CAS No.324763-51-1,3-Amino-2,2-dimethylpropionamide Suppliers

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Product name:3-Amino-2,2-dimethylpropionamide Cas No: 324763-51-1 Assay: 99%min Hangzhou Verychem Science And Technology Co. Ltd. was set up in year 2004, it’s a young but fast growing company. In

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Kono Chem Co.,Ltd

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Jinan Finer Chemical Co., Ltd

Product Description Product website: http://www.finerchem.com/pro01en/id/815.html Product Name 3-Amino-2,2-dimethylpropionamide

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Henan Tianfu Chemical Co., Ltd.

3-Amino-2,2-dimethylpropionamide Basic information Product Name: 3-Amino-2,2-dimethylpropionamide Synonyms: 2-(aminomethyl)-2-methylpropanamide;3-Amino-2,2-dimethyl

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Hebei Nengqian Chemical Import and Export Co., LTD

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EAST CHEMSOURCES LIMITED

organic intermediates Appearance:White powder Storage:Stored in the ventilated, low temperature and dry room away from direct sunlight. Package:25kg/drum Application:organic intermediates Port:QINGDAO

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Qingdao Beluga Import and Export Co., LTD

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Henan Wentao Chemical Product Co., Ltd.

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Xiamen Hisunny Chemical Co.,Ltd

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SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

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Hangzhou JINLAN Pharm-Drugs Technology Co., Ltd

Name 3-Amino-2,2-dimethylpropionamide Synonyms 3-Amino-2,2-dimethylpropanamide Molecular Structure Molecular

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Afine Chemicals Limited

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Siwei Development Group Ltd.

Product name: 3-Amino-2,2-Dimethylpropionamide CAS No.: 324763-51-1 Molecule Formula：C5H12N2O Molecule Weight：116.16 Purity: 99.0% Package: 25kg/drum Description：White crystalline powder Manufacture Standards：Enterprise Standard

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Zibo Dorne chemical technology co. LTD

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Shanghai Minstar Chemical Co., Ltd

Product Name: 3-Amino-2,2-dimethylpropionamide Synonyms: 2-(aminomethyl)-2-methylpropanamide;3-amino-2,2-dimethylpropionic acid amide;ALISKIREN InterMediates/ AM4;3-Amino-2,2-dimethylpropanamide;3-Amino-2,2-dimethylpropionamide;3-AMino-2,2-diMe

3-Amino-2,2-dimethylpropionamide

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Synthetic route

: 4300-97-4
3-Chloropivaloyl chloride

: 324763-51-1
aminopivalinamide

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: ammonia / dichloromethane / 2.75 h / 20 °C / Cooling with ice 2: sodium methylate; ammonia / methanol / 50 h / 60 °C / Autoclave View Scheme
Multi-step reaction with 4 steps 1.1: ammonia / dichloromethane / 2.75 h / 20 °C / Cooling with ice 2.1: sodium hydroxide / methanol / 70 h / 50 - 53 °C / Sealed tube 2.2: 0.17 h / 0 - 20 °C 3.1: hydrogenchloride / 20 h / 20 °C 4.1: ammonia / methanol / 48 h / 60 °C / 3750.38 Torr / Autoclave View Scheme

: 2843-17-6
3-bromo-2,2-dimethylpropionic acid

: 324763-51-1
aminopivalinamide

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: ammonia / 1,4-dioxane / 16 h / 60 °C / 2250.23 Torr / Autoclave 2: hydrogenchloride / 20 h / 20 °C 3: ammonia / methanol / 48 h / 60 °C / 3750.38 Torr / Autoclave View Scheme

: 324763-51-1
aminopivalinamide

: 324763-46-4
(3S,5S)-5-{(1S,3S)-1-azido-3-{[4-methoxy-3-(3-methoxypropoxy)phenyl]methyl}-4-methylpentyl}-dihydro-3-(1-methylethyl)furan-2(3H)-one

: acetic acid (1S,2S,4S)-2-azido-1-[(S)-2-(2-carbamoyl-2-methyl-propylcarbamoyl)-3-methyl-butyl]-4-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-5-methyl-hexyl ester

Conditions

Conditions	Yield
With 2-hydroxypyridin; triethylamine at 90℃; for 16h; After distillation of a part of Et3N over a period of 0.5 h further 8.5 h heating at 90 °ree;C;	100%

: 324763-51-1
aminopivalinamide

: 1309922-72-2
(3S,5R)-5-((1S,3S)-1-azido-3-(4-methoxy-3-(methoxypropoxy)benzyl)-4-methylpentyl)-3-isopropyl-dihydrofuran-2(3H)-one

: 1607844-94-9
(2S,4R,5S,7S)-N-(3-amino-2,2-dimethyl-3-oxopropyl)-5-azido-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(methoxypropoxy)benzyl)-8-methylnonanamide

Conditions

Conditions	Yield
With propionic acid at 110℃; for 2h;	95%

: 866030-35-5
tert-butyl {(1S,3S)-1-((2S,4S)-4-isopropyl-5-oxotetrahydrofuran-2-yl)-3-[4-methoxy-3-(3-methoxypropoxy)benzyl]-4-methylpentyl}carbamate

: 324763-51-1
aminopivalinamide

: 173338-07-3
tert-butyl (3S,5S,6S,8S)-8-(3-amino-2,2-dimethyl-3-oxopropylcarbamoyl)-6-hydroxy-3-(4-methoxy-3-(3-methoxypropoxy)benzyl)-2,9-dimethyldecan-5-ylcarbamate

Conditions

Conditions	Yield
With 2-Ethylhexanoic acid In n-heptane at 60℃; Reagent/catalyst; Temperature; Solvent; Time;	94%
With 2-Ethylhexanoic acid In n-heptane at 60℃; for 40h; Solvent; Reagent/catalyst;	93%
With 2-Ethylhexanoic acid In n-heptane at 70℃; for 8h; Inert atmosphere;	92%

: 324763-51-1
aminopivalinamide

: 1,1-dimethylethyl[(1S,3S)-3-[{4-methoxy-3-(3-methoxypropoxy)phenyl}methyl]-4-methyl-1-[tetrahydro-4-(1-methylethyl)-5-oxo-2-furanyl]pentyl]carbamate

: C35H61N3O8

Conditions

Conditions	Yield
2-Ethylhexanoic acid In tetrahydrofuran at 100℃; for 6h; Product distribution / selectivity;	93%

: 324763-51-1
aminopivalinamide

: 324763-46-4
(3S,5S)-5-{(1S,3S)-1-azido-3-{[4-methoxy-3-(3-methoxypropoxy)phenyl]methyl}-4-methylpentyl}-dihydro-3-(1-methylethyl)furan-2(3H)-one

: (2S,4S,5S,7S)-N-(3-amino-2,2-dimethyl-3-oxopropyl)-5-azido-4-hydroxy-2-isopropyl-7-[4-methoxy-3-(3-methoxypropoxy)benzyl]-8-methylnonanamide

Conditions

Conditions	Yield
With propionic acid at 120℃; for 1.5h;	87%

: 324763-51-1
aminopivalinamide

: 1236549-00-0
{(1S,3S)-1-((2S,4S)-4-isopropyl-5-oxo-furanidin-2-yl)-3-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-4-methyl-pentyl}-carbamic acid benzyl ester

: 1236549-06-6
(1S,2S,4S)-4-(2-carbamoyl-2-methylpropyl-carbamoyl)-2-hydroxy-1-{(S)-2-[4-methoxy-3-(3-methoxypropoxy)-benzyl]-3-methylbutyl}-5-methylhexyl-carbamic acid benzyl ester

Conditions

Conditions	Yield
With 2-Ethylhexanoic acid In di-isopropyl ether at 60℃; Solvent; Reagent/catalyst;	86%
With 2-Ethylhexanoic acid In di-isopropyl ether at 60℃; Reagent/catalyst; Solvent;	86%
With 2-hydroxypyridin; triethylamine In toluene for 16h; Reflux; Inert atmosphere;	82%

: 324763-51-1
aminopivalinamide

: C30H49NO7

: C35H61N3O8

Conditions

Conditions	Yield
With 2-Ethylhexanoic acid at 120℃; for 0.833333h;	84%

: 142-08-5
2-hydroxypyridin

: 324763-51-1
aminopivalinamide

: 324763-46-4
(3S,5S)-5-{(1S,3S)-1-azido-3-{[4-methoxy-3-(3-methoxypropoxy)phenyl]methyl}-4-methylpentyl}-dihydro-3-(1-methylethyl)furan-2(3H)-one

: 324763-47-5
(2S,4S,5S,7S)-N-(3-amino-2,2-dimethyl-3-oxopropyl)-5-azido-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(methoxypropoxy)benzyl)-8-methylnonanamide

Conditions

Conditions	Yield
With triethylamine	79%

...Expand

: 324763-51-1
aminopivalinamide

: (3S,5R)-5-[(1R,3S)-1-azido-3-[[4-methoxy-3-(3-methoxypropoxy)phenyl]methyl]-4-methylpentyl]dihydro-3-isopropyl-2(3H)-furanone

: (2S,4R,5R,7S)-N-(3-amino-2,2-dimethyl-3-oxopropyl)-5-azido-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(3-methoxypropoxy)benzyl)-8-methylnonanamide

Conditions

Conditions	Yield
With triethylamine In toluene at 80 - 90℃; for 20h;	78.5%

: 324763-51-1
aminopivalinamide

: 1000047-42-6
N-{(S)-2-[2,2-dimethyl-4-(2-methylphenyl)-5-oxopiperazin-1-yl]-1-[(2S,4S)-4-isopropyl-5-oxotetrahydrofuran-2-yl]ethyl}-2-nitrobenzenesulfonamide

: 1000047-43-7
(2S,4S,5S)-6-[2,2-dimethyl-4-(2-methylphenyl)-5-oxopiperazin-1-yl]-4-hydroxy-2-isopropyl-5-(2-nitrobenzenesulfonylamino)hexanoic acid (2-carbamoyl-2-methylpropyl)amide

Conditions

Conditions	Yield
With 2-hydroxypyridin; triethylamine at 80℃; for 15h;	78%

: 324763-51-1
aminopivalinamide

: 324763-46-4
(3S,5S)-5-{(1S,3S)-1-azido-3-{[4-methoxy-3-(3-methoxypropoxy)phenyl]methyl}-4-methylpentyl}-dihydro-3-(1-methylethyl)furan-2(3H)-one

: 324763-47-5
(2S,4S,5S,7S)-N-(3-amino-2,2-dimethyl-3-oxopropyl)-5-azido-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(methoxypropoxy)benzyl)-8-methylnonanamide

Conditions

Conditions	Yield
With 2-hydroxypyridin; triethylamine at 80℃;	76%
With 2-hydroxypyridin; triethylamine	59%

: 324763-51-1
aminopivalinamide

: N-{(1S)-2-{isopropyl[4-methoxy-3-(3-methoxypropoxy)benzyl]amino}-1-[(2S,4S)-4-isopropyl-5-oxotetrahydrofuran-2-yl]ethyl}-2-nitrobenzenesulfonamide

: (2S,4S,5S)-N-(3-amino-2,2-dimethyl-3-oxopropyl)-4-hydroxy-2-isopropyl-6-{isopropyl[4-methoxy-3-(3-methoxypropoxy)benzyl]amino}-5-{[(2-nitrophenyl)sulfonyl]amino}hexanamide

Conditions

Conditions	Yield
With 2-hydroxypyridin; triethylamine at 80℃; for 2h;	73%

: 25307-82-8
methyl 3-amino-2,2-dimethylpropionate

: 324763-51-1
aminopivalinamide

Conditions

Conditions	Yield
With ammonia In methanol at 60℃; under 3750.38 Torr; for 48h; Autoclave;	100%

: 7505-93-3
2-cyano-2-methylpropanamide

: 324763-51-1
aminopivalinamide

Conditions

Conditions	Yield
Stage #1: 2-cyano-2-methylpropanamide With ammonia; Raney nickel In methanol at 25 - 35℃; Autoclave; Stage #2: With hydrogen In methanol at 60 - 65℃; under 5149.01 - 5884.58 Torr; for 10h;	87.5%
With ammonia; hydrogen; Raney nickle In methanol at 60 - 70℃; under 3750.38 Torr; for 10h; Autoclave;	78%
Multi-step reaction with 2 steps 1.1: LAH / tetrahydrofuran 1.2: Et3N 2.1: H2 / Pd()OH)2/C View Scheme
With ammonia; hydrogen; raney nickel In methanol at 40 - 45℃; under 2942.29 Torr; for 14h;
With ammonium hydroxide; 5% rhodium on activated aluminium oxide; hydrogen In ethanol; water under 3102.97 Torr; for 72h;

: 666844-61-7
(2-carbamoyl-2-methylpropyl)carbamic acid benzyl ester

: 324763-51-1
aminopivalinamide

Conditions

Conditions	Yield
With hydrogen; palladium-carbon In ethanol at 20℃; for 2h;	85%
With hydrogen; palladium hydroxide - carbon
With hydrogen; palladium 10% on activated carbon In methanol at 20℃; for 2h;

: 41461-75-0
chloro-pivalic acid amide

: 324763-51-1
aminopivalinamide

Conditions

Conditions	Yield
With ammonia; sodium methylate In methanol at 60℃; for 50h; Autoclave;	62%
Multi-step reaction with 3 steps 1.1: sodium hydroxide / methanol / 70 h / 50 - 53 °C / Sealed tube 1.2: 0.17 h / 0 - 20 °C 2.1: hydrogenchloride / 20 h / 20 °C 3.1: ammonia / methanol / 48 h / 60 °C / 3750.38 Torr / Autoclave View Scheme

: 114583-17-4
α-(nitromethyl)isobutyronitrile

: 324763-51-1
aminopivalinamide

Conditions

Conditions	Yield
With methanol; Lindlar's catalyst Hydrogenation;
With nickel Hydrogenation;
With hydrogenchloride; iron

: 7647-01-0
hydrogenchloride

: 114583-17-4
α-(nitromethyl)isobutyronitrile

iron powder: iron powder

A: 859065-87-5
2-(5,5-dimethyl-hexahydro-pyrimidin-2-yl)-2-methyl-propionic acid amide

B: 7328-91-8
2,2-Dimethyl-1,3-diaminopropane

C: 67744-70-1
3-amino-2,2-dimethyl-propionitrile

D: 324763-51-1
aminopivalinamide

Conditions

Conditions	Yield
at 60 - 70℃;
at 60 - 70℃;

...Expand

: 67-56-1
methanol

: 114583-17-4
α-(nitromethyl)isobutyronitrile

palladium-CaCO3: palladium-CaCO3

A: 859065-87-5
2-(5,5-dimethyl-hexahydro-pyrimidin-2-yl)-2-methyl-propionic acid amide

B: 7328-91-8
2,2-Dimethyl-1,3-diaminopropane

C: 67744-70-1
3-amino-2,2-dimethyl-propionitrile

D: 324763-51-1
aminopivalinamide

Conditions

Conditions	Yield
Hydrogenation;
Hydrogenation;

...Expand

: 67-56-1
methanol

: 114583-17-4
α-(nitromethyl)isobutyronitrile

Raney nickel: Raney nickel

A: 859065-87-5
2-(5,5-dimethyl-hexahydro-pyrimidin-2-yl)-2-methyl-propionic acid amide

B: 7328-91-8
2,2-Dimethyl-1,3-diaminopropane

C: 67744-70-1
3-amino-2,2-dimethyl-propionitrile

D: 324763-51-1
aminopivalinamide

Conditions

Conditions	Yield
Hydrogenation;
Hydrogenation;

...Expand

: 114583-17-4
α-(nitromethyl)isobutyronitrile

Raney nickel: Raney nickel

methanolic NH3: methanolic NH3

A: 859065-87-5
2-(5,5-dimethyl-hexahydro-pyrimidin-2-yl)-2-methyl-propionic acid amide

B: 7328-91-8
2,2-Dimethyl-1,3-diaminopropane

C: 67744-70-1
3-amino-2,2-dimethyl-propionitrile

D: 324763-51-1
aminopivalinamide

Conditions

Conditions	Yield
at 100℃; Hydrogenation;
at 100℃; Hydrogenation;

...Expand

: 72291-30-6
methyl 2,2-dimethyl-cyanoacetate

: 324763-51-1
aminopivalinamide

Conditions

Conditions	Yield
Stage #1: methyl 2,2-dimethyl-cyanoacetate With ammonia; hydrogen; nickel In 1-methyl-pyrrolidin-2-one; water at 80℃; under 3750.38 Torr; for 1.5h; Stage #2: With ammonia; hydrogen; nickel In 1-methyl-pyrrolidin-2-one; water at 80℃; under 150015 Torr; Product distribution / selectivity;
Stage #1: methyl 2,2-dimethyl-cyanoacetate With ammonia; hydrogen; cobalt In water; butan-1-ol at 80℃; under 3750.38 Torr; for 1.5h; Stage #2: With ammonia; hydrogen; cobalt In water; butan-1-ol at 80℃; under 48754.9 Torr; Product distribution / selectivity;
Stage #1: methyl 2,2-dimethyl-cyanoacetate With ammonia; hydrogen; cobalt In methanol; water at 80℃; under 3750.38 Torr; for 1.5h; Stage #2: With ammonia; hydrogen; cobalt In methanol; water at 80℃; under 48754.9 Torr; Product distribution / selectivity;
Stage #1: methyl 2,2-dimethyl-cyanoacetate With ammonia; hydrogen; nickel In water; butan-1-ol at 80℃; under 3750.38 Torr; for 1.5h; Stage #2: With ammonia; hydrogen; nickel In water; butan-1-ol at 80℃; under 48754.9 Torr; Product distribution / selectivity;

: 72291-30-6
methyl 2,2-dimethyl-cyanoacetate

A: 324763-51-1
aminopivalinamide

B: 25307-82-8
methyl 3-amino-2,2-dimethylpropionate

Conditions

Conditions	Yield
With ammonia; hydrogen; mixture of 28percent NiO, 28percent CoO, 13percent CuO, 31percent ZrO2; hydrogenated In methanol at 100℃; under 150015 Torr; Product distribution / selectivity;
With ammonia; hydrogen; mixture of 28percent NiO, 28percent CoO, 13percent CuO, 31percent ZrO2; hydrogenated In tetrahydrofuran at 100℃; under 150015 Torr; Product distribution / selectivity;

: 2941-18-6
4,4-dimethylpyrazolidin-3-one

: 324763-51-1
aminopivalinamide

Conditions

Conditions	Yield
With hydrogen; Raney-Nickel In 2-methyl-propan-1-ol at 55 - 65℃; under 750.075 Torr; Inert atmosphere; Sealed tube;

: 1572-98-1
2-cyano-2-methyl-propionic acid ethyl ester

: 324763-51-1
aminopivalinamide

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: ammonia / methanol / 12 h / 25 - 30 °C 2: hydrogen; ammonia / raney nickel / methanol / 14 h / 40 - 45 °C / 2942.29 Torr View Scheme
Multi-step reaction with 2 steps 1.1: ammonia / methanol / 25 - 35 °C 2.1: ammonia / Raney nickel / methanol / 25 - 35 °C / Autoclave 2.2: 10 h / 60 - 65 °C / 5149.01 - 5884.58 Torr View Scheme
Multi-step reaction with 2 steps 1: ammonia / methanol / 96 h / 35 °C / Sealed tube; Cooling with ice 2: hydrogen; ammonium hydroxide; 5% rhodium on activated aluminium oxide / ethanol; water / 72 h / 3102.97 Torr View Scheme

: 4835-90-9
3-Hydroxy-2,2-dimethylpropanoic acid

: 324763-51-1
aminopivalinamide

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: hydrogen bromide / water / 19 h / 100 °C 2: ammonia / 1,4-dioxane / 16 h / 60 °C / 2250.23 Torr / Autoclave 3: hydrogenchloride / 20 h / 20 °C 4: ammonia / methanol / 48 h / 60 °C / 3750.38 Torr / Autoclave View Scheme

: 19036-43-2
aminopivalic acid

: 324763-51-1
aminopivalinamide

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: hydrogenchloride / 20 h / 20 °C 2: ammonia / methanol / 48 h / 60 °C / 3750.38 Torr / Autoclave View Scheme

: 4300-97-4
3-Chloropivaloyl chloride

: 324763-51-1
aminopivalinamide

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: ammonia / dichloromethane / 2.75 h / 20 °C / Cooling with ice 2: sodium methylate; ammonia / methanol / 50 h / 60 °C / Autoclave View Scheme
Multi-step reaction with 4 steps 1.1: ammonia / dichloromethane / 2.75 h / 20 °C / Cooling with ice 2.1: sodium hydroxide / methanol / 70 h / 50 - 53 °C / Sealed tube 2.2: 0.17 h / 0 - 20 °C 3.1: hydrogenchloride / 20 h / 20 °C 4.1: ammonia / methanol / 48 h / 60 °C / 3750.38 Torr / Autoclave View Scheme

: 2843-17-6
3-bromo-2,2-dimethylpropionic acid

: 324763-51-1
aminopivalinamide

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: ammonia / 1,4-dioxane / 16 h / 60 °C / 2250.23 Torr / Autoclave 2: hydrogenchloride / 20 h / 20 °C 3: ammonia / methanol / 48 h / 60 °C / 3750.38 Torr / Autoclave View Scheme

: 324763-51-1
aminopivalinamide

: 324763-46-4
(3S,5S)-5-{(1S,3S)-1-azido-3-{[4-methoxy-3-(3-methoxypropoxy)phenyl]methyl}-4-methylpentyl}-dihydro-3-(1-methylethyl)furan-2(3H)-one

: acetic acid (1S,2S,4S)-2-azido-1-[(S)-2-(2-carbamoyl-2-methyl-propylcarbamoyl)-3-methyl-butyl]-4-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-5-methyl-hexyl ester

Conditions

Conditions	Yield
With 2-hydroxypyridin; triethylamine at 90℃; for 16h; After distillation of a part of Et3N over a period of 0.5 h further 8.5 h heating at 90 °ree;C;	100%

: 324763-51-1
aminopivalinamide

: 1309922-72-2
(3S,5R)-5-((1S,3S)-1-azido-3-(4-methoxy-3-(methoxypropoxy)benzyl)-4-methylpentyl)-3-isopropyl-dihydrofuran-2(3H)-one

: 1607844-94-9
(2S,4R,5S,7S)-N-(3-amino-2,2-dimethyl-3-oxopropyl)-5-azido-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(methoxypropoxy)benzyl)-8-methylnonanamide

Conditions

Conditions	Yield
With propionic acid at 110℃; for 2h;	95%

: 866030-35-5
tert-butyl {(1S,3S)-1-((2S,4S)-4-isopropyl-5-oxotetrahydrofuran-2-yl)-3-[4-methoxy-3-(3-methoxypropoxy)benzyl]-4-methylpentyl}carbamate

: 324763-51-1
aminopivalinamide

: 173338-07-3
tert-butyl (3S,5S,6S,8S)-8-(3-amino-2,2-dimethyl-3-oxopropylcarbamoyl)-6-hydroxy-3-(4-methoxy-3-(3-methoxypropoxy)benzyl)-2,9-dimethyldecan-5-ylcarbamate

Conditions

Conditions	Yield
With 2-Ethylhexanoic acid In n-heptane at 60℃; Reagent/catalyst; Temperature; Solvent; Time;	94%
With 2-Ethylhexanoic acid In n-heptane at 60℃; for 40h; Solvent; Reagent/catalyst;	93%
With 2-Ethylhexanoic acid In n-heptane at 70℃; for 8h; Inert atmosphere;	92%

: 324763-51-1
aminopivalinamide

: 1,1-dimethylethyl[(1S,3S)-3-[{4-methoxy-3-(3-methoxypropoxy)phenyl}methyl]-4-methyl-1-[tetrahydro-4-(1-methylethyl)-5-oxo-2-furanyl]pentyl]carbamate

: C35H61N3O8

Conditions

Conditions	Yield
2-Ethylhexanoic acid In tetrahydrofuran at 100℃; for 6h; Product distribution / selectivity;	93%

: 324763-51-1
aminopivalinamide

: 324763-46-4
(3S,5S)-5-{(1S,3S)-1-azido-3-{[4-methoxy-3-(3-methoxypropoxy)phenyl]methyl}-4-methylpentyl}-dihydro-3-(1-methylethyl)furan-2(3H)-one

: (2S,4S,5S,7S)-N-(3-amino-2,2-dimethyl-3-oxopropyl)-5-azido-4-hydroxy-2-isopropyl-7-[4-methoxy-3-(3-methoxypropoxy)benzyl]-8-methylnonanamide

Conditions

Conditions	Yield
With propionic acid at 120℃; for 1.5h;	87%

: 324763-51-1
aminopivalinamide

: 1236549-00-0
{(1S,3S)-1-((2S,4S)-4-isopropyl-5-oxo-furanidin-2-yl)-3-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-4-methyl-pentyl}-carbamic acid benzyl ester

: 1236549-06-6
(1S,2S,4S)-4-(2-carbamoyl-2-methylpropyl-carbamoyl)-2-hydroxy-1-{(S)-2-[4-methoxy-3-(3-methoxypropoxy)-benzyl]-3-methylbutyl}-5-methylhexyl-carbamic acid benzyl ester

Conditions

Conditions	Yield
With 2-Ethylhexanoic acid In di-isopropyl ether at 60℃; Solvent; Reagent/catalyst;	86%
With 2-Ethylhexanoic acid In di-isopropyl ether at 60℃; Reagent/catalyst; Solvent;	86%
With 2-hydroxypyridin; triethylamine In toluene for 16h; Reflux; Inert atmosphere;	82%

: 324763-51-1
aminopivalinamide

: C30H49NO7

: C35H61N3O8

Conditions

Conditions	Yield
With 2-Ethylhexanoic acid at 120℃; for 0.833333h;	84%

: 142-08-5
2-hydroxypyridin

: 324763-51-1
aminopivalinamide

: 324763-46-4
(3S,5S)-5-{(1S,3S)-1-azido-3-{[4-methoxy-3-(3-methoxypropoxy)phenyl]methyl}-4-methylpentyl}-dihydro-3-(1-methylethyl)furan-2(3H)-one

: 324763-47-5
(2S,4S,5S,7S)-N-(3-amino-2,2-dimethyl-3-oxopropyl)-5-azido-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(methoxypropoxy)benzyl)-8-methylnonanamide

Conditions

Conditions	Yield
With triethylamine	79%

...Expand

: 324763-51-1
aminopivalinamide

: (3S,5R)-5-[(1R,3S)-1-azido-3-[[4-methoxy-3-(3-methoxypropoxy)phenyl]methyl]-4-methylpentyl]dihydro-3-isopropyl-2(3H)-furanone

: (2S,4R,5R,7S)-N-(3-amino-2,2-dimethyl-3-oxopropyl)-5-azido-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(3-methoxypropoxy)benzyl)-8-methylnonanamide

Conditions

Conditions	Yield
With triethylamine In toluene at 80 - 90℃; for 20h;	78.5%

: 324763-51-1
aminopivalinamide

: 1000047-42-6
N-{(S)-2-[2,2-dimethyl-4-(2-methylphenyl)-5-oxopiperazin-1-yl]-1-[(2S,4S)-4-isopropyl-5-oxotetrahydrofuran-2-yl]ethyl}-2-nitrobenzenesulfonamide

: 1000047-43-7
(2S,4S,5S)-6-[2,2-dimethyl-4-(2-methylphenyl)-5-oxopiperazin-1-yl]-4-hydroxy-2-isopropyl-5-(2-nitrobenzenesulfonylamino)hexanoic acid (2-carbamoyl-2-methylpropyl)amide

Conditions

Conditions	Yield
With 2-hydroxypyridin; triethylamine at 80℃; for 15h;	78%

: 324763-51-1
aminopivalinamide

: 324763-46-4
(3S,5S)-5-{(1S,3S)-1-azido-3-{[4-methoxy-3-(3-methoxypropoxy)phenyl]methyl}-4-methylpentyl}-dihydro-3-(1-methylethyl)furan-2(3H)-one

: 324763-47-5
(2S,4S,5S,7S)-N-(3-amino-2,2-dimethyl-3-oxopropyl)-5-azido-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(methoxypropoxy)benzyl)-8-methylnonanamide

Conditions

Conditions	Yield
With 2-hydroxypyridin; triethylamine at 80℃;	76%
With 2-hydroxypyridin; triethylamine	59%

: 324763-51-1
aminopivalinamide

: N-{(1S)-2-{isopropyl[4-methoxy-3-(3-methoxypropoxy)benzyl]amino}-1-[(2S,4S)-4-isopropyl-5-oxotetrahydrofuran-2-yl]ethyl}-2-nitrobenzenesulfonamide

: (2S,4S,5S)-N-(3-amino-2,2-dimethyl-3-oxopropyl)-4-hydroxy-2-isopropyl-6-{isopropyl[4-methoxy-3-(3-methoxypropoxy)benzyl]amino}-5-{[(2-nitrophenyl)sulfonyl]amino}hexanamide

Conditions

Conditions	Yield
With 2-hydroxypyridin; triethylamine at 80℃; for 2h;	73%

: 324763-51-1
aminopivalinamide

: 1663-61-2
triethoxymethylbenzene

: 5,5-dimethyl-2-phenyl-5,6-dihydropyrimidin-4(3H)-one

Conditions

Conditions	Yield
With acetic acid In ethanol at 110℃; for 24h; Inert atmosphere;	72%

: 324763-51-1
aminopivalinamide

: C29H49NO6S

: 173334-57-1
(2S,4S,5S,7S)-5-Amino-4-hydroxy-2-isopropyl-7-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-8-methyl-nonanoic acid (2-carbamoyl-2-methyl-propyl)-amide

Conditions

Conditions	Yield
With 2-hydroxypyridin; hydrogenchloride; triethylamine In methanol at 80℃;	68%

: 324763-51-1
aminopivalinamide

: 1000046-88-7
tert-butyl {(1S)-2-[4-(2-chlorophenyl)-2,2-dimethyl-5-oxopiperazin-1-yl]-1-[(2S,4S)-4-isopropyl-5-oxotetrahydrofuran-2-yl]ethyl}carbamate

: 1000046-90-1
tert-butyl {(2S,3S,5S)-5-[(3-amino-2,2-dimethyl-3-oxopropyl)carbamoyl]-1-[4-(2-chlorophenyl)-2,2-dimethyl-5-oxopiperazin-1-yl]-3-hydroxy-6-methylheptan-2-yl}carbamate

Conditions

Conditions	Yield
With 2-hydroxypyridin; triethylamine at 80℃; for 18h;	66%
With 2-hydroxypyridin; triethylamine at 80℃; for 18h;	66%

: 324763-51-1
aminopivalinamide

: 1236549-00-0
{(1S,3S)-1-((2S,4S)-4-isopropyl-5-oxo-furanidin-2-yl)-3-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-4-methyl-pentyl}-carbamic acid benzyl ester

A: 1236549-06-6
(1S,2S,4S)-4-(2-carbamoyl-2-methylpropyl-carbamoyl)-2-hydroxy-1-{(S)-2-[4-methoxy-3-(3-methoxypropoxy)-benzyl]-3-methylbutyl}-5-methylhexyl-carbamic acid benzyl ester

B: C31H51N3O7

Conditions

Conditions	Yield
With 2-hydroxypyridin In tert-butyl methyl ether at 65℃;	A 66% B n/a

...Expand

: 953820-47-8
tert-butyl (1S,3S)-1-((2S,4S)-4-isopropyl-5-oxotetrahydrofuran-2-yl)-3-((1-(3-methoxypropyl)-1H-indazol-6-yl)methyl)-4-methylpentylcarbamate

: 324763-51-1
aminopivalinamide

: 953820-48-9
tert-butyl (3S,5S,6S,8S)-8-(3-amino-2,2-dimethyl-3-oxopropylcarbamoyl)-6-hydroxy-3-((1-(3-methoxypropyl)-1H-indazol-6-yl)methyl)-2,9-dimethyldecan-5-ylcarbamate

Conditions

Conditions	Yield
With 2-hydroxypyridin; triethylamine at 80℃;	65%

: 324763-51-1
aminopivalinamide

: 325740-70-3
(3S,5S)-5-((1S,3S)-1-azido-3-(4-methoxy-3-(3-methoxypropoxy)benzyl)-4-methylpentyl)-3-isopropyldihydrofuran-2(3H)-one

: 325154-31-2
(2S,4S,5R,7S)-5-Azido-4-hydroxy-2-isopropyl-7-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-8-methyl-nonanoic acid (2-carbamoyl-2-methyl-propyl)-amide

Conditions

Conditions	Yield
With 2-hydroxypyridin; triethylamine	59%

: 324763-51-1
aminopivalinamide

: (3S,5S)-5-{(1R,3S)-1-Benzylamino-3-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-4-methyl-pentyl}-3-isopropyl-dihydro-furan-2-one

: 361460-41-5
(2S,4S,5R,7S)-5-Benzylamino-4-hydroxy-2-isopropyl-7-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-8-methyl-nonanoic acid (2-carbamoyl-2-methyl-propyl)-amide

Conditions

Conditions	Yield
With 2-hydroxypyridin; triethylamine at 80℃; for 72h;	53%

: 324763-51-1
aminopivalinamide

: 1000047-28-8
{(S)-1-[(2S,4S)-4-isopropyl-5-oxotetrahydrofuran-2-yl]-2-[4-(2-methoxymethoxyphenyl)-2,2-dimethyl-5-oxopiperazin-1-yl]ethyl}carbamic acid benzyl ester

: 1000047-29-9
{(1S,2S,4S)-4-(2-carbamoyl-2-methylpropylcarbamoyl)-2-hydroxy-1-[4-(2-methoxymethoxyphenyl)-2,2-dimethyl-5-oxopiperazin-1-ylmethyl]-5-methylhexyl}carbamic acid benzyl ester

Conditions

Conditions	Yield
With 2-hydroxypyridin; triethylamine at 80℃; for 11h;	52%

: 324763-51-1
aminopivalinamide

: 78-39-7
Triethyl orthoacetate

: 2,5,5-trimethyl-5,6-dihydropyrimidin-4(3H)-one

Conditions

Conditions	Yield
With acetic acid In ethanol at 110℃; for 24h; Inert atmosphere;	50%

: 324763-51-1
aminopivalinamide

: 1200341-46-3
(2R,2'S,3S,4'S,5S)-3-isopropyl-5-(4-isopropyl-5-oxo-tetrahydro-furan-2-yl)-2-(4-methoxy-3-(3-methoxypropoxy)-phenyl)-pyrrolidine-1-sulfonic acid 2,2,2-trichloro-ethyl ester

: 1219468-79-7
(2R,3S,5S)-2,2,2-trichloroethyl 5-((1S,3S)-3-(3-amino-2,2-dimethyl-3-oxopropylcarbamoyl)-1-hydroxy-4-methylpentyl)-3-isopropyl-2-(4-methoxy-3-(3-methoxypropoxy)phenyl)pyrrolidine-1-sulfonate

Conditions

Conditions	Yield
With 2-hydroxypyridin; triethylamine at 85℃; Inert atmosphere;	47%
With 2-hydroxypyridin; triethylamine at 85℃; for 72h; Inert atmosphere;

: 324763-51-1
aminopivalinamide

: 115-80-0
Triethyl orthopropionate

: 2-ethyl-5,5-dimethyl-5,6-dihydropyrimidin-4(3H)-one

Conditions

Conditions	Yield
With acetic acid In ethanol at 110℃; for 24h; Inert atmosphere;	44%

: 24964-76-9
triethyl orthobutyrate

: 324763-51-1
aminopivalinamide

: 5,5-dimethyl-2-propyl-5,6-dihydropyrimidin-4(3H)-one

Conditions

Conditions	Yield
With acetic acid In ethanol at 110℃; for 24h; Inert atmosphere;	36%

: 324763-51-1
aminopivalinamide

: 2-{[5-bromo-1-(2-chlorophenyl)-1H-1,2,4-triazol-3-yl]methyl}-5-(4-chlorophenyl)-4-[(2S)-3,3,3-trifluoro-2-hydroxypropyl]-2,4-dihydro-3H-1,2,4-triazol-3-one

: 3-{[1-(2-chlorophenyl)-3-({3-(4-chlorophenyl)-5-oxo-4-[(2S)-3,3,3-trifluoro-2-hydroxypropyl]-4,5-dihydro-1H-1,2,4-triazol-1-yl}methyl)-1H-1,2,4-triazol-5-yl]amino}-2,2-dimethylpropanamide

Conditions

Conditions	Yield
With N-ethyl-N,N-diisopropylamine In acetonitrile at 180℃; for 5h; Microwave irradiation;	29%

: 324763-51-1
aminopivalinamide

: 19036-43-2
aminopivalic acid

Conditions

Conditions	Yield
With sulfuric acid

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