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inquiryItems Result Appearance White crystalline powder Assay 99.17%(calculated as C2H5NS)
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Thioacetamide Basic information Product Name: Thioacetamide Synonyms: Acetamide, thio-;Acetimidic acid, thio-;Acetothioamide;CH3CSNH2;Rcra waste number U218;rcrawastenumberu218;Thiacetam
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inquiryAppearance & Physical State: white solid Density: 1.37 Melting Point: 112-114ºC Boiling Point: 111.7ºC at 760 mmHg Flash Point:
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inquiryThioacetamideAppearance:White or Almost White crystalline powder Storage:Store in refrigerator Package:according to customers' requirements Application:Steroids injection For Body building Transportation:By air(EMS or EUB or FedEx or TNT ect...) or b
supplier in China Appearance:white solid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:100g/bottle,1kg/bottle,25kg/drum or as per your request Application:Used in the manufacture of catalysts, stabilizing ag
Conditions | Yield |
---|---|
With Lawessons reagent In tetrahydrofuran at 20℃; for 3h; Solvent; | 93% |
With Lawessons reagent In tetrahydrofuran at 20℃; for 0.166667h; | 87% |
With Lawessons reagent for 0.0333333h; microwave irradiation; | 87% |
Conditions | Yield |
---|---|
With aluminum oxide; diethyl dithiophosphate ammonium salt for 6h; Heating; | 90% |
Stage #1: acetonitrile With calcium hydride; tiolacetic acid at 50℃; for 1h; Stage #2: With water In ethyl acetate at 20℃; | 80% |
With diammonium sulfide In methanol at 80℃; for 0.25h; microwave irradiation; | 53% |
propan-1-ol
dipropyl thioacetimidoylphosphite
A
tri-n-propyl phosphite
B
thioacetamide
Conditions | Yield |
---|---|
In benzene | A 51% B 59.1% |
Conditions | Yield |
---|---|
In acetonitrile for 4h; Heating; | A 13.3% B 54.5% |
ethylene glycol
2,4-(4-phenoxyphenyl)-1,3-dithia-2λ(5),4λ(5)-diphosphetane 2,4-disulfides
A
thioacetamide
Conditions | Yield |
---|---|
In acetonitrile for 4h; Ambient temperature; | A 53.3% B 12.3% |
dipropyl thioacetimidoylphosphite
A
dipropyl phosphorochloridite
B
thioacetamide
Conditions | Yield |
---|---|
With hydrogenchloride In benzene | A 37% B 53% |
Conditions | Yield |
---|---|
In acetonitrile for 4h; Product distribution; Mechanism; Heating; other diols; also with p-phenoxyphenyl-(LR); variation of condition; | A 37.3% B 52% C 5.6% |
In acetonitrile for 5h; Heating; | A 37.3% B 52% C 5.6% |
triethylamine
dipropyl thioacetimidoylphosphite
A
diethyl-phosphoramidous acid dipropyl ester
B
thioacetamide
Conditions | Yield |
---|---|
In benzene at 55℃; for 0.333333h; | A 36.4% B 52% |
Conditions | Yield |
---|---|
In water at 80℃; for 6h; | 45% |
2,3-dimethyl-2,3-butane diol
2,4-(4-phenoxyphenyl)-1,3-dithia-2λ(5),4λ(5)-diphosphetane 2,4-disulfides
A
thioacetamide
Conditions | Yield |
---|---|
In acetonitrile for 4h; Ambient temperature; | A 35.3% B 41.6% |
Conditions | Yield |
---|---|
In acetonitrile for 3h; Heating; | A 41.3% B 31.1% C 12.5% |
Lawessons reagent
bis-(3,5-dichloro-2-hydroxy-phenyl)-(4-nitro-phenyl)-methane
acetonitrile
A
thioacetamide
Conditions | Yield |
---|---|
for 12h; Heating; | A n/a B 37% |
Butane-1,4-diol
2,4-(4-phenoxyphenyl)-1,3-dithia-2λ(5),4λ(5)-diphosphetane 2,4-disulfides
A
thioacetamide
Conditions | Yield |
---|---|
In acetonitrile for 2h; Heating; | A 29.3% B 8.13% |
Conditions | Yield |
---|---|
In acetonitrile for 4h; Heating; | A 18.6% B 26% |
Conditions | Yield |
---|---|
In acetonitrile at 25℃; for 12h; | A 20% B 23% |
Conditions | Yield |
---|---|
With ethanol; ammonia |
Conditions | Yield |
---|---|
With aluminum sulfide at 240℃; |
Conditions | Yield |
---|---|
With diethyl ether; hydrogen sulfide |
ethanol
diethyl thioacetimidoylphosphite
A
thioacetamide
B
triethyl phosphite
Conditions | Yield |
---|---|
In benzene | A 2.5 g B 41.4 g |
Conditions | Yield |
---|---|
at 326.9℃; Kinetics; Thermodynamic data; log A, Ea; temperatures: 645.2 - 704.2 K; |
Conditions | Yield |
---|---|
at 198.9 - 250.9℃; Kinetics; Arrhenius parameters; |
N-tert-butylethanethioamide
thioacetamide
Conditions | Yield |
---|---|
at 364.9 - 425.9℃; Kinetics; Arrhenius parameters; |
thioacetamide sulfoxide
A
acetamide
B
thioacetamide
C
acetonitrile
Conditions | Yield |
---|---|
With sodium NADH*4H2O In water-d2 at 37℃; for 24h; Yield given. Yields of byproduct given; | |
With sodium NADPH In water-d2 at 37℃; for 96h; Yield given. Yields of byproduct given; |
O,O'-tetramethylene bis(hydrogen methylphosphonodithioate)
acetonitrile
thioacetamide
Conditions | Yield |
---|---|
In tetrachloromethane Ambient temperature; investigation of intermediate, stability of the product, oligomerization; |
Conditions | Yield |
---|---|
at 224.9℃; Rate constant; Thermodynamic data; Mechanism; Ea, var. temp.; |
hydrogenchloride
diethyl ether
isothiocyanatobenzene
acetonitrile
thioacetamide
Conditions | Yield |
---|---|
bei Einw. von Saeuren; |
hydrogenchloride
diethyl ether
thioacetanilide
acetonitrile
thioacetamide
Conditions | Yield |
---|---|
bei Einw. von Saeuren; |
Conditions | Yield |
---|---|
at 80℃; under 6251820 Torr; |
hydrogenchloride
diethyl ether
N-Phenylbenzothioamide
acetonitrile
A
N-phenyl benzoyl amide
B
thioacetamide
Conditions | Yield |
---|---|
bei Einw. von Saeuren; |
thioacetamide
2-Bromo-4'-methoxyacetophenone
methyl 4-(2-methyl-1,3-thiazol-4-yl)phenyl ether
Conditions | Yield |
---|---|
In ethanol for 2h; Reflux; | 100% |
In ethylene glycol at 20℃; for 0.0833333h; | 97% |
With 1,3-di-n-butyl-imidazolium tetrafluoroborate at 20℃; for 0.25h; | 96% |
2-Bromo-2',4'-dimethoxyacetophenone
thioacetamide
4-(2,4-dimethoxy-phenyl)-2-methyl-thiazole
Conditions | Yield |
---|---|
In ethanol for 2h; Heating / reflux; | 100% |
thioacetamide
5-Acetoxy-3-chloropentan-2-one
acetic acid 2-(2,4-dimethylthiazol-5-yl)-ethyl ester
Conditions | Yield |
---|---|
at 110 - 120℃; for 0.5h; | 100% |
at 110 - 120℃; for 0.5h; | 100% |
at 110 - 120℃; for 0.5h; | 100% |
3-chloro-1,6,6-trimethyl-5,6,7,8-tetrahydroisoquinoline-4-carbonitrile
thioacetamide
1-amino-5,8,8-trimethyl-6,7,8,9-tetrahydrothieno[2,3-c]isoquinoline-2-carboxamide
Conditions | Yield |
---|---|
With potassium carbonate In ethanol for 4h; Heating / reflux; | 100% |
thioacetamide
Conditions | Yield |
---|---|
With ammonium hydroxide; ammonium chloride In water NiCl2*6H2O dissolved in distilled water with NH4OH and NH4Cl buffer soln. adjusted the pH to 9.9 at 60°C; | A 0% B 100% C 0% D 0% |
With ammonium hydroxide; ammonium chloride In water NiCl2*6H2O dissolved in distilled water with NH4OH and NH4Cl buffer soln. adjusted the pH to 9.9 at 70°C; | A 0% B 100% C 0% D 0% |
With sodium hydroxide In water NiCl2*6H2O dissolved in distilled water with NaOH, thioacetamide added at 40°C, quickly mixed, boiled at 100°C for 1 h, refluxed at 60-80°C for 12 h; filtered, washed, dried at 120°C; | A 0% B 0% C 100% D 0% |
methyltriphenylbismuthonium tetrafluoroborate
thioacetamide
A
1-(methylthio)ethyleneiminium tetrafluoroborate
B
triphenylbismuthane
Conditions | Yield |
---|---|
In chloroform-d1 mixt. (Ph3BiMe)(BF4), thioacetamide, and CDCl3 was allowed to react at room temp. for 1 min; detn. by NMR; | A 100% B 100% |
1-(4-fluorophenyl)-3-(phenylsulfanyl)prop-2-yn-1-ol
thioacetamide
4-(4-fluorobenzyl)-2-methyl-5-(phenylsulfanyl)-thiazole
Conditions | Yield |
---|---|
With tetra(n-butyl)ammonium hydrogensulfate; scandium tris(trifluoromethanesulfonate) In nitromethane; water for 0.166667h; Reflux; regioselective reaction; | 100% |
thioacetamide
3-chloro-4-(bromoacetyl)nitrobenzene
Conditions | Yield |
---|---|
Stage #1: thioacetamide; 3-chloro-4-(bromoacetyl)nitrobenzene In ethanol at 85℃; for 1h; Stage #2: With hydrogenchloride; tin(II) chloride dihdyrate In ethanol; water for 1h; Reflux; Stage #3: With potassium hydroxide In ethanol; water at 0℃; | 100% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 60℃; for 1h; Hantzsch Thiazole Synthesis; Sealed tube; | 99% |
With tert-butylammonium hexafluorophosphate(V) In methanol at 20℃; for 0.25h; | 95% |
With 1,3-di-n-butyl-imidazolium tetrafluoroborate at 20℃; for 0.166667h; | 94% |
thioacetamide
3'-nitro-2-bromoacetophenone
2-methyl-4-(3-nitrophenyl)-thiazole
Conditions | Yield |
---|---|
In ethanol for 2h; Reflux; | 99% |
In ethanol for 1.5h; Heating; | 83% |
Conditions | Yield |
---|---|
With calcium oxide; palladium; triphenylphosphine In N,N-dimethyl-formamide at 60℃; for 3h; Product distribution; molar ratio of each component, 1,1'-bis(diphenylphosphino)ferrocene (dppf) ligand, reation time; | 99% |
With calcium oxide; palladium; triphenylphosphine In N,N-dimethyl-formamide at 60℃; for 3h; | 99 % Chromat. |
thioacetamide
2-[2-Bromo-3-[4-chloro-2-(2-fluorobenzoyl)phenyl]-3-oxopropyl]-1H-isoindole-1,3(2H)-dione
2-{4-[4-Chloro-2-(2-fluoro-benzoyl)-phenyl]-2-methyl-thiazol-5-ylmethyl}-isoindole-1,3-dione
Conditions | Yield |
---|---|
With sulfur dioxide In N,N-dimethyl-formamide for 1h; Heating; | 99% |
thioacetamide
(2S,3S,4S)-N-benzoyl-4-(bromoacetyl)-2-tert-butoxycarbonyl-3-tert-butoxycarbonylmethylpyrrolidine
(2S,3S,4S)-N-benzoyl-2-tert-butoxycarbonyl-3-tert-butoxycarbonylmethyl-4-(2'-methylthiazol-4'-yl)pyrrolidine
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In ethanol Condensation; Heating; | 99% |
With sodium hydrogencarbonate In ethanol for 2h; Heating; | 99% |
Conditions | Yield |
---|---|
With hydrogenchloride In 1,4-dioxane at 98℃; for 20h; | 99% |
Conditions | Yield |
---|---|
In water at 160℃; for 12h; High pressure; Autoclave; | 99% |
With layryl mercaptane In ethane-1,2-diol Sonication; thioacetamide in ethanediol heated to 65°C,, then SnCl4 in ethanediol and lauryl mercaptane added; sonicated for 0.5 h; mixt. injected into thioacetamide within 40 min; cooled down to room temp.; EtOH added; centrifuged; washed 3 times with EtOH; | |
With cetyltrimethylammonium bromide In ethanol High Pressure; cetyltrimethylammonium bromide, SnCl4*5H2O and thioacetamide added into Schlenk flask; sealed by Teflon screw cap; heated at 40, 80 or 120°C for 2, 4, 6, 8 or 10 h under inert atm.; allowed to cool naturally to room temp.; filtered out, washed with water for sseveral times; dispersed in Et2O/EtOH (1:1) via sonication, centrifuged; dried overnight under high vac. at40°C; |
thioacetamide
Conditions | Yield |
---|---|
In ethanol at 80℃; for 12h; Sealed tube; | 99% |
thioacetamide
2-bromo-3'-methoxyacetophenone
4-(3-methoxyphenyl)-2-methylthiazole
Conditions | Yield |
---|---|
In toluene for 24h; Heating / reflux; | 98.5% |
In ethanol at 80℃; for 1h; | 90% |
In ethanol at 80℃; for 1h; | 90% |
Conditions | Yield |
---|---|
In further solvent(s) Sonication; Cd salt and thioacetamide slowly dissolved 1-ethyl-3-methylimidazolium ethyl sulfate under stirring at room temp., sonicated for 60 min; centrifuged, washed 3 times (H2O, EtOH), dried at 50°C for 24 h; | 98.2% |
In water Sonication; Cd salt and thioacetamide slowly dissolved in H2O/1-ethyl-3-methylimidazolium ethyl sulfate (1:1) under stirring at room temp., sonicated for 60min; centrifuged, washed 3 times (H2O, EtOH), dried at 50°C for 24 h; | 89.8% |
In water Sonication; Cd salt and thioacetamide slowly dissolved in H2O under stirring at roomtemp., sonicated for 60 min; centrifuged, washed 3 times (H2O, EtOH), dried at 50°C for 24 h; | 82% |
thioacetamide
2-[2-Bromo-3-[4-chloro-2-(2-chlorobenzoyl)phenyl]-3-oxopropyl]-1H-isoindole-1,3(2H)-dione
2-{4-[4-Chloro-2-(2-chlorobenzoyl)phenyl-2-methyl]-5-thiazolyl-methyl}-1H-isoindole-1,3(2H)-dione
Conditions | Yield |
---|---|
With sulfur dioxide In N,N-dimethyl-formamide for 1h; Heating; | 98% |
With sulfur dioxide In methanol; dichloromethane; N,N-dimethyl-formamide |
2-Chloroacrylic acid
thioacetamide
S-(2-Carboxy-2-chlorethyl)thioacetamid-hydrochlorid
Conditions | Yield |
---|---|
With hydrogenchloride In acetonitrile for 4h; Ambient temperature; | 98% |
2-chloroacrylamide
thioacetamide
S-<2-Carbamoyl-2-chlorethyl>thioacetamid-hydrochlorid
Conditions | Yield |
---|---|
With hydrogenchloride In acetonitrile for 1h; Ambient temperature; | 98% |
Conditions | Yield |
---|---|
In 1,4-dioxane Ambient temperature; | 98% |
2-Bromo-1-(3,4-dimethoxyphenyl)ethanone
thioacetamide
4-(3,4-dimethoxyphenyl)-2-methylthiazole
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 65℃; for 8h; | 98% |
In ethanol for 2h; Reflux; Inert atmosphere; | 87% |
In N,N-dimethyl-formamide for 4h; Inert atmosphere; Reflux; | 82% |
2-bromo-1-(5-bromo-1H-pyrrolo[2,3-b]pyridin-3-yl)ethanone
thioacetamide
4-(5-bromo-1H-pyrrolo[2,3-b]pyridin-3-yl)-2-methylthiazole
Conditions | Yield |
---|---|
In tetrahydrofuran for 6h; Heating / reflux; | 98% |
4-(1-hydroxy-1,3-diphenylprop-2-ynyl)benzonitrile
thioacetamide
4-((2-methyl-5-phenylthiazol-4-yl)methyl)benzonitrile
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In 1,2-dichloro-ethane at 100℃; for 23h; Inert atmosphere; regioselective reaction; | 98% |
1,1,3-triphenylprop-2-yn-1-ol
thioacetamide
4-benzhydryl-2-methyl-5-phenylthiazole
Conditions | Yield |
---|---|
With 5 wtpercent H-USY zeolite In 1,2-dichloro-ethane at 100℃; for 16h; Concentration; | 98% |
With toluene-4-sulfonic acid In 1,2-dichloro-ethane at 100℃; for 5h; Inert atmosphere; regioselective reaction; | 90% |
1-(4-chlorophenyl)-1,3-diphenylprop-2-yn-1-ol
thioacetamide
4-((4-chlorophenyl)(phenyl)methyl)-2-methyl-5-phenylthiazole
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In 1,2-dichloro-ethane at 100℃; for 2.5h; Inert atmosphere; regioselective reaction; | 98% |
Conditions | Yield |
---|---|
In ethanol for 1h; Temperature; Solvent; Reflux; chemoselective reaction; | 98% |
In ethanol for 1h; Temperature; Reflux; | 98% |
thioacetamide
Methanesulfonyl azide
N-(methylsulfonyl)acetimidamide
Conditions | Yield |
---|---|
In ethanol for 1h; Solvent; Temperature; Reflux; chemoselective reaction; | 98% |
In water at 20℃; for 15h; Solvent; Temperature; | 63% |
thioacetamide
Conditions | Yield |
---|---|
In methanol at 20 - 70℃; for 2h; Inert atmosphere; | 98% |
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