CAS No.37794-15-3,p-(methylsulphinyl)benzaldehyde Suppliers

Shandong Mopai Biotechnology Co., LTD

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Benzaldehyde,4-(methylsulfinyl)-

Cas:37794-15-3

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Antimex Chemical Limied

hight degree of purity Application:Fine chemical intermediates, used as the main raw material for he synthesis of various pesticides, medicines, surfactants, polymer monomers, Ond Ontifungal agents

Benzaldehyde,4-(methylsulfinyl)-

Cas:37794-15-3

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BOC Sciences

We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:crystalline powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as pri

p-(methylsulphinyl)benzaldehyde

Cas:37794-15-3

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Chemlyte Solutions

factory?direct?sale Application:Fine chemical intermediates, used as the main raw material for the synthesis of various pesticides, medicines, surfactants, polymer monomers, and antifungal agents

Benzaldehyde,4-(methylsulfinyl)-

Cas:37794-15-3

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Zibo Hangyu Biotechnology Development Co., Ltd

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p-(methylsulphinyl)benzaldehyde

Cas:37794-15-3

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ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

p-(methylsulphinyl)benzaldehyde

Cas:37794-15-3

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Shanghai Yanchu chemicals Co., Ltd

mature process, custom synthesis,please emaile to check if we have in stock Application:building blocks; intermediates

4-(methylsulfinyl)benzaldehyde

Cas:37794-15-3

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Debye Scientific

Debyesci is here who supplied several kinds of chemical products to global pharmaceutical, drug discovery, agrochemical and biotechnology industries for four yearsOur key scientific leadership team has gained experience in top research and developmen

4-(Methylsulfinyl)benzaldehyde

Cas:37794-15-3

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Type:Lab/Research institutions

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Synthetic route

: 3446-89-7
4-(Methylthio)benzaldehyde

: 37794-15-3
p-methylsulfinylbenzaldehyde

Conditions

Conditions	Yield
With phthaloyl peroxide In dichloromethane at 25℃; for 8h; Schlenk technique; chemoselective reaction;	99%
Stage #1: 4-(Methylthio)benzaldehyde With aluminum (III) chloride In methanol; dichloromethane at 20℃; for 0.0166667h; Stage #2: With [bis(acetoxy)iodo]benzene In methanol; dichloromethane at 20℃; for 12h;	99%
With nitric acid; phosphorus pentoxide; silica gel In water for 0.0833333h;	97%

: 3446-90-0
4-(methylthio)benzyl alcohol

: 37794-15-3
p-methylsulfinylbenzaldehyde

Conditions

Conditions	Yield
With iodic acid In N,N-dimethyl-formamide at 60℃; for 2h; Inert atmosphere;	96%
With chromium(VI) oxide; sulfuric acid at 20℃; for 1h;	90%

: p-(methanesulfinyl)benzaldehyde dimethylacetal

: 37794-15-3
p-methylsulfinylbenzaldehyde

Conditions

Conditions	Yield
With sulfuric acid In tetrahydrofuran for 1.5h; Ambient temperature;	91%

: 3446-90-0
4-(methylthio)benzyl alcohol

A: 37794-15-3
p-methylsulfinylbenzaldehyde

B: 93183-64-3, 106732-70-1
(4-(methylsulfinyl)phenyl)methanol

Conditions

Conditions	Yield
With sodium bromate; ammonium cerium(IV) nitrate; silica gel In dichloromethane at 20℃; for 0.5h;	A 5% B 75%

: 93033-60-4
(E)-4-(methylthio)benzaldehyde oxime

A: 4-(methylsulfinyl)benzaldehyde oxime

B: 37794-15-3
p-methylsulfinylbenzaldehyde

C: 53147-98-1
4-(methylsulfonyl)benzaldehyde oxime

D: 3446-89-7
4-(Methylthio)benzaldehyde

Conditions

Conditions	Yield
With dihydrogen peroxide; bis(acetylacetonato)dioxidomolybdenum(VI) In acetone at 20℃; Product distribution; Further Variations:; Catalysts; Solvents;	A 5% B 3% C 3% D 60%

...Expand

: 3446-90-0
4-(methylthio)benzyl alcohol

A: 37794-15-3
p-methylsulfinylbenzaldehyde

B: 3446-89-7
4-(Methylthio)benzaldehyde

Conditions

Conditions	Yield
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical In n-heptane at 80℃; under 760.051 Torr; for 24h;	A 21% B 59%
With polystyrene-supported hypervalent iodine(V) reagent In 1,2-dichloro-ethane at 85℃; for 1h;
With N-(2-iodylphenyl)glutarylamide supported on amonomethylpolystyrene resin In 1,2-dichloro-ethane at 85℃; for 1h;	A 7 %Spectr. B 85 %Spectr.

: 3446-89-7
4-(Methylthio)benzaldehyde

A: 5398-77-6
para-methanesulfonylbenzaldehyde

B: 37794-15-3
p-methylsulfinylbenzaldehyde

Conditions

Conditions	Yield
With dihydrogen peroxide at 50℃; for 4h;	A 33% B 53%
With potassium bromide In water; acetonitrile at 20℃; for 24h;
With C68H108N4O44H(1+)Mo8O26(4-); dihydrogen peroxide In water; acetonitrile at 20℃; for 0.666667h; Overall yield = 78 %;
With oxygen; isobutyraldehyde In acetonitrile for 10h; Overall yield = 95.6 percent;

: 3446-90-0
4-(methylthio)benzyl alcohol

A: 37794-15-3
p-methylsulfinylbenzaldehyde

B: 93183-64-3, 106732-70-1
(4-(methylsulfinyl)phenyl)methanol

C: 3446-89-7
4-(Methylthio)benzaldehyde

Conditions

Conditions	Yield
With 1-iodyl-2-butoxybenzene In acetonitrile for 15h; Heating;	A 16% B 46% C 32%
With 4-(2-iodylphenoxy)butanoylaminomethylated polystyrene In 1,2-dichloro-ethane for 3h; Heating;

...Expand

: 65935-99-1
4-Methanesulfinyl-thiobenzoic acid S-p-tolyl ester

: 37794-15-3
p-methylsulfinylbenzaldehyde

Conditions

Conditions	Yield
In benzene Irradiation;

: 1442-06-4
4-(methylthio)benzoyl chloride

: 37794-15-3
p-methylsulfinylbenzaldehyde

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: Py 2: aq. H2O2 3: benzene / Irradiation View Scheme

: 65935-84-4
4-Methylsulfanyl-thiobenzoic acid S-p-tolyl ester

: 37794-15-3
p-methylsulfinylbenzaldehyde

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: aq. H2O2 2: benzene / Irradiation View Scheme

: 7722-84-1
dihydrogen peroxide

: 3446-89-7
4-(Methylthio)benzaldehyde

A: 5398-77-6
para-methanesulfonylbenzaldehyde

B: 37794-15-3
p-methylsulfinylbenzaldehyde

Conditions

Conditions	Yield
With sodium dithionite In formic acid; toluene

...Expand

: 180143-69-5
4-methylthiobenzaldehyde ethylene acetal

: 2-[4-(methylsulfinyl)phenyl]-1,3-dioxolane

B: 37794-15-3
p-methylsulfinylbenzaldehyde

C: 3446-89-7
4-(Methylthio)benzaldehyde

D: 184908-97-2
2-(4-(methylsulfonyl)phenyl)-1,3-dioxolane

Conditions

Conditions	Yield
With C62H52ClFeN2O2; dihydrogen peroxide In water at 0℃; for 6h; enantioselective reaction;	A 92 %Spectr. B n/a C n/a D 5 %Spectr.

...Expand

: 37794-15-3
p-methylsulfinylbenzaldehyde

: 3446-89-7
4-(Methylthio)benzaldehyde

Conditions

Conditions	Yield
With indium; tungsten(VI) chloride In tetrahydrofuran at 20℃; for 0.0833333h;	95%
With niobium pentachloride; sodium iodide In acetonitrile at 20℃; for 0.0833333h;	95%
With iododioxobis(triphenylphosphine)rhenium(V); phenylsilane In tetrahydrofuran at 20℃; for 2.25h; chemoselective reaction;	92%

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 37794-15-3
p-methylsulfinylbenzaldehyde

: 1360628-14-3
4-(4,4,5,5-tetramethyl-1,3-dioxolan-2-yl)phenyl methyl sulfide

Conditions

Conditions	Yield
With [MoO2Cl2(dmf)2] at 90℃; for 2h; Neat (no solvent); chemoselective reaction;	89%

: 37794-15-3
p-methylsulfinylbenzaldehyde

: 634604-04-9
4-phenyl-1-(p-tolyl)-1H-1,2,3-triazole

: [4-(methylsulfinyl)phenyl]{2-[1-(p-tolyl)-1H-1,2,3-triazol-4-yl]phenyl}methanone

Conditions

Conditions	Yield
With tert.-butylhydroperoxide; palladium diacetate; XPhos In 1,2-dichloro-ethane at 120℃; for 24h; Sealed tube;	83%
With tert.-butylhydroperoxide; palladium diacetate; XPhos In water; 1,2-dichloro-ethane at 120℃; for 24h; Sealed tube; regioselective reaction;	66%
With tert.-butylhydroperoxide; triphenylphosphine; palladium dichloride In N,N-dimethyl-formamide at 130℃; for 25h; Catalytic behavior;	65%

: 40164-53-2
1,4-diphenyl-1-butyne

: 37794-15-3
p-methylsulfinylbenzaldehyde

: 4-[(1-phenyl-3,4-dihydronaphthalen-2-yl)thio]benzaldehyde

Conditions

Conditions	Yield
Stage #1: 1,4-diphenyl-1-butyne; p-methylsulfinylbenzaldehyde With trifluoromethylsulfonic anhydride In dichloromethane at -78 - 20℃; for 1h; Schlenk technique; Inert atmosphere; Stage #2: With triethylamine In dichloromethane at 20℃; for 2h; Schlenk technique; Inert atmosphere;	82%

: 1450-74-4
5-chloro-2-hydroxyacetophenone

: 37794-15-3
p-methylsulfinylbenzaldehyde

: 6-chloro-4'-methylsulfinyl-3-(4''-methylsulfinylbenzyl)-flavone

Conditions

Conditions	Yield
With pyrrolidine In ethanol at 80℃; for 24h;	76%

: 37794-15-3
p-methylsulfinylbenzaldehyde

: 118-93-4
o-hydroxyacetophenone

: 4'-methylsulfinyl-3-(4''-methylsulfinylbenzyl)-flavone

Conditions

Conditions	Yield
With pyrrolidine In ethanol at 80℃; for 24h;	76%

: 37794-15-3
p-methylsulfinylbenzaldehyde

: 1449549-02-3
1-(hex-1-yn-1-yloxy)-3-methylbenzene

: m-tolyl 2-(5-formyl-2-(methylthio)phenyl)hexanoate

Conditions

Conditions	Yield
With trifluorormethanesulfonic acid In neat (no solvent) at 70℃; for 6h;	75%

: 34941-91-8
2-chloro-4-fluoropyridine

: 37794-15-3
p-methylsulfinylbenzaldehyde

: 4-(((2-chloro-4-oxopyridin-1(4H)-yl)methyl)thio)benzaldehyde

Conditions

Conditions	Yield
With trifluoromethylsulfonic anhydride In dichloromethane at -43 - 20℃; for 10h; Schlenk technique;	71%

: 37794-15-3
p-methylsulfinylbenzaldehyde

: 107-21-1
ethylene glycol

: 2-(4-(methylsulfinyl)phenyl)-1,3-dioxolane

Conditions

Conditions	Yield
With toluene-4-sulfonic acid In toluene for 16h; Inert atmosphere; Dean-Stark; Reflux;	66%

: 37794-15-3
p-methylsulfinylbenzaldehyde

: 31405-69-3
2’-hydroxy-5’-(methoxymethoxy)acetophenone

: 6-methoxymethoxy-4'-methylsulfinyl-3-(4''-methylsulfinylbenzyl)-flavone

Conditions

Conditions	Yield
With pyrrolidine In ethanol at 80℃; for 24h;	65%

: 37794-15-3
p-methylsulfinylbenzaldehyde

: 82192-57-2
triisopropyl(prop-1-ynyl)silane

: 4-(methylsulfanyl)-3-[3-(triisopropylsilyl)prop-2-yn-1-yl]benzaldehyde

Conditions

Conditions	Yield
With 2,6-dimethylpyridine; trifluoromethylsulfonic anhydride In dichloromethane at -78 - 65℃; for 16h; Inert atmosphere;	61%

: 37794-15-3
p-methylsulfinylbenzaldehyde

: 78105-28-9
4-(N,N'-dimethylamino)pyridinium-4-toluenesulfonate

: 76-05-1
trifluoroacetic acid

: (E)-1-methyl-4-(4-(methylsulfinyl)styryl)pyridin-1-ium 2,2,2-trifluoroacetate

Conditions

Conditions	Yield
Stage #1: p-methylsulfinylbenzaldehyde; 4-methyl-N-methylpyridinium p-toluenesulfonate salt With pyrrolidine In methanol for 4h; Knoevenagel Condensation; Reflux; Inert atmosphere; Stage #2: trifluoroacetic acid In acetonitrile	61%

...Expand

: 37794-15-3
p-methylsulfinylbenzaldehyde

: 51860-45-8
3-hydroxypropyltriphenylphosphonium bromide

: (E)-4-(4-(methylsulfinyl)phenyl)but-3-en-1-ol

Conditions

Conditions	Yield
Stage #1: p-methylsulfinylbenzaldehyde; 3-hydroxypropyltriphenylphosphonium bromide With lithium hexamethyldisilazane In tetrahydrofuran at -20℃; for 1h; Inert atmosphere; Stage #2: In tetrahydrofuran at -20 - 20℃; for 14h; Inert atmosphere;	57%

: 37794-15-3
p-methylsulfinylbenzaldehyde

: 96-32-2
bromoacetic acid methyl ester

: methyl 2-((4-formylphenyl)thio)acetate

Conditions

Conditions	Yield
With 1-(n-butyl)-3-methylimidazolium triflate at 100℃; for 48h;	55%

: 420-04-2
CYANAMID

: 37794-15-3
p-methylsulfinylbenzaldehyde

: N-[(4-formylphenyl)(methyl)(oxo)-λ6-sulfanylidene]cyanamide

Conditions

Conditions	Yield
Stage #1: CYANAMID; p-methylsulfinylbenzaldehyde With potassium tert-butylate In water for 0.166667h; Sealed tube; Stage #2: With N-chloro-succinimide In water at 20℃; for 2h; Sealed tube;	54%

: 1072-72-6
Tetrahydrothiopyran-4-one

: 37794-15-3
p-methylsulfinylbenzaldehyde

: 62041-00-3
3,5-Bis-[1-(4-methanesulfinyl-phenyl)-meth-(Z)-ylidene]-tetrahydro-thiopyran-4-one

Conditions

Conditions	Yield
With piperidine; acetic acid In ethanol Heating;	50%

: 37794-15-3
p-methylsulfinylbenzaldehyde

: 431-03-8
dimethylglyoxal

: 2380-36-1
3,5-di-tert-butylaniline

: 1,4-bis(3,5-di-(tert-butyl)phenyl)-2,5-bis(4-(methylsulfinyl)phenyl)-1,4-dihydropyrrolo[3,2-b]pyrrole

Conditions

Conditions	Yield
Stage #1: p-methylsulfinylbenzaldehyde; 3,5-di-tert-butylaniline In acetic acid; toluene at 50℃; for 1h; Stage #2: dimethylglyoxal With iron(III) perchlorate hydrate In acetic acid; toluene at 50℃;	45%

...Expand

: 29943-42-8
Tetrahydro-4H-pyran-4-one

: 37794-15-3
p-methylsulfinylbenzaldehyde

: 62513-36-4
3,5-Bis-[1-(4-methanesulfinyl-phenyl)-meth-(E)-ylidene]-tetrahydro-pyran-4-one

Conditions

Conditions	Yield
With piperidine; acetic acid In ethanol Heating;	43%

: 37794-15-3
p-methylsulfinylbenzaldehyde

A: (R)-4-(methylsulfinyl)benzaldehyde

B: 3446-89-7
4-(Methylthio)benzaldehyde

Conditions

Conditions	Yield
With DL-dithiothreitol; methionine sulfoxide reductase A from Pseudomonas alcaliphila In aq. phosphate buffer at 30℃; for 1h; pH=8; Resolution of racemate; Enzymatic reaction; enantioselective reaction;	A 43% B n/a
With recombinant methionine sulfoxide reductase A from Pseudomonas monteilii; diothiothreitol In aq. phosphate buffer at 30℃; for 4h; pH=8; Sealed tube; Resolution of racemate; Green chemistry; Enzymatic reaction; enantioselective reaction;	A n/a B n/a

: 372-48-5
2-fluoropyridine

: 37794-15-3
p-methylsulfinylbenzaldehyde

: 1-(((4-formylphenyl)thio)methyl)pyridin-2-one

Conditions

Conditions	Yield
Stage #1: 2-fluoropyridine; p-methylsulfinylbenzaldehyde With trifluoromethylsulfonic anhydride In dichloromethane at -43 - 20℃; for 10h; Schlenk technique; Stage #2: With water; sodium hydrogencarbonate at 20℃; for 0.166667h;	40%

: 37794-15-3
p-methylsulfinylbenzaldehyde

: 159152-14-4
5-(mesityl)dipyrromethane

: 10-(4-methylsulfoxyphenyl)-5,15-dimesitylcorrole

Conditions

Conditions	Yield
Stage #1: p-methylsulfinylbenzaldehyde; 5-(mesityl)dipyrromethane With trifluoroacetic acid In dichloromethane at 20℃; for 5h; Stage #2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone In dichloromethane; toluene at 20℃; for 0.25h; Further stages.;	21%

: 109-97-7
pyrrole

: 37794-15-3
p-methylsulfinylbenzaldehyde

: (5Z,10Z,14Z,19Z)-5,10,15,20-Tetrakis-(4-methanesulfinyl-phenyl)-porphyrin

Conditions

Conditions	Yield
With propionic acid at 150℃; for 1h;	20%

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