D

C17H15N3O3S

C17H15N3O3S

Conditions
ConditionsYield
In dimethyl sulfoxide for 24h; UV-irradiation; regioselective reaction;A 10%
B 8%
C 6%
D 5%
tubermycin B
2538-68-3

tubermycin B

phenazine-1-carboxylic acid methyl ester
3225-19-2

phenazine-1-carboxylic acid methyl ester

Conditions
ConditionsYield
With ethanol; acetone
In methanol; diethyl ether; chloroform
In diethyl ether for 2h; Ambient temperature;18.5 mg
In methanol at 20℃; Darkness;50 mg
tubermycin B
2538-68-3

tubermycin B

phenazine-1-carboxamide
550-89-0

phenazine-1-carboxamide

Conditions
ConditionsYield
With thionyl chloride und anschliessend Behandeln mit konz.wss.NH3;
Multi-step reaction with 2 steps
1: concentrated H2SO4
2: concentrated aqueous NH3
View Scheme
Multi-step reaction with 2 steps
1: methanol / 20 °C / Darkness
2: ammonia / methanol / 20 °C
View Scheme
tubermycin B
2538-68-3

tubermycin B

phenazine-1-carboxylic acid methyl ester
3225-19-2

phenazine-1-carboxylic acid methyl ester

Conditions
ConditionsYield
With thionyl chloride und Erwaermen des Reaktionsprodukts mit Methanol;
Multi-step reaction with 2 steps
1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / Reflux
2: dichloromethane / 2.5 h / 0 - 5 °C / Reflux
View Scheme
Multi-step reaction with 2 steps
1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0 °C / Reflux
2: triethylamine / dichloromethane / Reflux
View Scheme
tubermycin B
2538-68-3

tubermycin B

phenazine-1-carboxylic acid dimethylamide

phenazine-1-carboxylic acid dimethylamide

Conditions
ConditionsYield
With thionyl chloride und Behandeln des erhaltenen Saeurechlorids mit wss.Dimethylamin;
tubermycin B
2538-68-3

tubermycin B

phenazine-1-carboxylic acid-(2-diethylamino-ethyl ester); hydrochloride

phenazine-1-carboxylic acid-(2-diethylamino-ethyl ester); hydrochloride

Conditions
ConditionsYield
With thionyl chloride und Erwaermen des Reaktionsprodukts mit 2-Diaethylamino-aethanol in Benzol;
tubermycin B
2538-68-3

tubermycin B

5,10-dihydrophenazine-1-carboxylic acid
91822-73-0

5,10-dihydrophenazine-1-carboxylic acid

Conditions
ConditionsYield
With methanol; nickel Hydrogenation;
tubermycin B
2538-68-3

tubermycin B

N,N-dimethylethylenediamine
108-00-9

N,N-dimethylethylenediamine

Phenazine-1-carboxylic acid (2-dimethylamino-ethyl)-amide
103942-97-8

Phenazine-1-carboxylic acid (2-dimethylamino-ethyl)-amide

Conditions
ConditionsYield
With 1,1'-carbonyldiimidazole In N,N-dimethyl-formamide
tubermycin B
2538-68-3

tubermycin B

N-<2-(4-aminophenoxy)ethyl>-3,4-dimethoxy-N-methylbenzenemethanamine
143666-91-5

N-<2-(4-aminophenoxy)ethyl>-3,4-dimethoxy-N-methylbenzenemethanamine

N-[4-(2-(Methylveratrylamino)ethoxy)phenyl]-1-phenazinecarboxamide

N-[4-(2-(Methylveratrylamino)ethoxy)phenyl]-1-phenazinecarboxamide

Conditions
ConditionsYield
With 1-hydroxybenzotriazol-hydrate; dicyclohexyl-carbodiimide In N,N-dimethyl-formamide

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