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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

4-tert-Butylbenzenesulfonamide Manufacturer/High quality/Best price/In stock

Cas:6292-59-7

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply P-Tert-Butylbenzenesulfonamide

Cas:6292-59-7

Min.Order:1

Negotiable

Type:Other

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

4-tert-Butylbenzenesulfonamide

Cas:6292-59-7

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

4-tert-Butylbenzenesulfonamide

Cas:6292-59-7

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Factory direct supply CAS 6292-59-7 with best quality

Cas:6292-59-7

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Henan Sinotech Import&Export Corporation

Product Name Bosentan Intermediate; BUTTPARK 44\03-78;4-TERT-BUTYLBENZENESULFONAMIDE;4-TERT-BUTYLBENZENESULPHONAMIDE;4-(TERT-BUTYL)BENZENE-1-SULFONAMIDE;P-TERT-BUTYL-BENZENESULFONAMIDE;TertiaryButylBenzeneSulphon

4-tert-Butylbenzenesulfonamide CAS: 6292-59-7

Cas:6292-59-7

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

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Hubei Langyou International Trading Co., Ltd

1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:white or off-white powder Storage:Store in sealed containers

4-tert-Butylbenzenesulfonamide 6292-59-7

Cas:6292-59-7

Min.Order:100 Gram

Negotiable

Type:Other

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

4-tert-Butylbenzenesulfonamide 6292-59-7

Cas:6292-59-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

4-tert-Butylbenzenesulfonamide CAS:6292-59-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality org

4-tert-Butylbenzenesulfonamide CAS:6292-59-7

Cas:6292-59-7

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

4-tert-Butylbenzenesulfonamide

Cas:6292-59-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

4-tert-Butylbenzenesulfonamide

Cas:6292-59-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

P-Tert-Butylbenzenesulfonamide

Cas:6292-59-7

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Afine Chemicals Limited

Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter

4-tert-Butylbenzenesulfonamide

Cas:6292-59-7

Min.Order:1 Kilogram

FOB Price: $1.0 / 100000.0

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

4-tert-Butylbenzenesulfonamide

Cas:6292-59-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

4-tert-Butylbenzenesulfonamide

Cas:6292-59-7

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality Appearance:White solid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application: 4-tert-Butylbenzenesulfonamide is an intermediate as well

4-tert-Butylbenzenesulfonamide

Cas:6292-59-7

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Siwei Development Group Ltd.

Product name: 4-Tert-Butylbenzenesulfonamide CAS No.: 6292-59-7 Molecule Formula:C10H15NO2S Molecule Weight:213.30 Purity: 98.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard

Lower Price 4-Tert-Butylbenzenesulfonamide

Cas:6292-59-7

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

6292-59-7 4-tert-Butylbenzenesulfonamide

Cas:6292-59-7

Min.Order:1 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

4-tert-Butylbenzenesulfonamide

Cas:6292-59-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

4-tert-Butylbenzenesulfonamide

Cas:6292-59-7

Min.Order:1 Milligram

Negotiable

Type:Trading Company

inquiry

Shanghai Minstar Chemical Co., Ltd

4-tert-Butylbenzenesulfonamide Basic information Product Name: 4-tert-Butylbenzenesulfonamide Synonyms: BUTTPARK 44\03-78;4-TERT-BUTYLBENZENESULFONAMIDE;4-TERT-BUTYLBENZENESULPHONAMIDE;4-(TERT-BUTYL)BENZENE-1-SULFONAMIDE;P-TERT-BUTYL-BENZENESU

4-tert-Butylbenzenesulfonamide

Cas:6292-59-7

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as

4-tert-Butylbenzenesulphonamide

Cas:6292-59-7

Min.Order:0 Metric Ton

Negotiable

Type:Manufacturers

inquiry

HUNAN CHEMAPI BIOLOGICAL TECHNOLOGY CO.,LTD.

Hunan Kaimir Biotechnology Co., Ltd. is a professional technology company specializing in the research and production of raw materials and intermediates. In 2017, it was recognized as a high-tech enterprise and a small technological innovation giant

4-tert-Butylbenzenesulfonamide

Cas:6292-59-7

Min.Order:1 Metric Ton

Negotiable

Type:Other

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

4-tert-Butylbenzenesulfonamide

Cas:6292-59-7

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Zhongqi chem Co.,Ltd.

Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and h

4-tert-Butylbenzenesulfonamide

Cas:6292-59-7

Min.Order:0

Negotiable

Type:Other

inquiry

Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

4-Tert-butylbenzenesulfonamide cas no. 6292-59-7 98%

Cas:6292-59-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

4-tert-Butylbenzenesulfonamide

Cas:6292-59-7

Min.Order:0

Negotiable

Type:Other

inquiry

Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air

4-tert-Butylbenzenesulfonamide

Cas:6292-59-7

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier

4-tert-Butylbenzene sulfonamide

Cas:6292-59-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Acmec Biochemical Technology Co., Ltd.

Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea

Acmec 4-Tert-Butylbenzenesulfonamide 100g

Cas:6292-59-7

Min.Order:1 bottle

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

4-tert-butylbenzenesulfonyl chloride
15084-51-2

4-tert-butylbenzenesulfonyl chloride

4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

Conditions
ConditionsYield
With ammonium hydroxide for 72h; Ambient temperature;99%
With ammonium hydroxide In ethyl acetate at 20℃; for 1h;95%
With ammonium hydroxide In acetone at 20℃;94%
4,N-di-tert-butyl-benzenesulfonamide

4,N-di-tert-butyl-benzenesulfonamide

4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

Conditions
ConditionsYield
With scandium tris(trifluoromethanesulfonate) In nitromethane at 50℃; for 5h;96%
4-tert-Butyl-N-isopropyl-benzenesulfonamide
5636-16-8

4-tert-Butyl-N-isopropyl-benzenesulfonamide

4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

Conditions
ConditionsYield
With chromium(III) acetate hydroxide; periodic acid In acetonitrile at 20℃; for 14h;94%
(4-tert-butylphenyl)diazonium tetrafluoroborate
52436-75-6

(4-tert-butylphenyl)diazonium tetrafluoroborate

4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

Conditions
ConditionsYield
With sodium metabisulfite; sodium azide; tetrabutylammomium bromide; triphenylphosphine In water; acetonitrile at 80℃; for 12h; Inert atmosphere;84%
With sodium metabisulfite; sodium azide; tetrabutylammomium bromide; triphenylphosphine In water; acetonitrile at 80℃; for 12h; Inert atmosphere; Schlenk technique;84%
4-(tert-butyl)-N,N-diethylbenzenesulfonamide

4-(tert-butyl)-N,N-diethylbenzenesulfonamide

4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

Conditions
ConditionsYield
With chromium(III) acetate hydroxide; periodic acid In acetonitrile at 20℃; for 16h;81%
4-t-butylbenzenethiol
2396-68-1

4-t-butylbenzenethiol

4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

Conditions
ConditionsYield
With [bis(acetoxy)iodo]benzene; ammonium carbamate In methanol at 25℃; for 24h; Inert atmosphere; chemoselective reaction;80%
potassium tert-butyltrifluoroboranuide

potassium tert-butyltrifluoroboranuide

4-bromo-benzenesulfonic acid amide
701-34-8

4-bromo-benzenesulfonic acid amide

4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

Conditions
ConditionsYield
With dipotassium hydrogenphosphate; nickel(II) bis(2,2,6,6-tetramethylheptane-3,5-dionate); Ir(dF(CF3)ppy)2(bpy)PF6; zinc dibromide In N,N-dimethyl acetamide at 27℃; for 72h; Inert atmosphere; Irradiation;44%
1-tert-butyl-benzene-sulfonyl chloride-(4)

1-tert-butyl-benzene-sulfonyl chloride-(4)

ammonium carbonate

ammonium carbonate

4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

tert-butylbenzene
253185-03-4, 253185-04-5

tert-butylbenzene

4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: chlorosulfonic acid / 6 h / Reflux
2: ethanol / 1 h / 0 °C
View Scheme
4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

4,6-dichloro-5-(2-methoxyphenoxy)-2,2'-bipyrimidine
150728-13-5

4,6-dichloro-5-(2-methoxyphenoxy)-2,2'-bipyrimidine

4-tert-butyl-N-(6-chloro-5-(2-methoxyphenoxy)2,2'-bipyrimidin-4-yl)benzene sulfonamide
150727-06-3

4-tert-butyl-N-(6-chloro-5-(2-methoxyphenoxy)2,2'-bipyrimidin-4-yl)benzene sulfonamide

Conditions
ConditionsYield
Stage #1: 4-tert-butylbenzenesulphonamide; 4,6-dichloro-5-(2-methoxyphenoxy)-2,2'-bipyrimidine With potassium carbonate In acetonitrile at 25 - 83℃; Large scale reaction;
Stage #2: Large scale reaction;
100%
With potassium carbonate In dimethyl sulfoxide at 100 - 105℃;100%
Stage #1: 4-tert-butylbenzenesulphonamide With potassium carbonate In toluene at 50℃; for 0.5h; Large scale;
Stage #2: 4,6-dichloro-5-(2-methoxyphenoxy)-2,2'-bipyrimidine With tetrabutylammomium bromide In toluene at 110℃; for 10h; Large scale;
97%
4-(2-tert-butoxyethoxy)-5-(2-methoxyphenoxy)-6-chloro-2,2'-bipyrimidine
1177447-87-8

4-(2-tert-butoxyethoxy)-5-(2-methoxyphenoxy)-6-chloro-2,2'-bipyrimidine

4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

N-[6-[2-(1,1-dimethylethoxy)ethoxy]-5-(2-methoxyphenoxy)[2,2'-bipyrimidin]-4-yl]-4-(1,1-dimethylethyl)benzenesulfonamide

N-[6-[2-(1,1-dimethylethoxy)ethoxy]-5-(2-methoxyphenoxy)[2,2'-bipyrimidin]-4-yl]-4-(1,1-dimethylethyl)benzenesulfonamide

Conditions
ConditionsYield
With potassium carbonate In dimethyl sulfoxide at 120℃; for 10h;100%
4-methoxyphenethyl bromide
14425-64-0

4-methoxyphenethyl bromide

4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

C19H22O3S

C19H22O3S

Conditions
ConditionsYield
With aluminum (III) chloride; trifluorormethanesulfonic acid; niobium pentachloride; bis-[(trifluoroacetoxy)iodo]benzene; zinc(II) iodide In N,N-dimethyl acetamide at 75℃; for 2.5h; Solvent; Reagent/catalyst;97.3%
4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

4-tert-butylbenzenesulfonamide monosodium salt

4-tert-butylbenzenesulfonamide monosodium salt

Conditions
ConditionsYield
With sodium ethanolate for 2h; Heating;97%
4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

C15H11ClN4O3
1268612-27-6

C15H11ClN4O3

4-tert-butyl-N-(6-chloro-5-(2-methoxyphenoxy)2,2'-bipyrimidin-4-yl)benzene sulfonamide
150727-06-3

4-tert-butyl-N-(6-chloro-5-(2-methoxyphenoxy)2,2'-bipyrimidin-4-yl)benzene sulfonamide

Conditions
ConditionsYield
Stage #1: 4-tert-butylbenzenesulphonamide With potassium carbonate In toluene at 50℃; for 0.5h; Large scale;
Stage #2: C15H11ClN4O3 In toluene at 110℃; for 10h; Large scale;
97%
4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

4,6-dichloro-5-(2-methoxyphenoxy)-2,2'-bipyrimidine
150728-13-5

4,6-dichloro-5-(2-methoxyphenoxy)-2,2'-bipyrimidine

4-tert-butyl-N-[6-chloro-5-(2-methoxyphenoxy)-2-(2-pyrimidinyl)-4-pyrimidinyl]benzene sulfonamide potassium salt

4-tert-butyl-N-[6-chloro-5-(2-methoxyphenoxy)-2-(2-pyrimidinyl)-4-pyrimidinyl]benzene sulfonamide potassium salt

Conditions
ConditionsYield
Stage #1: 4,6-dichloro-5-(2-methoxyphenoxy)-2,2'-bipyrimidine With potassium carbonate for 0.25h;
Stage #2: 4-tert-butylbenzenesulphonamide at 140℃; for 3h; Solvent; Temperature; Time;
96.2%
Stage #1: 4-tert-butylbenzenesulphonamide With potassium hydroxide In acetone at 30℃; for 0.0833333h;
Stage #2: 4,6-dichloro-5-(2-methoxyphenoxy)-2,2'-bipyrimidine In acetone at 30℃; for 6.5h; Product distribution / selectivity; Reflux;
89%
With tetrabutylammomium bromide; potassium carbonate In toluene for 10h; Reflux;87.7%
4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

4-tert-butylbenzenesulfonamide-d2
1089215-18-8

4-tert-butylbenzenesulfonamide-d2

Conditions
ConditionsYield
With water-d2 In diethyl ether96%
4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

benzaldehyde
100-52-7

benzaldehyde

N-benzylidene-4-(tert-butyl)benzenesulfonamide

N-benzylidene-4-(tert-butyl)benzenesulfonamide

Conditions
ConditionsYield
With boron trifluoride diethyl etherate In benzene for 12h; Reflux;95%
4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

4,6-dichloro-5-(2-methoxyphenoxy)-2,2'-bipyrimidine
150728-13-5

4,6-dichloro-5-(2-methoxyphenoxy)-2,2'-bipyrimidine

4-(tert-butyl)-N-(6-chloro-5-(2-methoxyphenoxy)-(2,2'-bipyrimidine)-4-yl)benzenesulfonamide sodium salt

4-(tert-butyl)-N-(6-chloro-5-(2-methoxyphenoxy)-(2,2'-bipyrimidine)-4-yl)benzenesulfonamide sodium salt

Conditions
ConditionsYield
With sodium carbonate In dimethyl sulfoxide at 70 - 80℃; for 10h; Reagent/catalyst; Solvent; Temperature;95%
1-phenylpyrrolidin-2-one
4641-57-0

1-phenylpyrrolidin-2-one

4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

(E)-4-(tert-butyl)-N-(1-phenylpyrrolidin-2-ylidene)benzenesulfonamide

(E)-4-(tert-butyl)-N-(1-phenylpyrrolidin-2-ylidene)benzenesulfonamide

Conditions
ConditionsYield
With diazoacetic acid ethyl ester; zinc trifluoromethanesulfonate In cyclohexane for 12h; Reflux; stereoselective reaction;94%
N-methylcyclohexylamine
626-67-5

N-methylcyclohexylamine

4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

4-(tert-butyl)-N-(piperidin-1-ylmethylene)benzenesulfonamide

4-(tert-butyl)-N-(piperidin-1-ylmethylene)benzenesulfonamide

Conditions
ConditionsYield
With tetra-(n-butyl)ammonium iodide In ethanol at 20℃; for 12h; Electrochemical reaction; Inert atmosphere; regioselective reaction;94%
4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

4-methylphenylboronic acid
5720-05-8

4-methylphenylboronic acid

benzaldehyde
100-52-7

benzaldehyde

(R)-4-(tert-butyl)-N-(phenyl(p-tolyl)methyl)benzenesulfonamide

(R)-4-(tert-butyl)-N-(phenyl(p-tolyl)methyl)benzenesulfonamide

Conditions
ConditionsYield
With palladium(II) trifluoroacetate; (S,S)-4,4′-diisopropyl-4,5,4′,5′-tetrahydro[2.2]bioxazolyl In nitromethane at 40℃; for 64h; enantioselective reaction;93%
2-(5-(2-methoxy-phenoxy)-6-chloro-2-(pyrimidin-2-yl)pyrimidin-4-yloxy)ethanol acetyl ester
1160515-46-7

2-(5-(2-methoxy-phenoxy)-6-chloro-2-(pyrimidin-2-yl)pyrimidin-4-yloxy)ethanol acetyl ester

4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

2-[6-(4-tert-butyl-benzenesulfonylamino)-5-(2-methoxy-phenoxy)-[2,2']bipyrimidinyl-4-yloxy]-ethanol acetyl ester
1160515-53-6

2-[6-(4-tert-butyl-benzenesulfonylamino)-5-(2-methoxy-phenoxy)-[2,2']bipyrimidinyl-4-yloxy]-ethanol acetyl ester

Conditions
ConditionsYield
Stage #1: 4-tert-butylbenzenesulphonamide With potassium phosphate In N,N-dimethyl acetamide at 75 - 80℃; for 0.5h;
Stage #2: 2-(5-(2-methoxy-phenoxy)-6-chloro-2-(pyrimidin-2-yl)pyrimidin-4-yloxy)ethanol acetyl ester In N,N-dimethyl acetamide at 65 - 70℃; for 96h; Product distribution / selectivity;
92%
Stage #1: 4-tert-butylbenzenesulphonamide With potassium carbonate In N,N-dimethyl acetamide; acetonitrile at 75 - 80℃; for 0.5h;
Stage #2: 2-(5-(2-methoxy-phenoxy)-6-chloro-2-(pyrimidin-2-yl)pyrimidin-4-yloxy)ethanol acetyl ester In N,N-dimethyl acetamide; acetonitrile at 65 - 70℃; for 96h; Product distribution / selectivity;
75%
Stage #1: 4-tert-butylbenzenesulphonamide With potassium carbonate In dimethyl sulfoxide at 75 - 80℃; for 0.5h;
Stage #2: 2-(5-(2-methoxy-phenoxy)-6-chloro-2-(pyrimidin-2-yl)pyrimidin-4-yloxy)ethanol acetyl ester In dimethyl sulfoxide at 65 - 70℃; for 96h; Product distribution / selectivity;
60%
Stage #1: 4-tert-butylbenzenesulphonamide With potassium phosphate In N,N-dimethyl acetamide at 75 - 80℃; for 0.5h;
Stage #2: 2-(5-(2-methoxy-phenoxy)-6-chloro-2-(pyrimidin-2-yl)pyrimidin-4-yloxy)ethanol acetyl ester In ISOPROPYLAMIDE at 65 - 70℃; for 96h; Product distribution / selectivity;
diazoacetic acid ethyl ester
623-73-4

diazoacetic acid ethyl ester

4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

acetonitrile
75-05-8

acetonitrile

diethyl 2,2'-((1-(((4-(tert-butyl)phenyl)sulfonyl)imino)ethyl)azanediyl)(E)-diacetate

diethyl 2,2'-((1-(((4-(tert-butyl)phenyl)sulfonyl)imino)ethyl)azanediyl)(E)-diacetate

Conditions
ConditionsYield
With copper(II) bis(trifluoromethanesulfonate) at 80℃; for 2h;92%
diazoacetic acid ethyl ester
623-73-4

diazoacetic acid ethyl ester

4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

acetonitrile
75-05-8

acetonitrile

C20H30N2O6S

C20H30N2O6S

Conditions
ConditionsYield
With copper(II) bis(trifluoromethanesulfonate) at 80℃; for 2h;92%
4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

(E)-N'-(4-tert-butylphenylsulfonyl)-N,N-dimethylformimidamide

(E)-N'-(4-tert-butylphenylsulfonyl)-N,N-dimethylformimidamide

Conditions
ConditionsYield
With thionyl chloride In chloroform at 60℃; for 3h;91%
8-methylquinoline
611-32-5

8-methylquinoline

4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

4-(tert-butyl)-N-(quinolin-8-ylmethyl)benzenesulfonamide

4-(tert-butyl)-N-(quinolin-8-ylmethyl)benzenesulfonamide

Conditions
ConditionsYield
With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; [bis(acetoxy)iodo]benzene; sodium acetate In dichloromethane at 20℃; for 48h; Inert atmosphere; Schlenk technique;89%
4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

C34H62O6Si

C34H62O6Si

C44H75NO7SSi

C44H75NO7SSi

Conditions
ConditionsYield
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane; N,N-dimethyl-formamide at 20℃; for 3h;87%
4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

C36H68O4Si2

C36H68O4Si2

C46H81NO5SSi2

C46H81NO5SSi2

Conditions
ConditionsYield
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane; N,N-dimethyl-formamide at 20℃; for 3h;87%
4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

p-chlorphenylisocyanate
104-12-1

p-chlorphenylisocyanate

C17H19ClN2O3S
128924-62-9

C17H19ClN2O3S

Conditions
ConditionsYield
With sodium hydroxide In acetone86%
(4,4'-di-tert-butyl-2,2'-bipyridine)bis(trifluoromethanesulfonate)platinum(II)
177593-36-1

(4,4'-di-tert-butyl-2,2'-bipyridine)bis(trifluoromethanesulfonate)platinum(II)

4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

lithium tetrakis(pentafluorophenyl)borate
2797-28-6

lithium tetrakis(pentafluorophenyl)borate

[(t-Bu2-2,2'-bipyridyl)Pt(μ-NHSO2C6H4Bu-t)]2[B(C6F5)4]2

[(t-Bu2-2,2'-bipyridyl)Pt(μ-NHSO2C6H4Bu-t)]2[B(C6F5)4]2

Conditions
ConditionsYield
In dichloromethane under inert atm. to Pt complex soln. ligand and excess Li(B(C6F5)4) in CH2Cl2 was added, mixt. was stirred at room temp. for 1 h; mixt. was filtered, evapd., solid was washed 3 times with ether, dried under vac. for 4 h; elem. anal.;86%
4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

cyclohexanone
108-94-1

cyclohexanone

4-(tert-butyl)-N-phenylbenzenesulfonamide

4-(tert-butyl)-N-phenylbenzenesulfonamide

Conditions
ConditionsYield
With 1,10-Phenanthroline; palladium(II) trifluoroacetate; oxygen In toluene at 140℃; for 40h;86%
4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

4,6-dichloro-5-(2-methoxyphenyl)thiopyrimidine
374600-17-6

4,6-dichloro-5-(2-methoxyphenyl)thiopyrimidine

4-tert-butyl-N-(6-chloro-5-(2-methoxyphenyl)thio-4-pyrimidinyl)benzenesulfonamide
167403-91-0

4-tert-butyl-N-(6-chloro-5-(2-methoxyphenyl)thio-4-pyrimidinyl)benzenesulfonamide

Conditions
ConditionsYield
With potassium carbonate In dimethyl sulfoxide at 80℃; for 1h;85%
morpholine
110-91-8

morpholine

4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

(E)-4-(tert-butyl)-N-(morpholinomethylene)benzenesulfonamide

(E)-4-(tert-butyl)-N-(morpholinomethylene)benzenesulfonamide

Conditions
ConditionsYield
With copper(I) bromide In dimethyl sulfoxide at 100℃; for 24h; Schlenk technique; stereoselective reaction;85%
4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

(Z)-1-{2-[4-(tert-butyl)phenylsulfonamido]phenyl}-2-phenyldiazene oxide

(Z)-1-{2-[4-(tert-butyl)phenylsulfonamido]phenyl}-2-phenyldiazene oxide

Conditions
ConditionsYield
With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; [bis(acetoxy)iodo]benzene In 1,2-dichloro-ethane at 80℃; for 16h; regioselective reaction;84%
4-tert-butylbenzenesulphonamide
6292-59-7

4-tert-butylbenzenesulphonamide

4-(tert-butyl)benzene-1-sulfonyl fluoride

4-(tert-butyl)benzene-1-sulfonyl fluoride

Conditions
ConditionsYield
With potassium fluoride; pyrylium tetrafluoroborate; magnesium chloride In acetonitrile at 60℃; for 2h;84%

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