GuangZhou Medcan Pharmatech LTD.is a high-tech company engaged in new biopharmaceutical product development, sales, genetic engineering, bioinformatics and other areas of research and development, registered capital of 16660,000 RMB, the company h
Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; ...... Appearance:White or almost white crystalline powder Storage:0-6°C Packag
Cas:53716-49-7
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inquiryHebei yanxi chemical co. LTD. has expanded a compositive entity from initially only as a small manufacturer. The company dedicated to the development, production and marketing of chemicals. After many years of efforts, we have established stable
APIs Appearance:White Crystalline Powder Storage:0-6°C Package:25kg/drum or acc to customers' request Application:antiinflammatory, analgesic; Carprofen is a non steroidal anti-inflammatory that is used by veterinarians for the relief of arthritic
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inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Chinese Name: Carlofen Chinese synonyms: (+/-) -6-chloro-alpha-methyl carbazole-2-acetic acid; carlofen; caprofen; carlofen (FDA); 2-(6-chloro-9H-carbazole-2-yl) propionic acid; lofen; carlofen solution, 100PPM; 6-chloro-_-methyl-9H-ca
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:53716-49-7
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiryProduct name:Carprofen CAS#:53716-49-7 Molecular formula:C15H12ClNO2 Purity:99% min Appearance:Off-White Crystalline Appearance:White powder Storage:Store in cool and dry place, away from sun light. Package:drum Application:pharmaceutical
Appearance:White or almost white crystalline powder Storage:R.T Package:25kg/drum Application:Anti-inflammatory and analgesic Transportation:Express/Sea/Air Port:Any port in China
Cas:53716-49-7
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inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:powder Storage:Store in sealed containers at cool & dry pla
Cas:53716-49-7
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:53716-49-7
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inquiryWe are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery
Cas:53716-49-7
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present,
Cas:53716-49-7
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Type:Trading Company
inquiryCarprofen CAS:53716-49-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates,
Cas:53716-49-7
Min.Order:1 Gram
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
Cas:53716-49-7
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inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s
1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France etc. 3) OEM/ODM Available; 4) Reasonable & Compet
Cas:53716-49-7
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inquiryOur Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Hubei Yuanmeng Biological Technology Co., Ltd., which is located in Wuhan, China. We are specializing in the exportation of APIs, and plant extracts ect. Our products has been exported to America, Australia, Brazil, the Europe, Middle East and other
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inquiry2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
With sodium hydroxide In methanol at 80℃; for 1.5h; | 92% |
ethyl 2-(6-chloro-9H-carbazol-2-yl)propanoate
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
With water; sodium hydroxide In methanol at 20℃; for 8h; Inert atmosphere; Schlenk technique; | 91% |
With sodium hydroxide In methanol; water | 52% |
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
With triphenylphosphine; palladium dichloride; sodium t-butanolate In N,N-dimethyl-formamide at 100℃; for 10h; Reagent/catalyst; Inert atmosphere; | 91% |
Stage #1: 2-(3-((4-chlorophenyl)amino)-4-chlorophenyl)propanoic acid With triphenylphosphine; nickel dichloride; palladium dichloride; sodium t-butanolate In N,N-dimethyl-formamide at 100℃; for 10h; Inert atmosphere; Stage #2: With acetic acid In N,N-dimethyl-formamide at 20℃; for 0.166667h; | 87.9% |
With triphenylphosphine; nickel dichloride; palladium dichloride; sodium t-butanolate In N,N-dimethyl-formamide at 100℃; for 10h; Reagent/catalyst; Inert atmosphere; | 87.9% |
With triphenylphosphine; nickel dichloride; palladium dichloride; sodium t-butanolate In N,N-dimethyl-formamide at 100℃; for 10h; Inert atmosphere; | 87.9% |
methyl (2RS)-2-(6-chloro-9H-carbazol-2-yl)propanoate
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
With water; sodium hydroxide In methanol at 50℃; | 90% |
With sodium hydroxide In water for 4h; Reflux; | 88% |
With potassium hydroxide for 1.5h; Heating; Yield given; |
B
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
Stage #1: 2-(3-((4-chlorophenyl)amino)-4-aminophenyl)propionic acid With toluene-4-sulfonic acid; orthoformic acid triethyl ester; copper(l) chloride In tetrahydrofuran; methanol for 0.5h; Stage #2: With sodium nitrite In tetrahydrofuran; methanol at 35 - 40℃; for 1h; | A 88.2% B 11.5% |
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
With hydrogenchloride In water at 20 - 60℃; for 1.5h; pH=3; | 82.7% |
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
With pyridine hydrochloride at 200℃; for 1h; Inert atmosphere; | 81.8% |
2-(1-cyanoethyl)-6-chlorocarbazole
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
With sodium hydroxide In ethylene glycol at 180 - 185℃; for 2.5h; | 75.9 g |
2-(6-Chloro-9H-carbazol-2-yl)-2-trimethylsilanyloxy-propionitrile
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
With hydrogenchloride; acetic acid; tin(ll) chloride 1.) 10 min, 2a.) RT, 18 h, 2b.) 100 deg C, 2.5 h; Yield given. Multistep reaction; |
(6-chloro-2-carbazolyl)methylmalonic acid diethyl ester
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
With hydrogenchloride In acetic acid |
(6-chloro-1,2,3,4-tetrahydro-2-carbazolyl)methylmalonic acid diethyl ester
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Cl2 / toluene / 4 h / 75 °C / 450.04 Torr 2: HCl / acetic acid View Scheme |
2-acetylcarbazole
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 1.) (EtO)3PO, BF3*Et2O, 2.) trichloroisocyanuric acid, (EtO)3PO / 1.) 5 deg C, 15 min, 2a.) from 0 deg C to 5 deg C, 1.0 h, 2b.) RT, 4.0 h 2: 83 percent / ZnI2 / CHCl3 / 22 h / Heating 3: 1.) SnCl2, HOAc, 2.) conc. HCl / 1.) 10 min, 2a.) RT, 18 h, 2b.) 100 deg C, 2.5 h View Scheme |
1-(2-acetylcarbazol-9-yl)ethanone
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 71 percent / trichloroisocyanuric acid / dimethylformamide / 5.5 h / Ambient temperature 2: 92 percent / NaOH / ethanol; H2O / 1.25 h / Heating 3: 83 percent / ZnI2 / CHCl3 / 22 h / Heating 4: 1.) SnCl2, HOAc, 2.) conc. HCl / 1.) 10 min, 2a.) RT, 18 h, 2b.) 100 deg C, 2.5 h View Scheme | |
Multi-step reaction with 5 steps 1: 71 percent / trichloroisocyanuric acid / dimethylformamide / 5.5 h / Ambient temperature 2: 98 percent / NaBH4, 14 N NaOH / ethanol / 2 h / Heating 3: 99.8 percent / 4-dimethylaminopyridine / ethyl acetate / 3 h / Ambient temperature 4: dimethylsulfoxide / a) 97 deg C, 2.5 mmHg, b) from 130 deg C to 132 deg C, 9.5 h 5: 75.9 g / NaOH / ethane-1,2-diol / 2.5 h / 180 - 185 °C View Scheme | |
Multi-step reaction with 5 steps 1: 71 percent / trichloroisocyanuric acid / dimethylformamide / 5.5 h / Ambient temperature 2: 98 percent / NaBH4, 14 N NaOH / ethanol / 2 h / Heating 3: 99.8 percent / 4-dimethylaminopyridine / ethyl acetate / 3 h / Ambient temperature 4: 1.) LiH / 1.) DMF, 50 deg C, 2.5 h, 2.) DMF, reflux, 5 h 5: 75.9 g / NaOH / ethane-1,2-diol / 2.5 h / 180 - 185 °C View Scheme |
9H-carbazole
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: conc. H2So4 / tetrachloroethene / 4 h / Heating 2: 71 percent / trichloroisocyanuric acid / dimethylformamide / 5.5 h / Ambient temperature 3: 92 percent / NaOH / ethanol; H2O / 1.25 h / Heating 4: 83 percent / ZnI2 / CHCl3 / 22 h / Heating 5: 1.) SnCl2, HOAc, 2.) conc. HCl / 1.) 10 min, 2a.) RT, 18 h, 2b.) 100 deg C, 2.5 h View Scheme | |
Multi-step reaction with 6 steps 1: conc. H2So4 / tetrachloroethene / 4 h / Heating 2: 71 percent / trichloroisocyanuric acid / dimethylformamide / 5.5 h / Ambient temperature 3: 98 percent / NaBH4, 14 N NaOH / ethanol / 2 h / Heating 4: 99.8 percent / 4-dimethylaminopyridine / ethyl acetate / 3 h / Ambient temperature 5: dimethylsulfoxide / a) 97 deg C, 2.5 mmHg, b) from 130 deg C to 132 deg C, 9.5 h 6: 75.9 g / NaOH / ethane-1,2-diol / 2.5 h / 180 - 185 °C View Scheme | |
Multi-step reaction with 6 steps 1: conc. H2So4 / tetrachloroethene / 4 h / Heating 2: 71 percent / trichloroisocyanuric acid / dimethylformamide / 5.5 h / Ambient temperature 3: 98 percent / NaBH4, 14 N NaOH / ethanol / 2 h / Heating 4: 99.8 percent / 4-dimethylaminopyridine / ethyl acetate / 3 h / Ambient temperature 5: 1.) LiH / 1.) DMF, 50 deg C, 2.5 h, 2.) DMF, reflux, 5 h 6: 75.9 g / NaOH / ethane-1,2-diol / 2.5 h / 180 - 185 °C View Scheme |
1-(6-chloro-9H-carbazol-2-yl)ethanone
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 83 percent / ZnI2 / CHCl3 / 22 h / Heating 2: 1.) SnCl2, HOAc, 2.) conc. HCl / 1.) 10 min, 2a.) RT, 18 h, 2b.) 100 deg C, 2.5 h View Scheme |
1-(6-chloro-9H-carbazol-2-yl)ethanol
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 99.8 percent / 4-dimethylaminopyridine / ethyl acetate / 3 h / Ambient temperature 2: dimethylsulfoxide / a) 97 deg C, 2.5 mmHg, b) from 130 deg C to 132 deg C, 9.5 h 3: 75.9 g / NaOH / ethane-1,2-diol / 2.5 h / 180 - 185 °C View Scheme | |
Multi-step reaction with 3 steps 1: 99.8 percent / 4-dimethylaminopyridine / ethyl acetate / 3 h / Ambient temperature 2: 1.) LiH / 1.) DMF, 50 deg C, 2.5 h, 2.) DMF, reflux, 5 h 3: 75.9 g / NaOH / ethane-1,2-diol / 2.5 h / 180 - 185 °C View Scheme |
6-chloro-2,9-diacetylcarbazole
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 92 percent / NaOH / ethanol; H2O / 1.25 h / Heating 2: 83 percent / ZnI2 / CHCl3 / 22 h / Heating 3: 1.) SnCl2, HOAc, 2.) conc. HCl / 1.) 10 min, 2a.) RT, 18 h, 2b.) 100 deg C, 2.5 h View Scheme | |
Multi-step reaction with 4 steps 1: 98 percent / NaBH4, 14 N NaOH / ethanol / 2 h / Heating 2: 99.8 percent / 4-dimethylaminopyridine / ethyl acetate / 3 h / Ambient temperature 3: dimethylsulfoxide / a) 97 deg C, 2.5 mmHg, b) from 130 deg C to 132 deg C, 9.5 h 4: 75.9 g / NaOH / ethane-1,2-diol / 2.5 h / 180 - 185 °C View Scheme | |
Multi-step reaction with 4 steps 1: 98 percent / NaBH4, 14 N NaOH / ethanol / 2 h / Heating 2: 99.8 percent / 4-dimethylaminopyridine / ethyl acetate / 3 h / Ambient temperature 3: 1.) LiH / 1.) DMF, 50 deg C, 2.5 h, 2.) DMF, reflux, 5 h 4: 75.9 g / NaOH / ethane-1,2-diol / 2.5 h / 180 - 185 °C View Scheme |
2-(1-acetoxyethyl)-6-chlorocarbazole
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dimethylsulfoxide / a) 97 deg C, 2.5 mmHg, b) from 130 deg C to 132 deg C, 9.5 h 2: 75.9 g / NaOH / ethane-1,2-diol / 2.5 h / 180 - 185 °C View Scheme | |
Multi-step reaction with 2 steps 1: 1.) LiH / 1.) DMF, 50 deg C, 2.5 h, 2.) DMF, reflux, 5 h 2: 75.9 g / NaOH / ethane-1,2-diol / 2.5 h / 180 - 185 °C View Scheme |
2-(6-chloro-carbazol-2-yl)-acrylic acid
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
In ethanol | 13 mg. (32.3%) |
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
With pyridine hydrochloride at 230℃; for 3h; Inert atmosphere; |
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
With pyridine hydrochloride at 200℃; for 3h; Inert atmosphere; |
recorcinol
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: iodine / tetrahydrofuran; water / 20 °C 2: triethylamine / dichloromethane / 0 - 20 °C 3: phenylmagnesium bromide / toluene; diethyl ether / -30 - 20 °C 4: cesium fluoride / acetonitrile / 12 h / 20 °C 5: potassium carbonate; palladium diacetate; Trimethylacetic acid / 24 h / Reflux 6: sodium hydroxide; water / methanol / 50 °C View Scheme |
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium carbonate; palladium diacetate; Trimethylacetic acid / 24 h / Reflux 2: sodium hydroxide; water / methanol / 50 °C View Scheme |
2-iodoresorcinol
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: triethylamine / dichloromethane / 0 - 20 °C 2: phenylmagnesium bromide / toluene; diethyl ether / -30 - 20 °C 3: cesium fluoride / acetonitrile / 12 h / 20 °C 4: potassium carbonate; palladium diacetate; Trimethylacetic acid / 24 h / Reflux 5: sodium hydroxide; water / methanol / 50 °C View Scheme |
2-iodo-1,3-phenylene bis(trifluoromethanesulfonate)
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: phenylmagnesium bromide / toluene; diethyl ether / -30 - 20 °C 2: cesium fluoride / acetonitrile / 12 h / 20 °C 3: potassium carbonate; palladium diacetate; Trimethylacetic acid / 24 h / Reflux 4: sodium hydroxide; water / methanol / 50 °C View Scheme |
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: cesium fluoride / acetonitrile / 12 h / 20 °C 2: potassium carbonate; palladium diacetate; Trimethylacetic acid / 24 h / Reflux 3: sodium hydroxide; water / methanol / 50 °C View Scheme |
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: copper(I) thiophene-2-carboxylate; triphenylphosphine; sodium azide; 1,10-Phenanthroline / N,N-dimethyl acetamide / 12 h / 100 °C / Inert atmosphere; Schlenk technique 2: sodium hydroxide / water; methanol View Scheme |
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: sulfuryl dichloride / 1,2-dichloro-ethane 2: hydrogenchloride; sodium hydroxide; sodium chloride; magnesium / tetrahydrofuran; ethanol; water 3: sulfuric acid / tetrahydrofuran 4: ethanol View Scheme |
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: hydrogenchloride; sodium hydroxide; sodium chloride; magnesium / tetrahydrofuran; ethanol; water 2: sulfuric acid / tetrahydrofuran 3: ethanol View Scheme |
methanol
2-(6-chloro-carbazol-2-yl)-propionic acid
methyl (2RS)-2-(6-chloro-9H-carbazol-2-yl)propanoate
Conditions | Yield |
---|---|
With sulfuric acid at 20℃; for 12h; | 100% |
With toluene-4-sulfonic acid for 1h; Reflux; | 99% |
With sulfuric acid | 98% |
benzyl bromide
2-(6-chloro-carbazol-2-yl)-propionic acid
benzyl 2-(3-chloro-9H-carbazol-7-yl)propionate
Conditions | Yield |
---|---|
Stage #1: 2-(6-chloro-carbazol-2-yl)-propionic acid With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 0.5h; Stage #2: benzyl bromide In N,N-dimethyl-formamide at 20℃; for 2h; | 98% |
Stage #1: 2-(6-chloro-carbazol-2-yl)-propionic acid With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 0.5h; Stage #2: benzyl bromide In N,N-dimethyl-formamide at 20℃; for 3h; | 84% |
With potassium carbonate In acetone at 20℃; |
isoniazid
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
With trichlorophosphate for 2.5h; Reflux; | 91% |
2-(6-chloro-carbazol-2-yl)-propionic acid
temozolomide
methyl (2RS)-2-(6-chloro-9H-carbazol-2-yl)propanoate
Conditions | Yield |
---|---|
With sodium carbonate In 1,4-dioxane; water at 60℃; for 6h; Sealed tube; | 88% |
sodium acetate
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
Stage #1: 2-bromo-N,N-diethylethanamine hydrobromide; 2-(6-chloro-carbazol-2-yl)-propionic acid With C11H16NPol In chloroform at 20℃; for 5h; not specified; Stage #2: sodium acetate In tetrahydrofuran; chloroform for 2h; | 87.8% |
sodium acetate
2-bromo-N,N-diethylethanamine hydrobromide
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
Stage #1: 2-bromo-N,N-diethylethanamine hydrobromide; 2-(6-chloro-carbazol-2-yl)-propionic acid With triethylamine In chloroform at 20℃; for 5h; Stage #2: sodium acetate for 2h; | 87.8% |
Stage #1: 2-bromo-N,N-diethylethanamine hydrobromide; 2-(6-chloro-carbazol-2-yl)-propionic acid With polymer bound triethylamine In chloroform at 20℃; for 5h; Stage #2: sodium acetate for 2h; | 87.8% |
2-(6-chloro-carbazol-2-yl)-propionic acid
aniline
Conditions | Yield |
---|---|
Stage #1: 2-(6-chloro-carbazol-2-yl)-propionic acid With pyridine; 1,1'-carbonyldiimidazole at 20℃; for 2h; Stage #2: aniline for 12h; Heating; | 86% |
2-(6-chloro-carbazol-2-yl)-propionic acid
ethanolamine
2-(6-chloro-9H-carbazol-2-yl)-N-(2-hydroxyethyl)propanamide
Conditions | Yield |
---|---|
Stage #1: 2-(6-chloro-carbazol-2-yl)-propionic acid With pyridine; 1,1'-carbonyldiimidazole at 20℃; for 2h; Stage #2: ethanolamine for 12h; Heating; | 85% |
2,6-dimethylphenyl isonitrile
2-(6-chloro-carbazol-2-yl)-propionic acid
1-iodo-2-((2-methylallyl)oxy)benzene
Conditions | Yield |
---|---|
Stage #1: 2-(6-chloro-carbazol-2-yl)-propionic acid With tetrabutyl-ammonium chloride; caesium carbonate In water at 80℃; for 0.5h; Stage #2: 1-iodo-2-((2-methylallyl)oxy)benzene With bis(dibenzylideneacetone)-palladium(0); catacxium A In water; toluene at 20℃; Inert atmosphere; Stage #3: 2,6-dimethylphenyl isonitrile In water; toluene at 100℃; for 2h; chemoselective reaction; | 73% |
methanesulfonamide
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
Stage #1: 2-(6-chloro-carbazol-2-yl)-propionic acid With 1,1'-carbonyldiimidazole In dichloromethane at 0 - 5℃; for 2h; Stage #2: methanesulfonamide With 1,2-diazabicyclo[5.4.0]undec-7-ene In dichloromethane for 4h; | 72% |
N-hydroxyphthalimide
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0 - 20℃; for 18h; | 68% |
With diisopropyl-carbodiimide In dichloromethane |
2-amino-3-chloropyridine
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
Stage #1: 2-(6-chloro-carbazol-2-yl)-propionic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In acetonitrile at 20℃; for 0.5h; Stage #2: 2-amino-3-chloropyridine In acetonitrile at 20℃; for 36h; | 61% |
Conditions | Yield |
---|---|
With (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile; caesium carbonate In dimethyl sulfoxide at 20℃; under 760.051 Torr; for 2h; Glovebox; Inert atmosphere; Sealed tube; Irradiation; | 60% |
Stage #1: 2-(6-chloro-carbazol-2-yl)-propionic acid With caesium carbonate In methanol at 20℃; for 1h; Inert atmosphere; Stage #2: carbon dioxide In dimethyl sulfoxide at 150℃; for 4h; Inert atmosphere; Cooling with liquid nitrogen; | 10 mg |
{(1R,2R)-cyclohexane-1,2-diamine}dichloridoplatinum(II)
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
With sodium carbonate; silver nitrate In N,N-dimethyl-formamide at 20℃; for 24h; Darkness; | 56% |
morpholine
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
With copper(l) iodide; Nb6O19(7-)*7K(1+)*H(1+)*13H2O; oxygen In dimethyl sulfoxide at 100℃; | 55% |
4-iodoanisol
2,6-dimethylphenyl isonitrile
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
Stage #1: 2-(6-chloro-carbazol-2-yl)-propionic acid With tetrabutyl-ammonium chloride; caesium carbonate In water at 80℃; for 0.5h; Inert atmosphere; Stage #2: 4-iodoanisol With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; bis(dibenzylideneacetone)-palladium(0) In water; toluene at 100℃; for 0.5h; Inert atmosphere; Stage #3: 2,6-dimethylphenyl isonitrile In water; toluene at 100℃; for 1.5h; Inert atmosphere; | 52% |
2-(6-chloro-carbazol-2-yl)-propionic acid
1-(6-chloro-9H-carbazol-2-yl)ethanol
Conditions | Yield |
---|---|
Stage #1: 2-(6-chloro-carbazol-2-yl)-propionic acid With dipotassium hydrogenphosphate; oxygen; 9-(2-mesityl)-10-methylacridinium perchlorate In chloroform at 20℃; for 72h; Schlenk technique; Irradiation; Green chemistry; Stage #2: With sodium tetrahydroborate In methanol; chloroform for 0.5h; Green chemistry; | 51% |
3-methylpyridin-2-ylamine
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
Stage #1: 2-(6-chloro-carbazol-2-yl)-propionic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In acetonitrile at 20℃; for 0.5h; Stage #2: 3-methylpyridin-2-ylamine In acetonitrile at 20℃; for 36h; | 44% |
2-Amino-3-bromopyridine
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
Stage #1: 2-(6-chloro-carbazol-2-yl)-propionic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In acetonitrile at 20℃; for 0.5h; Stage #2: 2-Amino-3-bromopyridine In acetonitrile at 20℃; for 36h; | 43% |
2-(6-chloro-carbazol-2-yl)-propionic acid
2-amino-3-trifluoromethylpyridine
Conditions | Yield |
---|---|
Stage #1: 2-(6-chloro-carbazol-2-yl)-propionic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In acetonitrile at 20℃; for 0.5h; Stage #2: 2-amino-3-trifluoromethylpyridine In acetonitrile at 20℃; for 36h; | 41% |
2-(6-chloro-carbazol-2-yl)-propionic acid
2-(9H-carbazol-2-yl)propanoic acid
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; hydrogen In ethanol; ethyl acetate under 760.051 Torr; | 40% |
3-iodo-2-aminopyridine
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
Stage #1: 2-(6-chloro-carbazol-2-yl)-propionic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In acetonitrile at 20℃; for 0.5h; Stage #2: 3-iodo-2-aminopyridine In acetonitrile at 20℃; for 36h; | 37% |
(OC-6-33)-(diammine)dichloridodihydroxidoplatinum(IV)
2-(6-chloro-carbazol-2-yl)-propionic acid
Conditions | Yield |
---|---|
With triethylamine; O‐(1H‐benzotriazol‐1‐yl)‐N,N,N′,N′‐tetramethyluronium tetrafluoroborate In N,N-dimethyl-formamide at 20℃; for 48h; Darkness; | 30% |
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