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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

Hexyl chloroformate Manufacturer/High quality/Best price/In stock

Cas:6092-54-2

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality Hexyl Chloroformate supplier in China

Cas:6092-54-2

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

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Henan Allgreen Chemical Co.,Ltd

high quality Appearance:white powder Storage:Sealed, dry, microtherm , avoid light and smell Package:According to the demand of customer Application:Pharmaceutical intermediates Transportation:by air or by sea Port:shanghai

Carbonochloridic acid, hexyl ester

Cas:6092-54-2

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Hexyl chloroformate

Cas:6092-54-2

Min.Order:1

Negotiable

Type:Other

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Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

High Quality 99% 6092-54-2 HEXYL CHLOROFORMATE Manufacturer

Cas:6092-54-2

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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ANQING CHICO PHARMACEUTICAL CO.,LTD.

High quality. Factory supply. In stock. Best price.1.Quick response within 24 hours;2.Best quality in your requirement;?3.We pay more attention on delivery time, and usually ship on time;4.Under the premise of safety and effectiveness, we can produce

Hexyl chloroformate

Cas:6092-54-2

Min.Order:0

Negotiable

Type:Trading Company

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Chemwill Asia Co., Ltd.

Hexyl chloroformate Manufacturer Factory CAS 6092-54-2 Hexyl chloroformate Manufacturer High quality Best price In stock factory CAS 6092-54-2 Hexyl chloroformate COA TDS price MSDS HEXYL CHLOROFORMATE Chemical Properties Boiling point 60-

Hexyl chloroformate Manufacturer Factory CAS 6092-54-2

Cas:6092-54-2

Min.Order:5 Kiloliter

FOB Price: $3.5 / 5.0

Type:Manufacturers

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Jinan Finer Chemical Co., Ltd

Product Description Product website: http://www.finerchem.com/pro01en/id/840.html Product Name Hexyl chloroformate CAS No.

Hexyl chloroformate

Cas:6092-54-2

Min.Order:1 Gram

FOB Price: $23.0

Type:Lab/Research institutions

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Henan Tianfu Chemical Co., Ltd.

Competitive Price High Quality Fast Delivery custom-made Welcome to Henan Tianfu Chemical Co., Ltd. website. Our company engages in Sodium Tripolyphosphate (STPP) and Sodium Hexametabphosphate (SHMP) production; development of noble me

HEXYL CHLOROFORMATE

Cas:6092-54-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Hebei Nengqian Chemical Import and Export Co., LTD

Product Name:HEXYL CHLOROFORMATE Other Name:hexyl carbonochloridate; Carbonochloridic acid, hexyl ester; hexyl chloroformate; Chloroformic acid n-hexyl ester; hexyl chlorocarbonate; n-hexyl chloroformate; hexyloxycarbonyl chloride; hexyl alcohol, chl

HEXYL CHLOROFORMATE 6092-54-2

Cas:6092-54-2

Min.Order:1 Kilogram

FOB Price: $20.0 / 80.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Manufacturer supply CAS 6092-54-2 with best quality

Cas:6092-54-2

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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LIDE PHARMACEUTICALS LIMITED

Advantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&amp

Hexyl chloroformate/ LIDE PHARMA- Factory supply / Best price

Cas:6092-54-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Henan Sinotech Import&Export Corporation

Product name Chloroformic acid n-hexyl ester CAS 6092-54-2 EINECS 228-036-4 Product appearance Clear colorless Liquid Purity

Chloroformic acid n-hexyl ester

Cas:6092-54-2

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

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Hubei Langyou International Trading Co., Ltd

Advantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best service is

HEXYL CHLOROFORMATE CAS NO 6092-54-2

Cas:6092-54-2

Min.Order:1 Kilogram

Negotiable

Type:Other

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Carbonochloridic acid,hexyl ester 6092-54-2

Cas:6092-54-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese

Pharmaceutical Intermediates, HEXYL CHLOROFORMATE CAS:6092-54-2

Cas:6092-54-2

Min.Order:1 Kilogram

FOB Price: $148.0 / 153.0

Type:Trading Company

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Qingdao Beluga Import and Export Co., LTD

HEXYL CHLOROFORMATE CAS:6092-54-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interm

HEXYL CHLOROFORMATE CAS:6092-54-2

Cas:6092-54-2

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Carbonochloridic acid,hexyl ester

Cas:6092-54-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:6092-54-2

Cas:6092-54-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hebei Mojin Biotechnology Co.,Ltd

Hebei Mojin Biotechnology Co., Ltd, Our company is a professional chemical raw materials and chemical reagents research and development production enterprises. We have several production line,So we can control the lowest price. We also have several

Hexyl chlorocarbonate cas:6092-54-2

Cas:6092-54-2

Min.Order:25 Gram

FOB Price: $90.0 / 100.0

Type:Trading Company

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Wuhan Zenuo Biological Medicine Technology Co Ltd

Product Name: HEXYL CHLOROFORMATE Synonyms: hexylchlorocarbonate;n-Hexylchloroformate 97%;Hexyl chloroformate,98%;chlorocarbonic acid hexyl ester;hexyl carbonochloridate;Hexyl carbonochloridoate;CHLOROFORMIC ACID HEXYL ESTER;CHLOROFORMIC ACID N-

HEXYL CHLOROFORMATE Manufactory best quality

Cas:6092-54-2

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

Hexyl chloroformate

Cas:6092-54-2

Min.Order:0

Negotiable

Type:Manufacturers

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Triumph International Development Limilted

Triumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Business Custom Synthesis: Trading(Raw Mater

Carbonochloridic acid,hexyl ester

Cas:6092-54-2

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Hexyl chloroformate CAS NO.: 6092-54-2

Cas:6092-54-2

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

Hexyl chloroformate

Cas:6092-54-2

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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Afine Chemicals Limited

Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter

Hexyl chloroformate

Cas:6092-54-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Hexyl Chloroformate

Cas:6092-54-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Chemlyte Solutions

Chemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff

Featured products Carbonochloridic acid hexyl ester

Cas:6092-54-2

Min.Order:100 Gram

Negotiable

Type:Other

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Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

HEXYL CHLOROFORMATE

Cas:6092-54-2

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality Hexyl Chloroformate

Cas:6092-54-2

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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Synthetic route

bis(trichloromethyl) carbonate
32315-10-9

bis(trichloromethyl) carbonate

hexan-1-ol
111-27-3

hexan-1-ol

n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

Conditions
ConditionsYield
Stage #1: bis(trichloromethyl) carbonate With potassium carbonate; N,N-dimethyl-formamide In toluene at 0℃; for 0.5h; Inert atmosphere;
Stage #2: hexan-1-ol In toluene at 0 - 20℃; for 12h; Inert atmosphere;
83%
With pyridine In dichloromethane for 0.166667h;
With triethylamine In dichloromethane cooling;
With pyridine In dichloromethane at 0 - 20℃; for 2h;
With triethylamine In dichloromethane at 0 - 10℃; for 2h;
phosgene
75-44-5

phosgene

hexan-1-ol
111-27-3

hexan-1-ol

n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

hexan-1-ol
111-27-3

hexan-1-ol

trichloromethyl chloroformate
503-38-8

trichloromethyl chloroformate

n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

Conditions
ConditionsYield
With pyrographite In tetrahydrofuran at 20℃; for 1h; Condensation;
With dmap In toluene at 20℃; for 24h;
chloroform
67-66-3

chloroform

hexan-1-ol
111-27-3

hexan-1-ol

n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

Conditions
ConditionsYield
With oxygen at 30℃; for 3h; Irradiation;
n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

(R)-Phenylglycinol
56613-80-0

(R)-Phenylglycinol

hexyl (1R)-2-hydroxy-1-phenylethylcarbamate
532986-19-9

hexyl (1R)-2-hydroxy-1-phenylethylcarbamate

Conditions
ConditionsYield
With sodium hydrogencarbonate In 1,4-dioxane at 0℃; for 2h;99%
n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

4,6-O-benzylidene-1-O-methyl-α-D-glucopyranoside
3162-96-7

4,6-O-benzylidene-1-O-methyl-α-D-glucopyranoside

C28H42O10

C28H42O10

Conditions
ConditionsYield
With N,N,N,N,-tetramethylethylenediamine In dichloromethane at 0℃; for 1h;99%
1-methyl-2-[N-(4-amidino-phenyl)-aminomethyl]-benzimidazol-5-yl-carboxylic acid N-(2-pyridyl)-N-2-(ethoxycarbonylethyl)-amide p-toluenesulfonic acid salt
872728-85-3

1-methyl-2-[N-(4-amidino-phenyl)-aminomethyl]-benzimidazol-5-yl-carboxylic acid N-(2-pyridyl)-N-2-(ethoxycarbonylethyl)-amide p-toluenesulfonic acid salt

n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

dabigatran etexilate
211915-06-9

dabigatran etexilate

Conditions
ConditionsYield
With potassium carbonate In acetonitrile at 0℃; Reagent/catalyst; Solvent; Temperature;98.4%
With potassium carbonate In water; acetone at 12 - 25℃; for 1.5h; Solvent; Temperature; Time;17.5 g
n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

benzylamine
100-46-9

benzylamine

hexyl benzylcarbamate
1239969-89-1

hexyl benzylcarbamate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0℃; Inert atmosphere;98%
n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

4-aminobenzamidine dihydrochloride
2498-50-2

4-aminobenzamidine dihydrochloride

4-aminobenzamidine-N-hexylcarbamate hydrochloride
1307233-93-7

4-aminobenzamidine-N-hexylcarbamate hydrochloride

Conditions
ConditionsYield
Stage #1: n-hexyl chloroformate; 4-aminobenzamidine dihydrochloride With sodium hydroxide In acetone at 5 - 20℃; for 0.25h;
Stage #2: With hydrogenchloride In water
97.2%
n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

4-nitrobenzamidine
25412-75-3

4-nitrobenzamidine

p-nitrobenzamidine iminocarboxylate

p-nitrobenzamidine iminocarboxylate

Conditions
ConditionsYield
With potassium carbonate In ethyl acetate at 0℃; for 1.5h; Temperature; Time; Reagent/catalyst;96.7%
n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

(1R,2S)-1-amino-1-(3-methoxyphenyl)propan-2-ol hydrochloride

(1R,2S)-1-amino-1-(3-methoxyphenyl)propan-2-ol hydrochloride

hexyl (1R,2S)-2-hydroxy-1-(3-methoxyphenyl)propylcarbamate
289051-64-5

hexyl (1R,2S)-2-hydroxy-1-(3-methoxyphenyl)propylcarbamate

Conditions
ConditionsYield
With sodium hydrogencarbonate In tetrahydrofuran; water at 0 - 20℃; for 1h;96%
n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

phenethylamine
64-04-0

phenethylamine

hexyl phenethylcarbamate

hexyl phenethylcarbamate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0℃; Inert atmosphere;96%
n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

5-[(tert-butyldimethylsilyl)oxy]pyridin-2-amine

5-[(tert-butyldimethylsilyl)oxy]pyridin-2-amine

hexyl N-[5-[(tert-butyldimethylsilyl)oxy]pyridin-2-yl]carbamate

hexyl N-[5-[(tert-butyldimethylsilyl)oxy]pyridin-2-yl]carbamate

Conditions
ConditionsYield
With pyridine for 2h;95%
1-methyl-2-[N-[4-(1,2,4-oxadiazol-5-one-3-yl)phenyl]-amino-methyl]-benzimidazol-5-yl-carboxylic acid N-(2-pyridyl)-N-(2-ethoxycarbonylethyl)amide
872728-84-2

1-methyl-2-[N-[4-(1,2,4-oxadiazol-5-one-3-yl)phenyl]-amino-methyl]-benzimidazol-5-yl-carboxylic acid N-(2-pyridyl)-N-(2-ethoxycarbonylethyl)amide

n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

ethyl 3-(1-{2-[({4-[amino({[(hexyloxy)carbonyl]imino})methyl]phenyl}amino)methyl]-1-methyl-1H-1,3-benzodiazol-5-yl}-N-(pyridin-2-yl)formamido)propanoate
211915-06-9

ethyl 3-(1-{2-[({4-[amino({[(hexyloxy)carbonyl]imino})methyl]phenyl}amino)methyl]-1-methyl-1H-1,3-benzodiazol-5-yl}-N-(pyridin-2-yl)formamido)propanoate

Conditions
ConditionsYield
Stage #1: 1-methyl-2-[N-[4-(1,2,4-oxadiazol-5-one-3-yl)phenyl]-amino-methyl]-benzimidazol-5-yl-carboxylic acid N-(2-pyridyl)-N-(2-ethoxycarbonylethyl)amide With hydrogen; palladium 10% on activated carbon In tetrahydrofuran; water at 40℃; under 3000.3 Torr; for 0.416667h;
Stage #2: n-hexyl chloroformate With potassium carbonate In tetrahydrofuran; water at 20 - 45℃; Product distribution / selectivity;
94%
n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

6-Chloro-2-methyl-4-(4-methylsulfanyl-phenyl)-1,4-dihydro-pyrimidine-5-carboxylic acid ethyl ester
97934-95-7

6-Chloro-2-methyl-4-(4-methylsulfanyl-phenyl)-1,4-dihydro-pyrimidine-5-carboxylic acid ethyl ester

4-Chloro-2-methyl-6-(4-methylsulfanyl-phenyl)-3,6-dihydro-1λ5-pyrimidine-1,5-dicarboxylic acid 5-ethyl ester 1-hexyl ester

4-Chloro-2-methyl-6-(4-methylsulfanyl-phenyl)-3,6-dihydro-1λ5-pyrimidine-1,5-dicarboxylic acid 5-ethyl ester 1-hexyl ester

Conditions
ConditionsYield
With sodium hydride In tetrahydrofuran at 80℃; for 2h;93%
n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

benzyl (2S,3R)-3-[(2-aminopyridin-4-yl)methyl]-4-oxo-1-{[(1R)-1-phenylethyl]carbamoyl}azetidine-2-carboxylate

benzyl (2S,3R)-3-[(2-aminopyridin-4-yl)methyl]-4-oxo-1-{[(1R)-1-phenylethyl]carbamoyl}azetidine-2-carboxylate

benzyl (2S,3R)-3-[(2-{[(hexyloxy)carbonyl]amino}pyridin-4-yl)methyl]-4-oxo-1-{[(1R)-1-phenylethyl]carbamoyl}azetidine-2-carboxylate

benzyl (2S,3R)-3-[(2-{[(hexyloxy)carbonyl]amino}pyridin-4-yl)methyl]-4-oxo-1-{[(1R)-1-phenylethyl]carbamoyl}azetidine-2-carboxylate

Conditions
ConditionsYield
With pyridine In dichloromethane at 0 - 25℃; for 3.5h; Inert atmosphere;92%
n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

4-bromobenzamidine
22265-36-7

4-bromobenzamidine

C14H19BrN2O2

C14H19BrN2O2

Conditions
ConditionsYield
Stage #1: 4-bromobenzamidine With potassium carbonate In tetrahydrofuran; water at 20℃; for 0.25h;
Stage #2: n-hexyl chloroformate In tetrahydrofuran; water for 12h;
90.4%
n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

1-benzyl-N-[(4-carbamimidoylphenyl)methyl]pyrazole-4-carboxamide hydrochloride

1-benzyl-N-[(4-carbamimidoylphenyl)methyl]pyrazole-4-carboxamide hydrochloride

(Z)-hexyl amino-(4-((1-benzylpyrazole-4-carbonylamino)methyl)phenyl)methylenecarbamate
1312689-18-1

(Z)-hexyl amino-(4-((1-benzylpyrazole-4-carbonylamino)methyl)phenyl)methylenecarbamate

Conditions
ConditionsYield
With potassium carbonate In tetrahydrofuran; water at 20℃; for 1h;90%
n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

N-[(4-carbamimidoylphenyl)methyl]-1-(4-fluorophenyl)-2,5-dimethyl-pyrrole-3-carboxamide hydrochloride

N-[(4-carbamimidoylphenyl)methyl]-1-(4-fluorophenyl)-2,5-dimethyl-pyrrole-3-carboxamide hydrochloride

(Z)-hexyl amino-(4-((1-(4-fluorophenyl)-2,5-dimethyl-pyrrole-3-carbonylamino)methyl)phenyl)methylenecarbamate
1312689-19-2

(Z)-hexyl amino-(4-((1-(4-fluorophenyl)-2,5-dimethyl-pyrrole-3-carbonylamino)methyl)phenyl)methylenecarbamate

Conditions
ConditionsYield
With potassium carbonate In tetrahydrofuran; water at 20℃; for 1h;90%
n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

p-chlorobenzamidine
19563-04-3

p-chlorobenzamidine

C14H19ClN2O2

C14H19ClN2O2

Conditions
ConditionsYield
Stage #1: p-chlorobenzamidine With triethylamine In tetrahydrofuran; water at 20℃; for 0.25h;
Stage #2: n-hexyl chloroformate In tetrahydrofuran; water for 12h;
89.6%
methanesulfonic acid
75-75-2

methanesulfonic acid

1-methyl-2-[N-(4-amidino-phenyl)-aminomethyl]-benzimidazol-5-yl-carboxylic acid N-(2-pyridyl)-N-2-(ethoxycarbonylethyl)-amide p-toluenesulfonic acid salt
872728-85-3

1-methyl-2-[N-(4-amidino-phenyl)-aminomethyl]-benzimidazol-5-yl-carboxylic acid N-(2-pyridyl)-N-2-(ethoxycarbonylethyl)-amide p-toluenesulfonic acid salt

n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

[14C]-Dabigatran etexilate mesylate

[14C]-Dabigatran etexilate mesylate

Conditions
ConditionsYield
Stage #1: 1-methyl-2-[N-(4-amidino-phenyl)-aminomethyl]-benzimidazol-5-yl-carboxylic acid N-(2-pyridyl)-N-2-(ethoxycarbonylethyl)-amide p-toluenesulfonic acid salt; n-hexyl chloroformate With potassium carbonate In water; acetone at 20 - 50℃;
Stage #2: methanesulfonic acid In acetone at 30 - 36℃; for 0.333333h; Product distribution / selectivity;
89%
Stage #1: 1-methyl-2-[N-(4-amidino-phenyl)-aminomethyl]-benzimidazol-5-yl-carboxylic acid N-(2-pyridyl)-N-2-(ethoxycarbonylethyl)-amide p-toluenesulfonic acid salt; n-hexyl chloroformate With potassium carbonate In methanol at 20℃; for 3h;
Stage #2: methanesulfonic acid In water; acetone at 42℃;
n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

1-methyl-2-[N-(4-amidinophenyl)-aminomethyl]benzimidazol-5-yl-carboxylicacid-N-(2-pyridyl)-N-(2-ethoxycarbonylethyl)-amide hydrochloride

1-methyl-2-[N-(4-amidinophenyl)-aminomethyl]benzimidazol-5-yl-carboxylicacid-N-(2-pyridyl)-N-(2-ethoxycarbonylethyl)-amide hydrochloride

dabigatran etexilate
211915-06-9

dabigatran etexilate

Conditions
ConditionsYield
With triethylamine In acetone at 0 - 20℃; for 1.5h; Product distribution / selectivity; Inert atmosphere;89%
Stage #1: 1-methyl-2-[N-(4-amidinophenyl)-aminomethyl]benzimidazol-5-yl-carboxylicacid-N-(2-pyridyl)-N-(2-ethoxycarbonylethyl)-amide hydrochloride With hydrogenchloride In 2-methyltetrahydrofuran; water at 25℃; pH=3.5;
Stage #2: With potassium carbonate In 2-methyltetrahydrofuran; water at 25℃; for 0.5h;
Stage #3: n-hexyl chloroformate In 2-methyltetrahydrofuran; water at 25℃; for 2h;
83%
n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

3-Phenylpropan-1-amine
2038-57-5

3-Phenylpropan-1-amine

hexyl (3-phenylpropyl)carbamate

hexyl (3-phenylpropyl)carbamate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0℃; Inert atmosphere;89%
n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

4-phenyl-1-butylamine
13214-66-9

4-phenyl-1-butylamine

hexyl (4-phenylbutyl)carbamate

hexyl (4-phenylbutyl)carbamate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0℃; Inert atmosphere;89%
n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

4-(methoxycarbonyloxy)benzhydrol

4-(methoxycarbonyloxy)benzhydrol

n-hexyl 4-(methoxycarbonyloxy)benzhydryl carbonate

n-hexyl 4-(methoxycarbonyloxy)benzhydryl carbonate

Conditions
ConditionsYield
With pyridine at 0℃; for 1h;89%
1-methyl-2-[N-(4-amidino-phenyl)-aminomethyl]-benzimidazol-5-yl-carboxylic acid N-(2-pyridyl)-N-2-(ethoxycarbonylethyl)-amide p-toluenesulfonic acid salt
872728-85-3

1-methyl-2-[N-(4-amidino-phenyl)-aminomethyl]-benzimidazol-5-yl-carboxylic acid N-(2-pyridyl)-N-2-(ethoxycarbonylethyl)-amide p-toluenesulfonic acid salt

n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

dabigatran etexilate
211915-06-9

dabigatran etexilate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 10 - 20℃; Large scale;88.94%
With potassium carbonate In water; acetone at 15℃; Product distribution / selectivity;
5-aminomethyl-2-[(3S)-3-methyl-2,6-dioxo-piperidin-3-yl]-isoindole-1,3-dione hydrochloride
1010100-25-0

5-aminomethyl-2-[(3S)-3-methyl-2,6-dioxo-piperidin-3-yl]-isoindole-1,3-dione hydrochloride

n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

{2-[(3S)-3-methyl-2,6-dioxo-piperidin-3-yl]-1,3-dioxo-2,3-dihydro-1H-isoindol-5-ylmethyl}-carbamic acid hexyl ester

{2-[(3S)-3-methyl-2,6-dioxo-piperidin-3-yl]-1,3-dioxo-2,3-dihydro-1H-isoindol-5-ylmethyl}-carbamic acid hexyl ester

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 1h;88%
n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

3-({2-[(4-carbamimidoylphenylamino)methyl]-1-methyl-1H-benzoimidazole-5-carbonyl}pyridin-2-yl-amino)propionic acid ethyl ester

3-({2-[(4-carbamimidoylphenylamino)methyl]-1-methyl-1H-benzoimidazole-5-carbonyl}pyridin-2-yl-amino)propionic acid ethyl ester

dabigatran etexilate
211915-06-9

dabigatran etexilate

Conditions
ConditionsYield
With potassium carbonate In water; acetone at 10 - 25℃;88%
Stage #1: 3-({2-[(4-carbamimidoylphenylamino)methyl]-1-methyl-1H-benzoimidazole-5-carbonyl}pyridin-2-yl-amino)propionic acid ethyl ester With potassium carbonate In tetrahydrofuran; water at 20℃; for 0.5h;
Stage #2: n-hexyl chloroformate In tetrahydrofuran; water at 10℃; for 2h;
78%
n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

ethyl 2-{[(4-{carbamimidoyl}phenyl)amino]methyl}-1-methyl-1H-benzimidazol-5-carboxylate
1408238-41-4

ethyl 2-{[(4-{carbamimidoyl}phenyl)amino]methyl}-1-methyl-1H-benzimidazol-5-carboxylate

ethyl 2-[[4-[(n-hexyloxycarbonyl)aminoiminomethyl]phenylamino]methyl]-1-methyl-1H-benzimidazole-5-carboxylate
1408238-36-7

ethyl 2-[[4-[(n-hexyloxycarbonyl)aminoiminomethyl]phenylamino]methyl]-1-methyl-1H-benzimidazole-5-carboxylate

Conditions
ConditionsYield
With sodium hydroxide In water; acetone at 10 - 25℃;87%
n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

1-methyl-2-[N-(4-amidinophenyl)aminomethyl]benzimidazole-5-ylcarboxylic acid N-(2-pyridyl)-N-(2-ethoxycarbonylethyl)amide hydrochloride salt

1-methyl-2-[N-(4-amidinophenyl)aminomethyl]benzimidazole-5-ylcarboxylic acid N-(2-pyridyl)-N-(2-ethoxycarbonylethyl)amide hydrochloride salt

dabigatran etexilate
211915-06-9

dabigatran etexilate

Conditions
ConditionsYield
With sodium hydroxide In water; acetone at 20℃; for 1h; Reagent/catalyst;86.4%
Stage #1: 3-({2-[(4-carbamimidoyl-phenylamino)methyl]-1-methyl-1H-benzoimidazole-5-carbonyl}pyridin-2-ylamino)propionic acid ethyl ester hydrochloride With potassium carbonate In tetrahydrofuran; water at 0 - 5℃; for 0.5h;
Stage #2: n-hexyl chloroformate In tetrahydrofuran; water at 0 - 5℃;
72.7%
With triethylamine In water; acetonitrile at 15℃;
n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

p-aminobenzamidine
3858-83-1

p-aminobenzamidine

hexyl ((4-aminophenyl)(imino)methyl)carbamate

hexyl ((4-aminophenyl)(imino)methyl)carbamate

Conditions
ConditionsYield
With sodium hydroxide In acetone at 0 - 10℃;85.9%
n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

methyl (2RS)-2-(6-chloro-9H-carbazol-2-yl)propanoate
52263-88-4

methyl (2RS)-2-(6-chloro-9H-carbazol-2-yl)propanoate

hexyl 6-chloro-2-(1-methoxy-1-oxoprop-2-yl)-9H-carbazole-9-carboxylate

hexyl 6-chloro-2-(1-methoxy-1-oxoprop-2-yl)-9H-carbazole-9-carboxylate

Conditions
ConditionsYield
With dmap; triethylamine In tetrahydrofuran at 100℃; for 3h; Microwave irradiation;85%
n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

ethyl N-[(2-{[(4-carbamimidoylphenyl)amino]methyl}-1-methyl-1H-benzimidazole-5-yl)carbonyl]-N-(pyridine-2-yl)-β-alaninate bis(p-toluenesulfonic acid salt)

ethyl N-[(2-{[(4-carbamimidoylphenyl)amino]methyl}-1-methyl-1H-benzimidazole-5-yl)carbonyl]-N-(pyridine-2-yl)-β-alaninate bis(p-toluenesulfonic acid salt)

dabigatran etexilate
211915-06-9

dabigatran etexilate

Conditions
ConditionsYield
With potassium carbonate In ethanol; water; acetone at 28 - 32℃; for 0.333333h;85%
With potassium carbonate In ethanol; water; acetone at 28 - 32℃; for 0.333333h;85%
n-hexyl chloroformate
6092-54-2

n-hexyl chloroformate

4-nitrobenzamide
619-80-7

4-nitrobenzamide

4-[[[(hexyloxy)carbonyl]amino]carbonyl]nitrobenzene

4-[[[(hexyloxy)carbonyl]amino]carbonyl]nitrobenzene

Conditions
ConditionsYield
With sodium hydride In tetrahydrofuran for 2h;85%

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