Changzhou Wujin Linchuan Chemical Co., Ltd. is re-established in 1996 from an old stated factory. Changzhou Wujin Linchuan Chemical Co., Ltd. is a privately owned independent company plants located in Changzhou and Yan Cheng City, who is stri
Cas:3597-91-9
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inquiryDayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:3597-91-9
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inquiryItems Standard Result Assay 98%min ---------------------------------------------------------------------------------------------
Cas:3597-91-9
Min.Order:1 Gram
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inquiryProduct description: Product name 4-Biphenylmethanol CAS number 3597-91-9 Assay ≥99% Appearance Off-white crystalline powder Capacity 200mt/year Application Organic intermedi
Cas:3597-91-9
Min.Order:10 Gram
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:3597-91-9
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:3597-91-9
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryName: 4-Biphenylmethanol Synonyms: 4-Biphenylmethanol(6CI,7CI,8CI);4-(Hydroxymethyl)biphenyl;4-Biphenylylmethanol;4-Hydroxymethyl-1,1'-biphenyl;4-Phenylbenzyl alcohol;[1,1'-Biphenyl]-4-methanol;NSC 233860;NSC84169;p-Phenylbenzyl alcohol;
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Min.Order:5 Metric Ton
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Type:Other
inquiry99%min best quality 4-Biphenylmethanol 3597-91-9 in large stock 1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appea
Cas:3597-91-9
Min.Order:100 Gram
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:3597-91-9
Min.Order:1 Kilogram
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At presen
Cas:3597-91-9
Min.Order:25 Milliliter
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Type:Trading Company
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
superiorquality moderate price & quick delivery Appearance:white to beige powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Used to make
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:3597-91-9
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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Min.Order:1 Gram
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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Min.Order:1 Kilogram
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:3597-91-9
Min.Order:1 Kilogram
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inquiryWe product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Product Name:4-Biphenylmethanol CAS No:3597-91-9 Sy
Product Name: 4-Biphenylmethanol Synonyms: (1,1’-biphenyl)-4-methanol;4hmb;NSC 233860;Biphenyl-4-methanol 98%;4-Biphenylyl-methanol for synthesis;RARECHEM AL BD 0106;P-PHENYLBENZYL ALCOHOL;BIPHENYL-4-METHANOL CAS: 3597-91-9 MF: C13H
factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:3597-91-9
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Best quality & Attractive price & Professional service; Trial & Pilot & CommercialHisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, special chemicals and OLED
1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:3597-91-9
Min.Order:1 Metric Ton
FOB Price: $1.5
Type:Trading Company
inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
Conditions | Yield |
---|---|
100% | |
Stage #1: biphenyl-4-carboxylic acid With lithium aluminium tetrahydride In tetrahydrofuran; diethyl ether at 20℃; for 4h; Cooling with ice; Inert atmosphere; Stage #2: With water In tetrahydrofuran; diethyl ether for 16h; | 99% |
With lithium aluminium tetrahydride In tetrahydrofuran at 20℃; for 2h; Inert atmosphere; | 89% |
Conditions | Yield |
---|---|
Stage #1: 4-Phenylbenzaldehyde With zinc diacetate In tetrahydrofuran at 65℃; for 0.166667h; Stage #2: With methyl-di(n-propoxy)silane In tetrahydrofuran at 65℃; for 24h; Stage #3: With hydrogenchloride; water at 0℃; for 1h; | 99% |
With iron(II) fluoro{tris[2-(diphenylphosphino)phenyl]phospino}tetrafluoroborate; hydrogen; trifluoroacetic acid In isopropyl alcohol at 120℃; under 15001.5 Torr; for 2h; Inert atmosphere; Autoclave; chemoselective reaction; | 99% |
With C46H49CoN3P4(2+)*2BF4(1-); hydrogen; potassium hydroxide In ethanol; acetonitrile at 60℃; under 22801.5 Torr; for 24h; Autoclave; Glovebox; chemoselective reaction; | 99% |
Conditions | Yield |
---|---|
With C20H20N2O2Pd; sodium hydrogencarbonate In water at 80℃; for 6h; Suzuki-Miyaura Coupling; | 99% |
With trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); potassium carbonate In water for 0.5h; Catalytic behavior; Suzuki-Miyaura Coupling; Sealed tube; Inert atmosphere; Reflux; | 98% |
With palladium diacetate; potassium carbonate In water; isopropyl alcohol at 20℃; for 0.25h; Suzuki-Miyaura Coupling; | 98% |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃; Inert atmosphere; | 98% |
With hydrogenchloride In water; acetone for 1.5h; pH=12; | 24% |
With lithium aluminium tetrahydride | |
With diisobutylaluminium hydride In dichloromethane; toluene at -78℃; | |
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃; for 1h; Inert atmosphere; |
Conditions | Yield |
---|---|
With sodium carbonate at 80℃; for 1.16667h; Catalytic behavior; Suzuki Coupling; | 98% |
With potassium carbonate for 4.25h; Suzuki-Miyaura Coupling; | 92% |
With potassium carbonate at 100℃; for 5.25h; Catalytic behavior; | 90% |
Conditions | Yield |
---|---|
With sodium hydroxide; aluminum oxide; ruthenium In 1,2-dimethoxyethane; water at 90℃; for 12h; Suzuki-Miyaura-type cross coupling reaction; | 97% |
With sodium t-butanolate In water at 28℃; for 4h; Catalytic behavior; Suzuki-Miyaura Coupling; Irradiation; | 96% |
With potassium carbonate In ethanol at 20℃; for 6h; Suzuki-Miyaura Coupling; | 91% |
p-hydroxymethylphenylboronic acid
chlorobenzene
biphenyl-4-yl methanol
Conditions | Yield |
---|---|
With C37H44ClN2O3PPd; caesium carbonate In water at 100℃; for 12h; Suzuki Coupling; Schlenk technique; Inert atmosphere; | 97% |
With potassium carbonate In water at 70℃; for 12h; Catalytic behavior; Temperature; Reagent/catalyst; Suzuki Coupling; Green chemistry; | 5 %Chromat. |
Conditions | Yield |
---|---|
With potassium carbonate for 4h; Stille Cross Coupling; | 96% |
With potassium carbonate at 100℃; for 5.5h; Catalytic behavior; Stille Cross Coupling; | 93% |
Conditions | Yield |
---|---|
With [PdCl[(η5-C5H5)]Fe[(η5-C5H3)-C(CH3)=NOH](2-dicyclohexylphosphanyl-2'-(N,N-dimethylamino)biphenyl)]; caesium carbonate In water at 100℃; for 24h; Catalytic behavior; Reagent/catalyst; Concentration; Suzuki Coupling; Schlenk technique; Inert atmosphere; | 92% |
With potassium carbonate In N,N-dimethyl-formamide at 100℃; for 5h; Catalytic behavior; Suzuki-Miyaura Coupling; | 88% |
With C20H16Cl2N2Pd; potassium carbonate In N,N-dimethyl-formamide at 100℃; for 4h; Suzuki-Miyaura Coupling; | 83% |
Conditions | Yield |
---|---|
With potassium tert-butylate; C44H47I3IrN4PPd In tetrahydrofuran; isopropyl alcohol at 90℃; for 9h; Reagent/catalyst; Inert atmosphere; Schlenk technique; | 92% |
With C31H37I3IrN5Pd; potassium tert-butylate; isopropyl alcohol In tetrahydrofuran at 90℃; for 2h; Reagent/catalyst; Inert atmosphere; Schlenk technique; | 85% |
Conditions | Yield |
---|---|
With water; sodium formate; sodium carbonate at 100 - 105℃; for 1h; pH=7 - 7.5; Reagent/catalyst; | 91% |
With water at 100℃; for 24h; | 52% |
With water In N,N-dimethyl-formamide at 80℃; under 2250.23 Torr; for 20h; Temperature; Sealed tube; |
N, N-dimethyl [1,1’-biphenyl]-4-carboxamide
biphenyl-4-yl methanol
Conditions | Yield |
---|---|
With sodium hydride; sodium iodide; zinc(II) iodide In tetrahydrofuran; mineral oil at 40℃; for 10h; Sealed tube; | 89% |
Conditions | Yield |
---|---|
With potassium carbonate In methanol; water at 40 - 45℃; for 4h; Suzuki Coupling; | 88% |
With palladium diacetate; potassium carbonate In 2-methoxy-ethanol; water at 21℃; for 0.5h; Suzuki coupling; | > 99 %Chromat. |
With potassium phosphate In ethanol; water at 80℃; for 2h; Solvent; Reagent/catalyst; Time; Temperature; Suzuki-Miyaura Coupling; | |
With potassium carbonate In water at 70℃; for 12h; Catalytic behavior; Temperature; Reagent/catalyst; Suzuki Coupling; Green chemistry; | 75 %Chromat. |
4-methoxyphenylboronic acid
benzenediazonium tetrafluoroborate
biphenyl-4-yl methanol
Conditions | Yield |
---|---|
polystyrene-supported N-heterocyclic carbene-Pd complex In ethanol at 20℃; for 10h; Suzuki-Miyaura cross-coupling; | 87% |
4-bromo-1,1'-biphenyl
2-bromomethoxy-tetrahydro-pyran
biphenyl-4-yl methanol
Conditions | Yield |
---|---|
Stage #1: 4-bromo-1,1'-biphenyl With n-Butyl chloride; iodine; magnesium In 2-methyltetrahydrofuran at 60℃; for 2h; Inert atmosphere; Reflux; Stage #2: 2-bromomethoxy-tetrahydro-pyran In 2-methyltetrahydrofuran at -20 - 20℃; for 3h; Inert atmosphere; Stage #3: With hydrogenchloride In 2-methyltetrahydrofuran; water at 0 - 20℃; | 86% |
biphenyl-4-ylmethyl (4R,5S)-2,2-di-tert-butyl-5-methyl-1,3,2-dioxasilolane-4-carboxylate
methylmagnesium chloride
A
biphenyl-4-yl methanol
B
(3R,4S)-4-((di-tert-butyl(methyl)silyl)oxy)-3-hydroxypentan-2-one
C
(3R,4S)-4-((di-tert-butyl(methyl)silyl)oxy)-2-methylpentane-2,3-diol
Conditions | Yield |
---|---|
Stage #1: biphenyl-4-ylmethyl (4R,5S)-2,2-di-tert-butyl-5-methyl-1,3,2-dioxasilolane-4-carboxylate; methylmagnesium chloride With N,O-dimethylhydroxylamine*hydrochloride In tetrahydrofuran at -10℃; for 0.166667h; Inert atmosphere; Stage #2: With ammonium chloride In tetrahydrofuran; water at -10℃; Inert atmosphere; regioselective reaction; | A 85% B 65% C 16% |
Conditions | Yield |
---|---|
Stage #1: 4'-biphenyl chloride With n-Butyl chloride; iodine; magnesium In 2-methyltetrahydrofuran at 60℃; for 2h; Inert atmosphere; Reflux; Stage #2: C4H11BrOSi In 2-methyltetrahydrofuran at -20 - 20℃; for 3h; Inert atmosphere; Stage #3: With hydrogenchloride In 2-methyltetrahydrofuran; water at 0 - 20℃; | 85% |
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; potassium acetate; palladium diacetate; tris-(o-tolyl)phosphine In 1-methyl-pyrrolidin-2-one at 110℃; for 4h; Schlenk technique; Inert atmosphere; | 85% |
4-methoxybenzenediazonium tetrafluoroborate
phenylboronic acid
biphenyl-4-yl methanol
Conditions | Yield |
---|---|
polystyrene-supported N-heterocyclic carbene-Pd complex In ethanol at 20℃; for 12h; Suzuki-Miyaura cross-coupling; | 84% |
Conditions | Yield |
---|---|
With sodium hydroxide In water at 20℃; for 12h; Suzuki-Miyaura Coupling; Inert atmosphere; Green chemistry; | 84% |
With potassium carbonate In water at 70℃; for 12h; Catalytic behavior; Temperature; Reagent/catalyst; Suzuki Coupling; Green chemistry; | 100 %Chromat. |
Conditions | Yield |
---|---|
Stage #1: 4'-biphenyl chloride With n-Butyl chloride; iodine; magnesium In tetrahydrofuran at 60℃; for 2h; Inert atmosphere; Reflux; Stage #2: bromethyl methyl ether In tetrahydrofuran at -20 - 20℃; for 3h; Inert atmosphere; Stage #3: With hydrogen bromide In tetrahydrofuran at 0 - 10℃; | 84% |
4-bromo-1,1'-biphenyl
chloromethyl trimethylsilyl ether
biphenyl-4-yl methanol
Conditions | Yield |
---|---|
Stage #1: 4-bromo-1,1'-biphenyl With n-Butyl chloride; iodine; magnesium In 2-methyltetrahydrofuran at 60℃; for 2h; Inert atmosphere; Reflux; Stage #2: trimethylsilyl chloromethyl ether In 2-methyltetrahydrofuran at -20 - 20℃; for 3h; Inert atmosphere; | 83% |
Conditions | Yield |
---|---|
Stage #1: 4'-biphenyl chloride With n-Butyl chloride; iodine; magnesium In tetrahydrofuran at 60℃; for 2h; Inert atmosphere; Reflux; Stage #2: C6H11ClO2 In tetrahydrofuran at -20 - 20℃; for 3h; Inert atmosphere; Stage #3: With hydrogenchloride In tetrahydrofuran; water at 0 - 20℃; | 83% |
Conditions | Yield |
---|---|
Stage #1: 4-bromo-1,1'-biphenyl With n-Butyl chloride; iodine; magnesium In tetrahydrofuran at 60℃; for 2h; Inert atmosphere; Reflux; Stage #2: chloromethyl methyl ether In tetrahydrofuran at -20 - 20℃; for 3h; Inert atmosphere; Stage #3: With hydrogen bromide In tetrahydrofuran at 0 - 10℃; | 81% |
biphenyl-4-methylchloride
potassium carbonate
A
di(biphenyl-4-ylmethyl)carbonate
B
biphenyl-4-yl methanol
Conditions | Yield |
---|---|
With 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate at 110℃; for 36h; | A 80% B 2% |
Conditions | Yield |
---|---|
With potassium phosphate; water; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate In 1,4-dioxane at 20℃; Heating / reflux; | 80% |
Conditions | Yield |
---|---|
Stage #1: triallyl(phenyl)silane With tetrabutyl ammonium fluoride In water; dimethyl sulfoxide at 20℃; for 1h; Stage #2: 4-bromobenzenemethanol With tricyclohexylphosphine; palladium dichloride In water; dimethyl sulfoxide at 80℃; for 4h; | 79% |
Conditions | Yield |
---|---|
Stage #1: 4-iodo-benzyl alcohol With dilithium tetra(tert-butyl)zincate In tetrahydrofuran at 20℃; for 2h; Stage #2: iodobenzene With tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 20℃; for 18h; | 73% |
Stage #1: 4-iodo-benzyl alcohol With dilithium tetra(tert-butyl)zincate In tetrahydrofuran at -78 - 20℃; Inert atmosphere; Stage #2: iodobenzene With tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at -78 - 20℃; Inert atmosphere; chemoselective reaction; | 73% |
Conditions | Yield |
---|---|
With cesium fluoride In N,N-dimethyl-formamide at 70℃; | A 21% B 2% C 70% |
[1,1'-biphenyl]-4-ylmethyl methanesulfonate
biphenyl-4-yl methanol
Conditions | Yield |
---|---|
Multistep reaction; | 70% |
biphenyl-4-yl methanol
trichloroacetonitrile
4-phenylbenzyl trichloroacetimidate
Conditions | Yield |
---|---|
With tetra(n-butyl)ammonium hydrogensulfate; potassium hydroxide In dichloromethane; water at 0 - 25℃; | 100% |
Stage #1: biphenyl-4-yl methanol With sodium hydride In diethyl ether; oil at 20℃; for 0.0833333h; Stage #2: trichloroacetonitrile In diethyl ether; oil at 20℃; for 2h; | 97% |
With sodium hydride In diethyl ether 1.) 20 min, 2.) r.t., 1 h; | 69% |
Conditions | Yield |
---|---|
With n-butyltriphenylphosphonium permanganate In acetonitrile at 20℃; for 0.25h; | 100% |
With silica-supported Jones reagent In dichloromethane for 0.00269444h; | 99.7% |
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; N-methyl-N-[3-(4'-diacetoxyiodo)phenoxy-1-propyl]pyrrolidinium 4-methylbenzenesulfonate In dichloromethane at 20℃; for 6h; | 99% |
methyl 2-isocyanatobenzoate
biphenyl-4-yl methanol
methyl 2-({[(4-biphenylylmethyl)oxy]carbonyl}amino)benzoate
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; Heating / reflux; | 100% |
biphenyl-4-yl methanol
4-(azidomethyl)-1,1'-biphenyl
Conditions | Yield |
---|---|
Stage #1: biphenyl-4-yl methanol With 1,2-Diiodoethane; N,N-dimethyl-formamide; triphenylphosphine at 20℃; for 0.0166667h; Sealed tube; Inert atmosphere; Stage #2: With sodium azide at 20℃; Sealed tube; Inert atmosphere; | 100% |
With 2-azido-1,3-dimethyl-4,5-dihydro-1H-imidazol-3-ium hexafluorophosphate (V); 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran at 20℃; for 0.166667h; | 93% |
biphenyl-4-yl methanol
N-benzoyloxybenzotriazole
[1,1'-biphenyl]-4-ylmethyl benzoate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; | 100% |
Conditions | Yield |
---|---|
Stage #1: biphenyl-4-yl methanol With 1,2-Diiodoethane; N,N-dimethyl-formamide; triphenylphosphine at 50℃; for 0.0166667h; Sealed tube; Inert atmosphere; Stage #2: N-methylaniline at 50℃; Sealed tube; Inert atmosphere; | 100% |
sodium benzoate
biphenyl-4-yl methanol
[1,1'-biphenyl]-4-ylmethyl benzoate
Conditions | Yield |
---|---|
Stage #1: biphenyl-4-yl methanol With 1,2-Diiodoethane; N,N-dimethyl-formamide; triphenylphosphine at 20℃; for 0.0166667h; Sealed tube; Inert atmosphere; Stage #2: sodium benzoate at 20℃; Sealed tube; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With silica-supported Jones reagent In dichloromethane for 0.035h; | 99.5% |
With diethylene glycol dimethyl ether at 70℃; for 0.583333h; Sonication; | 96% |
With sodium tetrahydroborate; 1% Pd/C; water; potassium hydroxide In methanol at 20℃; for 6h; In air; | 89% |
Conditions | Yield |
---|---|
Stage #1: biphenyl-4-yl methanol With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tert-butylhypochlorite In dichloromethane at 20℃; for 2h; Inert atmosphere; Stage #2: With ammonia; iodine In dichloromethane; water at 20℃; for 2h; Inert atmosphere; | 99% |
With ammonia; oxygen In tert-Amyl alcohol; water at 100℃; under 3750.38 Torr; for 6h; Autoclave; High pressure; | 99% |
With 1,4-diaza-bicyclo[2.2.2]octane; TEMPOL; ammonia; copper(l) chloride In water; acetonitrile at 20℃; for 24h; | 91% |
biphenyl-4-yl methanol
potassium acetate
[1,1’-biphenyl]-4-ylmethyl acetate
Conditions | Yield |
---|---|
Stage #1: biphenyl-4-yl methanol With 1,2-Diiodoethane; N,N-dimethyl-formamide; triphenylphosphine at 20℃; for 0.0166667h; Sealed tube; Inert atmosphere; Stage #2: potassium acetate at 20℃; Sealed tube; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With potassium hydroxide In diethyl ether at 20℃; for 12h; | 99% |
biphenyl-4-yl methanol
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
With fluorosulfonyl fluoride; caesium carbonate at 20℃; for 12h; Reagent/catalyst; Sealed tube; | 99% |
Conditions | Yield |
---|---|
With potassium tert-butylate In toluene at 120℃; for 3h; Inert atmosphere; | 99% |
With [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; potassium tert-butylate In toluene at 120℃; for 18h; Inert atmosphere; Sealed tube; | 73% |
Conditions | Yield |
---|---|
With bromine; triphenylphosphine In dichloromethane at -78 - 20℃; for 18h; Inert atmosphere; | 98% |
With bromine; triphenylphosphine In dichloromethane at -78 - 25℃; for 18h; | 97% |
With carbon tetrabromide; triphenylphosphine In dichloromethane at 20℃; for 1.5h; | 95% |
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; potassium tert-butylate; nickel diacetate In 1,4-dioxane; toluene at 80℃; for 12h; Inert atmosphere; Glovebox; Schlenk technique; | 98% |
With [2,2]bipyridinyl; (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); potassium tert-butylate at 140℃; for 18h; | 89% |
With potassium tert-butylate In 1,3,5-trimethyl-benzene at 164℃; for 6h; | 75% |
biphenyl-4-yl methanol
[1,1'-biphenyl]-4-ylmethyl benzoate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; | 98% |
biphenyl-4-yl methanol
sodium phenoxide
1-phenyl-4-phenoxymethylbenzene
Conditions | Yield |
---|---|
Stage #1: biphenyl-4-yl methanol With 1,2-Diiodoethane; N,N-dimethyl-formamide; triphenylphosphine at 20℃; for 0.0166667h; Sealed tube; Inert atmosphere; Stage #2: sodium phenoxide at 20℃; Sealed tube; Inert atmosphere; | 98% |
biphenyl-4-yl methanol
Conditions | Yield |
---|---|
With 3,3-dimethyl-2-nitroso-2,3-dihydrobenzo[d]isothiazole 1,1-dioxide; trifluoroacetic acid In acetonitrile at 20℃; for 0.5h; Temperature; Solvent; Sealed tube; | 98% |
5-Fluoro-4-trifluoromethyl-2-phenyloxazole
biphenyl-4-yl methanol
5-(Biphenyl-4-ylmethoxy)-2-phenyl-4-trifluoromethyl-oxazole
Conditions | Yield |
---|---|
With potassium hydroxide In 1,4-dioxane | 97% |
Conditions | Yield |
---|---|
With magnesium hydrogen sulfate at 20℃; for 4h; | 97% |
biphenyl-4-yl methanol
phenyl 2,3,4-tri-O-benzyl-6-O-[2-[(4-phenylbenzyl)oxycarbonyl]benzoyl]-1-thio-α-D-glucopyranoside
Conditions | Yield |
---|---|
With dacarbazine; dmap In dichloromethane | 97% |
biphenyl-4-yl methanol
acetic anhydride
[1,1’-biphenyl]-4-ylmethyl acetate
Conditions | Yield |
---|---|
With colloidal gold nanoparticle-supported gadolinium complex In N,N-dimethyl-formamide for 0.0166667h; Reagent/catalyst; Microwave irradiation; | 97% |
Conditions | Yield |
---|---|
With oxygen In toluene at 90℃; Sealed tube; | 97% |
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