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inquiryProduct Description Product Name 3-Amino-3-azabicyclo[3.3.0]octane hydrochloride CAS No. 1461-97-8 Appearance Yellowish to white crystalline powder Assay ≥99% Capacity
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inquiryName 3-Amino-3-azabicyclo[3.3.0]octane hydrochloride Molecular Structure Molecular Formula C7H14N2.HCl Molecular Weight 162.66
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inquiry3-Amino-3-azabicyclo[3.3.0]octane hydrochloride Chemical Properties Melting point 170-174 °C(lit.) storage temp. Inert atmosphere,Room Temperature InChIKey WPYNXKFLSQEEFE-UHFFFAOYSA-N CAS DataBase Reference 58108-05-7(CAS DataBase R
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inquiryPacking: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Appearance:white powder/ Refer to COA Storage:Refer to COA
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inquiryN-amino-aza-3-bicyclo<3.3.0>octane
3-azabicyclo<3.3.0>oct-3-yl-amine monohydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride | 96% |
3-azabicyclo<3.3.0>oct-3-yl-amine monohydrochloride
Conditions | Yield |
---|---|
Stage #1: N-amino-1,2-cyclopentanedicarboximide With aluminum (III) chloride In tetrahydrofuran at 45℃; for 0.333333h; Large scale; Stage #2: With sodium tetrahydroborate In tetrahydrofuran for 6h; Reflux; Large scale; Stage #3: With hydrogenchloride In tetrahydrofuran pH=3; Solvent; Temperature; Large scale; | 81.3% |
Multi-step reaction with 2 steps 1: acetic acid; pyrographite; ruthenium(III) chloride trihydrate; hydrogen / water / 16 h / 140 °C / 60006 Torr / Autoclave 2: hydrogenchloride View Scheme |
gliclazide
A
toluene-4-sulfonamide
B
3-azabicyclo<3.3.0>oct-3-yl-amine monohydrochloride
Conditions | Yield |
---|---|
With chloride ions In various solvent(s) at 37℃; for 24h; Product distribution; various concentrations of anions and cations, with and without human serum proteins; |
3-azabicyclo<3.3.0>oct-3-yl-amine monohydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride; hydrazine hydrochloride In water at 140℃; under 1672.11 - 4256.29 Torr; for 5h; Autoclave; |
3-azabicyclo<3.3.0>oct-3-yl-amine monohydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride; hydrazine hydrochloride In water for 4h; Reflux; |
3-azabicyclo<3.3.0>oct-3-yl-amine monohydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride; hydrazine hydrochloride In water for 10h; Reflux; |
3-azabicyclo<3.3.0>oct-3-yl-amine monohydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride; hydrazine hydrochloride In water at 115 - 120℃; under 1140.08 - 1900.13 Torr; Autoclave; |
3-azabicyclo<3.3.0>oct-3-yl-amine monohydrochloride
4-toluenesulfonylurea
gliclazide
Conditions | Yield |
---|---|
In toluene for 3h; Reflux; | 86% |
1-(4-chlorophenyl)-2-(2,4-dichlorophenyl)-5-methyl-1H-imidazole-4-carboxylic acid
3-azabicyclo<3.3.0>oct-3-yl-amine monohydrochloride
Conditions | Yield |
---|---|
With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 16h; | 84% |
benzaldehyde
3-azabicyclo<3.3.0>oct-3-yl-amine monohydrochloride
Conditions | Yield |
---|---|
With magnesium sulfate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; | 71% |
3-azabicyclo<3.3.0>oct-3-yl-amine monohydrochloride
phenylpropyolic acid
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; for 2h; | 50% |
5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-4,5-dihydro-1H-pyrazole-3-carboxylic acid
3-azabicyclo<3.3.0>oct-3-yl-amine monohydrochloride
Conditions | Yield |
---|---|
With 1-hydroxybenzotriazol-hydrate; triethylamine In dichloromethane at 28 - 29℃; for 0.5h; | 34% |
formaldehyd
3-azabicyclo<3.3.0>oct-3-yl-amine monohydrochloride
(3aR,6aS)-cis-N-methylenehexahydrocyclopenta[c]pyrrol-2(1H)-amine
Conditions | Yield |
---|---|
With sodium acetate In water |
3-azabicyclo<3.3.0>oct-3-yl-amine monohydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: magnesium sulfate; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C 2: tris[2-phenylpyridinato-C2,N]iridium(III); lithium acetate / dimethyl sulfoxide / 0.17 h / 40 °C / Inert atmosphere; Irradiation View Scheme |
3-azabicyclo<3.3.0>oct-3-yl-amine monohydrochloride
phenyl chloroformate
phenyl hexahydrocyclopenta[c]pyrrol-2(1H)-ylcarbamate
Conditions | Yield |
---|---|
With TEA In dichloromethane at 0 - 20℃; for 3h; |
3-azabicyclo<3.3.0>oct-3-yl-amine monohydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: triethylamine / tetrahydrofuran / 2 h / 20 °C 2: copper(ll) bromide; Bathocuproine / chlorobenzene / 0.5 h / Reflux View Scheme |
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