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inquiryDirect Manufacturer 2,6-Dimethylbenzoic acid 632-46-2 in bulk supply 2,6-dimethylbenzoic acid is a white solid powder under normal temperature and pressure. During the organic synthesis and conversion, the carboxyl group in 2,6-dimethylbenzoic acid
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Product Name: 2,6-Dimethylbenzoic acid Synonyms: M-XYLENE-2-CARBOXYLIC ACID;TIMTEC-BB SBB007881;RARECHEM AL BO 0401;VIC-M-XYLYLIC ACID;2,6-dimethyl-benzoicaci;2,6-DIMETHYLBENZOIC ACID;Benzoic acid, 2,6-dimethyl- (7CI,8CI,9CI);Benzoic acid, 2,6-di
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inquiry2,6-Dimethylbenzoic acid Chemical Properties Melting point 114-116 °C (lit.) Boiling point 160 °C / 17mmHg density 1.0937 (estimate) refractive index 1.5236 (estimate) form Crystalline Powder pka pKa: 3.362(25°C) co
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
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inquiryQ1: Are you a manufacturer Answer: Yes, we are factory founded on 2012.Q2: How to contact with us Click "contact supplier" And then send us message the product you interest in, you will get reply within 12 hours.Q3:Which kind of payment terms do you
ethylene glycol
A
2,6-dimethylbenzoic acid
B
2-(4-methoxybenzyloxy)ethanol
Conditions | Yield |
---|---|
at 140℃; for 4h; | A 96% B n/a |
Conditions | Yield |
---|---|
Stage #1: 2-Bromo-m-xylene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h; Inert atmosphere; Stage #2: carbon dioxide In tetrahydrofuran; hexane at -78 - 20℃; | 93.2% |
Stage #1: 2-Bromo-m-xylene With ethyl bromide; magnesium In diethyl ether Grignard reaction; Inert atmosphere; Reflux; Stage #2: carbon dioxide In diethyl ether at 20℃; Grignard reaction; Inert atmosphere; | 54% |
(i) Mg, (ii) /BRN= 1900390/; Multistep reaction; | |
(i) Mg, EtBr, Et2O, (ii) /BRN= 1900390/; Multistep reaction; |
carbon dioxide
2,6-dimethylbenzene boronic acid
2,6-dimethylbenzoic acid
Conditions | Yield |
---|---|
With chloro[1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]copper(I); potassium methanolate In tetrahydrofuran at 70℃; for 24h; Schlenk technique; Sealed tube; | 88% |
dicobalt octacarbonyl
2,6-dimethylphenyl trifluoromethanesulphonate
2,6-dimethylbenzoic acid
Conditions | Yield |
---|---|
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate In 1,4-dioxane; water at 50℃; for 12h; Schlenk technique; Inert atmosphere; chemoselective reaction; | 82% |
2,6-dimethyl-N-(quinolin-8-yl)benzamide
2,6-dimethylbenzoic acid
Conditions | Yield |
---|---|
With sulfuric acid; water at 120℃; for 24h; | 80% |
dicobalt octacarbonyl
2,6-dimethylbenzoic acid
Conditions | Yield |
---|---|
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate In 1,4-dioxane; water at 50℃; for 12h; Schlenk technique; Inert atmosphere; chemoselective reaction; | 79% |
ortho-methylbenzoic acid
dihydroxy-methyl-borane
2,6-dimethylbenzoic acid
Conditions | Yield |
---|---|
With dipotassium hydrogenphosphate; silver carbonate; p-benzoquinone; palladium diacetate In tert-butyl alcohol at 100℃; for 3h; | 75% |
Conditions | Yield |
---|---|
Stage #1: carbon dioxide With bis(1,5-cyclooctadiene)nickel (0); 1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene In 1,3,5-trimethyl-benzene at 20℃; under 760.051 Torr; for 0.166667h; Schlenk technique; Stage #2: C10H14Si In 1,3,5-trimethyl-benzene at 160℃; for 20h; Schlenk technique; | 58% |
Conditions | Yield |
---|---|
With silver carbonate; p-benzoquinone; palladium diacetate In tert-butyl alcohol at 100℃; for 3h; | 50% |
dihydroxy-methyl-borane
2-methylbenzoic acid potassium salt
2,6-dimethylbenzoic acid
Conditions | Yield |
---|---|
With silver carbonate; p-benzoquinone; palladium diacetate In tert-butyl alcohol at 100℃; for 3h; | 48% |
Conditions | Yield |
---|---|
With potassium acetate; palladium diacetate at 80℃; under 760.051 Torr; for 24h; | 48% |
With potassium acetate; palladium diacetate at 80℃; for 24h; Schlenk technique; | 48% |
Conditions | Yield |
---|---|
Stage #1: 2-fluoro-m-xylene With C78H70Al2Cl4N6P4Rh2; magnesium; ethylene dibromide In tetrahydrofuran at 50℃; for 22h; Inert atmosphere; Glovebox; Stage #2: carbon dioxide In tetrahydrofuran at 20℃; under 760.051 Torr; for 0.5h; | 48% |
1,2,3-trimethylbenzene
A
2,6-dimethylbenzoic acid
B
2,3-dimethylbenzoic acid
Conditions | Yield |
---|---|
With air; acetic acid; 1N,3N,5N-trihydroxy-1,3,5-triazin-2,4,6[1H,3H,5H]-trione; cobalt(II) acetate; manganese(II) acetate at 100℃; under 760 Torr; for 1h; | A 13% B 36% |
carbon monoxide
2,6-dimethylbenzenediazonium tetrafluoroborate
A
2,6-dimethylbenzoic acid
B
N-(2,6-dimethylphenyl)acetamide
C
2,6-Dimethylbenzoic anhydride
Conditions | Yield |
---|---|
With sodium acetate; palladium diacetate In acetonitrile under 6619.6 Torr; for 1h; Ambient temperature; | A 28% B 16% C 3% |
2,5-dimethylbenzamide
2,6-dimethylbenzoic acid
Conditions | Yield |
---|---|
With phosphoric acid at 145 - 150℃; |
4-amino-2,6-dimethyl benzoic acid
2,6-dimethylbenzoic acid
Conditions | Yield |
---|---|
Diazotization.Reaktion ueber mehrere Stufen; |
2,2,2-trichloro-1-(2,6-dimethyl-phenyl)-ethanone
A
2,6-dimethylbenzoic acid
B
(2,6-dimethyl-phenyl)-hydroxy-acetic acid
Conditions | Yield |
---|---|
With sodium hydroxide |
(2,6-dimethyl-benzyl)-dimethyl-amine
2,6-dimethylbenzoic acid
Conditions | Yield |
---|---|
With sodium hydroxide; potassium permanganate |
2,6-dimethylbenzoyl chloride
2,6-dimethylbenzoic acid
Conditions | Yield |
---|---|
With water In acetone at -20℃; Rate constant; |
Conditions | Yield |
---|---|
1) diazotation; Multistep reaction; | |
Multi-step reaction with 2 steps 1: (i) (diazotization), aq. HBr, (ii) Cu 2: (i) Mg, (ii) /BRN= 1900390/ View Scheme | |
Multi-step reaction with 2 steps 1: (i) NaNO2, aq. HBr, (ii) CuBr 2: (i) Mg, EtBr, Et2O, (ii) /BRN= 1900390/ View Scheme | |
Multi-step reaction with 2 steps 1: (i) NaNO2, aq. HCl, (ii) /BRN= 4652394/, CuSO4, aq. NH3, benzene 2: aq. H2SO4 / Heating View Scheme |
bis(2,6-dimethylbenzoyl) peroxide
A
2,6-dimethylbenzoic acid
B
m-xylene
Conditions | Yield |
---|---|
With 2,4,6-tri-tert-butylphenoxol In acetonitrile Ambient temperature; Irradiation; laser flash photolyses with 308-nm laser puses; Yield given. Yields of byproduct given; | |
With 2,4,6-tri-tert-butylphenoxol In acetonitrile Ambient temperature; Irradiation; Yield given. Yields of byproduct given; | |
In acetonitrile Product distribution; Mechanism; Irradiation; in the presence or absence of 2,4,6-tri-tert-butylphenol and/or dibenzoyl peroxide; structural and solvent effect upon decarboxylation investigated of various 2,6-disubstituited benzoyloxy radicals; |
ethanol
2,6-dimethylbenzoyl chloride
A
2,6-dimethylbenzoic acid
B
2,6-dimethylbenzoic acid ethyl ester
Conditions | Yield |
---|---|
With water at 10℃; Kinetics; Thermodynamic data; Product distribution; solvolysis examined; var. solvents and ratio of ones; mechanism; ΔH(excit.), ΔS(excit.); |
Conditions | Yield |
---|---|
(i) Mg, EtBr, I2, (ii) /BRN= 1900390/; Multistep reaction; |
Conditions | Yield |
---|---|
With sulfuric acid Heating; | |
Multi-step reaction with 2 steps 1: concentrated sulfuric acid / 75 - 80 °C 2: phosphoric acid / 145 - 150 °C View Scheme |
4-chloro-2,6-dimethyl benzoic acid
2,6-dimethylbenzoic acid
Conditions | Yield |
---|---|
With sodium hydroxide; nickel |
methanol
methyl 2,6-dimethylbenzoate
A
7-methyl-3H-isobenzofuran-1-one
B
2,6-dimethylbenzoic acid
Conditions | Yield |
---|---|
With sodium hydroxide; N-Bromosuccinimide 1.) CCl4, reflux, 3 h, irradiation, 2.) reflux, 35 h; Yield given. Multistep reaction. Yields of byproduct given; |
methylammonium carbonate
2,6-dimethylbenzoic acid
methylammonium carbonate
2,6-dimethylbenzoic acid
2,6-dimethylbenzoic acid
Conditions | Yield |
---|---|
durch Verseifung; |
2,6-dimethylbenzoic acid
2,6-dimethylbenzyl alcohol
Conditions | Yield |
---|---|
With Trimethyl borate; dimethylsulfide borane complex In tetrahydrofuran for 72h; Ambient temperature; | 100% |
Stage #1: 2,6-dimethylbenzoic acid With borane-THF In tetrahydrofuran at 0 - 20℃; for 64.3333h; Stage #2: With methanol In tetrahydrofuran | 99% |
With borane-THF In tetrahydrofuran at 0 - 20℃; for 64.3h; | 99% |
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 20℃; | 100% |
With potassium carbonate In acetone at 20℃; for 4h; | 93% |
With potassium hydroxide | |
With potassium carbonate at 25℃; for 1h; |
Conditions | Yield |
---|---|
100% |
Conditions | Yield |
---|---|
In methanol; dichloromethane at 20℃; for 6h; | 100% |
Conditions | Yield |
---|---|
With water In ethanol at 0 - 20℃; for 0.0833333h; | 100% |
Conditions | Yield |
---|---|
With [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 In toluene at 0 - 20℃; for 5h; | 99.9% |
Conditions | Yield |
---|---|
silver trifluoromethanesulfonate; iron(III) chloride In 1,2-dichloro-ethane at 80℃; | 99% |
Conditions | Yield |
---|---|
With [{Au(IPr)}2(μ-OH)][BF4] In neat (no solvent) at 80℃; for 15h; regioselective reaction; | 99% |
Conditions | Yield |
---|---|
With sulfuric acid; nitric acid at 0℃; for 1.5h; | 98% |
With sulfuric acid; nitric acid at 0℃; for 1h; | |
With nitric acid; acetic acid In (2S)-N-methyl-1-phenylpropan-2-amine hydrate; sulfuric acid |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; sodium acetate; tetra-(n-butyl)ammonium iodide In tetrahydrofuran; water at 80℃; for 12h; | 98% |
With tert.-butylhydroperoxide; sodium acetate; tetra-(n-butyl)ammonium iodide In tetrahydrofuran; water at 80℃; for 12h; | 96% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 24h; Inert atmosphere; | 97% |
With potassium carbonate In N,N-dimethyl-formamide at 0 - 25℃; for 5h; Inert atmosphere; | 95% |
With potassium carbonate In N,N-dimethyl-formamide at 0 - 20℃; for 16h; Inert atmosphere; | 89% |
Conditions | Yield |
---|---|
With C19H27NO2 In n-heptane at 23℃; Darkness; Green chemistry; | 97% |
With N-Bromosuccinimide; C25H44NO2PS In chloroform at 25℃; for 20h; Darkness; regioselective reaction; | 90% |
2,6-dimethylbenzoic acid
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In N,N-dimethyl-formamide Ambient temperature; | 96.3% |
2,6-dimethylbenzoic acid
2,6-dimethylcyclohexa-2,5-diene-1-carboxylic acid
Conditions | Yield |
---|---|
With ammonia; sodium In ethanol at -50℃; Birch reduction; | 96% |
With tert-Amyl alcohol; lithium In tetrahydrofuran; ammonia Birch Reduction; Reflux; liquid NH3; | 90% |
With N,N'-Dimethylurea; tris(pyrrolidino)phosphine oxide; lithium bromide In tetrahydrofuran Electrochemical reaction; | 90% |
2,6-dimethylbenzoic acid
2,6-Dimethylbenzoic anhydride
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine; tris(2,2'-bipyridyl)ruthenium dichloride; carbon tetrabromide; N,N-dimethyl-formamide at 25 - 30℃; for 12h; Inert atmosphere; Photolysis; | 96% |
With potassium carbonate; p-toluenesulfonyl chloride In dichloromethane; acetonitrile at 20℃; for 48h; | 94% |
With copper(II) bis(trifluoromethanesulfonate) at 80℃; for 0.5h; | 81% |
Conditions | Yield |
---|---|
With sulfuric acid at 100℃; for 12h; Sealed tube; | 95% |
2,6-dimethylbenzoic acid
(R)-[1-(naphthalen-2-yl)ethyl]amine
2,6-dimethyl-N-[(R)-1-(2-naphthyl)ethyl]benzamide
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 0 - 23℃; Combinatorial reaction / High throughput screening (HTS); Inert atmosphere; | 94% |
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 0 - 20℃; Inert atmosphere; | 94% |
2,6-dimethylbenzoic acid
Conditions | Yield |
---|---|
With silver carbonate; cobalt acetylacetonate In 1,2-dichloro-ethane at 100℃; for 3h; | 94% |
2,6-dimethylbenzoic acid
carbonic acid dimethyl ester
methyl 2,6-dimethylbenzoate
Conditions | Yield |
---|---|
With tributyl-amine In N,N-dimethyl-formamide at 285℃; under 112511 Torr; for 0.05h; | 93% |
With sulfuric acid at 80 - 85℃; for 8h; Neat (no solvent); | 74.5% |
Conditions | Yield |
---|---|
With C19H27NO2 In n-heptane at 23℃; Darkness; Green chemistry; | 93% |
2,6-dimethylbenzoic acid
Conditions | Yield |
---|---|
With silver carbonate; cobalt acetylacetonate In 1,2-dichloro-ethane at 100℃; for 3h; | 92% |
Conditions | Yield |
---|---|
With C19H27NO2 In n-heptane at 23℃; Darkness; Green chemistry; | 92% |
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In 1,4-dioxane at 20℃; for 0.5h; Mitsunobu Displacement; Inert atmosphere; stereoselective reaction; | 92% |
Conditions | Yield |
---|---|
With potassium fluoride In acetonitrile at 20℃; for 12h; Cooling with ice; | 91% |
Conditions | Yield |
---|---|
With C19H27NO2 In n-heptane at 23℃; Darkness; Green chemistry; | 91% |
Methyl trichloroacetate
2,6-dimethylbenzoic acid
methyl 2,6-dimethylbenzoate
Conditions | Yield |
---|---|
With 18-crown-6 ether; potassium carbonate at 90 - 150℃; for 2h; | 90% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide In water; ethyl acetate at 80℃; for 12h; | 90% |
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