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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Competitve Price in stock CAS 67000-89-9 with best price

Cas:67000-89-9

Min.Order:10 Gram

FOB Price: $146.0 / 176.0

Type:Trading Company

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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for the fine chemicals, ph

1-Pyrenebutanol

Cas:67000-89-9

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Qingdao Beluga Import and Export Co., LTD

1-PYRENEBUTANOL CAS:67000-89-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedi

1-PYRENEBUTANOL CAS:67000-89-9

Cas:67000-89-9

Min.Order:1 Gram

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

1-Pyrenebutanol

Cas:67000-89-9

Min.Order:1 Kilogram

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

1-Pyrenebutanol

Cas:67000-89-9

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SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

1-Pyrenebutanol

Cas:67000-89-9

Min.Order:4 Kilogram

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High Quality 1-(2,6-Dichlorophenyl)indolin-2-one

Cas:67000-89-9

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates

1-Pyrenebutanol

Cas:67000-89-9

Min.Order:0

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Type:Manufacturers

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Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

1-PYRENEBUTANOL

Cas:67000-89-9

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Henan Tianfu Chemical Co., Ltd.

1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.

1-Pyrenebutanol

Cas:67000-89-9

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Xian Changyue Biological Technology Co., Ltd.

best seller Application:API

1-Pyrenebutanol

Cas:67000-89-9

Min.Order:0

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Type:Manufacturers

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Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

1-Pyrenebutanol

Cas:67000-89-9

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HANGZHOU TIANYE CHEMICALS CO., LTD.

We product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Application:Chemical intermediate

1-Pyrenebutanol

Cas:67000-89-9

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DB BIOTECH CO., LTD

best seller Application:API

1-Pyrenebutanol

Cas:67000-89-9

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Hangzhou Fandachem Co.,Ltd

4-(1-PYRENYL)-N-BUTANOLAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

4-(1-PYRENYL)-N-BUTANOL

Cas:67000-89-9

Min.Order:0

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Type:Other

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Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

1-Pyrenebutanol

Cas:67000-89-9

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Shanghai Chinqesen Biotechnology Co., Ltd.

Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen

67000-89-9

Cas:67000-89-9

Min.Order:0

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Hebei Muhuang Technology Co., Ltd

best seller Application:API

1-Pyrenebutanol

Cas:67000-89-9

Min.Order:0

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Type:Trading Company

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ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

1-Pyrenebutanol

Cas:67000-89-9

Min.Order:0

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Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

1-Pyrenebutanol

Cas:67000-89-9

Min.Order:10 Milligram

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Zhengzhou Kingorgchem Chemical Technology Co., Ltd.

Zhengzhou Kingorgchem Chemical Technology Co., Ltd. was founded on the basis of Organophosphorus Chemistry Lab of Institute of Chemistry Henan Academy of Sciences in 2015. The laboratory covers 600 m2 and the pilot plant covers 2000 m2. Kingorgchem i

National Research Platform ISO 9001 67000-89-9

Cas:67000-89-9

Min.Order:0

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Type:Lab/Research institutions

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Qingdao Sigma Chemical Co., Ltd.

Qingdao Sigma Chemical Ltd is is a global chemical industry manufacturers and suppliers of pharmaceuticals and intermediates, peptide,Nootropis etc API, food and feed additives, herbal extracts, agrochemicals and fine chemicals etc. Our Labo

High Quality 1-(2,6-Dichlorophenyl)indolin-2-one

Cas:67000-89-9

Min.Order:1 Gram

FOB Price: $1.0

Type:Trading Company

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HuBei Ipure Biotech CO.,ltd

HuBei ipure is a diversified product production and operation enterprise, with API, pharma intermediates, and other fine chemicals as well as R&D and pigments development and sales as one of the large enterprises, with more than 130 acres of pl

High Quality 1-(2,6-Dichlorophenyl)indolin-2-one

Cas:67000-89-9

Min.Order:1 Gram

FOB Price: $1.0 / 2.0

Type:Trading Company

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Hangzhou Share Chemical Co., Ltd

At Share Chemical Company, we scrupulously abide by our policy of “Excellent Quality at a Reasonable Price”. We strive to satisfy all of our customers by providing the finest quality products supported by the finest in customer servi

1-Pyrenebutanol

Cas:67000-89-9

Min.Order:1 Gram

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Type:Other

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Luminescence Technology Corp.

World-class service, High quality, Low cost and Quick delivery. All made in our plant! Storage:To be stored in cool dry environment Package:1g,5g,10g or Bulk Application:Fluorescent Probes > Additional Stains, Dyes and Fluorescent Probes

1-Pyrenebutanol

Cas:67000-89-9

Min.Order:0 Metric Ton

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Type:Manufacturers

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Chungking Joyinchem Co., Ltd.

Joyinchem have been committed to chemical supply for several years and have built good cooperation records with multinational chemical corporations and importers from all over the world. Our services include:-Spot goods-Contract manufacturing-Custom

1-Pyrenebutanol

Cas:67000-89-9

Min.Order:0

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Finetech Industry Limited

FINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the 1-PYRENEBUTANOL, CAS:67000-89-9 with the most competitive price and the best quality.

1-PYRENEBUTANOL

Cas:67000-89-9

Min.Order:0

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Type:Trading Company

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Nanjing Raymon Biotech Co., Ltd.

4-pyren-1-ylbutan-1-ol Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediates Transportation:By Sea,by Air,By courier like DHL or Fedx. Port:Shanghai/Shenzhen

4-pyren-1-ylbutan-1-ol

Cas:67000-89-9

Min.Order:0

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Hebei Ruishun Trade Co.,Ltd

Supply top quality products with a reasonable price Application:api

67000-89-9

Cas:67000-89-9

Min.Order:0

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Type:Trading Company

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Chemical Co.Ltd

1-PyrenebutanolAppearance:Off white to slight yellow solid Storage:Stored in shaded, cool and dry places Package:1L 5L 10L 25L bottle Application:pharma intermediate Transportation:Handle with cares to avoid damaging the packages. Protect them from s

1-Pyrenebutanol

Cas:67000-89-9

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Synthetic route

4-(1-pyrene)butyric acid methyl ester
70570-29-5

4-(1-pyrene)butyric acid methyl ester

4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

Conditions
ConditionsYield
With diisobutylaluminium hydride In tetrahydrofuran; hexane at 0 - 20℃; Inert atmosphere;99%
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃;
1-pyrenebutyric acid
3443-45-6

1-pyrenebutyric acid

4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

Conditions
ConditionsYield
With lithium aluminium tetrahydride95%
With dimethylsulfide borane complex In tetrahydrofuran at 0 - 20℃;90.2%
With borane-THF In tetrahydrofuran at 20℃; Cooling with ice;79%
4-(1-pyrene)butanoic acid ethyl ester
59275-39-7

4-(1-pyrene)butanoic acid ethyl ester

4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

Conditions
ConditionsYield
With lithium aluminium tetrahydride In tetrahydrofuran at 20℃; for 4h;88%
C20H18O(2-)*2Li(1+)

C20H18O(2-)*2Li(1+)

4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

Conditions
ConditionsYield
With 2,3-dicyano-5,6-dichloro-p-benzoquinone 1.) methanol, -78 deg C, 2.) abs. toluene, reflux, 1h.; Yield given. Multistep reaction;
2,2-dibromo-malonic acid bis-(4-pyren-1-yl-butyl) ester

2,2-dibromo-malonic acid bis-(4-pyren-1-yl-butyl) ester

4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

Conditions
ConditionsYield
With caesium carbonate In N,N-dimethyl-formamide100 % Chromat.
pyrene
129-00-0

pyrene

4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1.) lithium wire / 1.)-78 deg C, 12 h., 2.) room temp., 12 h.
2: 2.) DDQ / 1.) methanol, -78 deg C, 2.) abs. toluene, reflux, 1h.
View Scheme
Multi-step reaction with 4 steps
1.1: aluminum (III) chloride / nitrobenzene / 18 h / 0 - 20 °C
2.1: potassium hydroxide; hydrazine / diethylene glycol / 2 h / Heating / reflux
2.2: 0 °C
3.1: thionyl chloride / 0 - 20 °C
4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C
View Scheme
C53H48O5S2
1452863-03-4

C53H48O5S2

Hg(2+)

Hg(2+)

A

bis(acetic acid thiolato)mercury(II)

bis(acetic acid thiolato)mercury(II)

B

4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

C

4-ethoxybenzaldehyde
10031-82-0

4-ethoxybenzaldehyde

Conditions
ConditionsYield
In acetonitrile for 0.166667h; pH=4.8;
γ-oxo-1-pyrenebutyric acid
7499-60-7

γ-oxo-1-pyrenebutyric acid

4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: potassium hydroxide; hydrazine / diethylene glycol / 2 h / Heating / reflux
1.2: 0 °C
2.1: thionyl chloride / 0 - 20 °C
3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C
View Scheme
11-(tert-butoxycarbonylamino)undecanoic acid
10436-25-6

11-(tert-butoxycarbonylamino)undecanoic acid

4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

C36H47NO4
1416547-75-5

C36H47NO4

Conditions
ConditionsYield
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 120h;99%
4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

methanesulfonyl chloride
124-63-0

methanesulfonyl chloride

4-(pyren-1-yl)butyl methanesulfonate
205488-04-6

4-(pyren-1-yl)butyl methanesulfonate

Conditions
ConditionsYield
With triethylamine In dichloromethane Cooling with ice;98%
With triethylamine In dichloromethane at 0℃; for 12h;96%
With triethylamine In dichloromethane Cooling with ice;91.2%
With triethylamine In dichloromethane at 20℃; for 2h; Inert atmosphere;91%
With triethylamine In dichloromethane at 20℃; for 4h;
4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

4-(pyren-1-yl)butanal

4-(pyren-1-yl)butanal

Conditions
ConditionsYield
With pyridinium chlorochromate In dichloromethane at 20℃; for 2h;97%
With dipyridinium dichromate In dichloromethane at 20℃; Inert atmosphere;97%
With pyridinium chlorochromate In dichloromethane at 20℃;95%
4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

1-bromo-4-(1-pyrenyl)butane
117846-05-6

1-bromo-4-(1-pyrenyl)butane

Conditions
ConditionsYield
With carbon tetrabromide; triphenylphosphine In acetonitrile at 25℃; for 0.333333h; Appel Halogenation;96%
With carbon tetrabromide; triphenylphosphine In dichloromethane Bromination; substitution;90%
With carbon tetrabromide; triphenylphosphine In tetrahydrofuran90%
4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

4-cyano-4-(thiobenzoylthio)pentanoic acid
201611-92-9

4-cyano-4-(thiobenzoylthio)pentanoic acid

4-cyano-4-methyl-4-thiobenzoylsulfanyl-butyric acid 4-pyren-1-yl-butyl ester
1048735-14-3

4-cyano-4-methyl-4-thiobenzoylsulfanyl-butyric acid 4-pyren-1-yl-butyl ester

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In tetrahydrofuran; dichloromethane at 0 - 20℃;95%
4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

2-Bromoacetyl bromide
598-21-0

2-Bromoacetyl bromide

C22H19BrO2

C22H19BrO2

Conditions
ConditionsYield
Stage #1: 4-pyrenylbutanol In dichloromethane Alkaline conditions; Cooling with ice;
Stage #2: 2-Bromoacetyl bromide In dichloromethane at 20℃; for 24h; Cooling with ice;
92%
11-mercaptounadecanoic acid
71310-21-9

11-mercaptounadecanoic acid

4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

4-(pyren-4-yl) butyl-11-mercaptoundecanoate

4-(pyren-4-yl) butyl-11-mercaptoundecanoate

Conditions
ConditionsYield
With hafnium/THF In toluene for 48h; Reflux; Molecular sieve;89%
2,4,6-tri(4-pyridyl)-1,3,5-triazine
42333-78-8

2,4,6-tri(4-pyridyl)-1,3,5-triazine

[Ru2(η6-p-cymene)2(C6H2O4)Cl2]
1039768-31-4

[Ru2(η6-p-cymene)2(C6H2O4)Cl2]

4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

silver trifluoromethanesulfonate
2923-28-6

silver trifluoromethanesulfonate

[(1-pyrenebutanol)*Ru6(p-cymene)6(2,4,6-tris(pyridin-4-yl)-1,3,5-triazine)2(2,5-dioxydo-1,4-benzoquinonato)3](triflate)6

[(1-pyrenebutanol)*Ru6(p-cymene)6(2,4,6-tris(pyridin-4-yl)-1,3,5-triazine)2(2,5-dioxydo-1,4-benzoquinonato)3](triflate)6

Conditions
ConditionsYield
In methanol byproducts: AgCl; Ru complex and AgCF3SO3 stirred in MeOH for 2 h; filtered into suspn. ofN3C3(C5H4N)3 and pyrenyl in MeOH; stirred at room temp. for 18 h; solvent removed under reduced pressure; dissolved in CH2Cl2; filtered; vol. of filtrate reduced; pptd. with Et2O; collected by filtration;88%
2-bromoisobutyric acid bromide
20769-85-1

2-bromoisobutyric acid bromide

4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

C24H23BrO2

C24H23BrO2

Conditions
ConditionsYield
With triethylamine In dichloromethane88%
4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

3-oxo-3-(pent-4-yn-1-yloxy)propanoic acid
1448599-87-8

3-oxo-3-(pent-4-yn-1-yloxy)propanoic acid

pent-4-yn-1-yl (4-(pyren-1-yl)butyl) malonate
1448599-89-0

pent-4-yn-1-yl (4-(pyren-1-yl)butyl) malonate

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0℃; for 2h; Cooling with ice; Inert atmosphere;87%
4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

O-(2-Acetamido-3,4,6-tri-O-acetyl-2-desoxy-α-D-glucopyranosyl)trichloracetimidat
94715-74-9

O-(2-Acetamido-3,4,6-tri-O-acetyl-2-desoxy-α-D-glucopyranosyl)trichloracetimidat

4-(1-pyrenyl)butyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside
1160291-41-7

4-(1-pyrenyl)butyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

Conditions
ConditionsYield
With trimethylsilyl trifluoromethanesulfonate In dichloromethane at 20℃; for 3h;85%
4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

N-tert-butyl-O-[1-(4-chloromethyl-phenyl)-ethyl]-N-(2-methyl-1-phenyl-propyl)-hydroxylamine
227000-85-3

N-tert-butyl-O-[1-(4-chloromethyl-phenyl)-ethyl]-N-(2-methyl-1-phenyl-propyl)-hydroxylamine

N-tert-butyl-N-(2-methyl-1-phenyl-propyl)-O-{1-[4-(4-pyren-1-yl-butoxymethyl)-phenyl]-ethyl}-hydroxylamine

N-tert-butyl-N-(2-methyl-1-phenyl-propyl)-O-{1-[4-(4-pyren-1-yl-butoxymethyl)-phenyl]-ethyl}-hydroxylamine

Conditions
ConditionsYield
With sodium hydride In tetrahydrofuran for 16h; Heating;84%
4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

malonoyl dichloride
1663-67-8

malonoyl dichloride

bis[4-pyrene-1-butoxy]malonyl ester

bis[4-pyrene-1-butoxy]malonyl ester

Conditions
ConditionsYield
With sodium hydride In tetrahydrofuran at 20℃; for 24h;84%
3,3'-dithiobis(propionic acid)
1119-62-6

3,3'-dithiobis(propionic acid)

4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

3-((3-oxo-3-(4-(pyren-1-yl)butoxy)propyl)disulfanyl)propanoic acid
1259437-62-1

3-((3-oxo-3-(4-(pyren-1-yl)butoxy)propyl)disulfanyl)propanoic acid

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In tetrahydrofuran at 20℃; for 20h;81.3%
4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

propargyl bromide
106-96-7

propargyl bromide

1-(4-(prop-2-yn-1-yloxy)butyl)pyrene
1211548-30-9

1-(4-(prop-2-yn-1-yloxy)butyl)pyrene

Conditions
ConditionsYield
Stage #1: 4-pyrenylbutanol With sodium hydride In tetrahydrofuran at 0℃; for 0.5h; Inert atmosphere;
Stage #2: propargyl bromide In tetrahydrofuran; toluene at 0℃; Inert atmosphere; Reflux; Darkness;
81%
Stage #1: 4-pyrenylbutanol With sodium hydride In tetrahydrofuran at 0℃; for 1h; Inert atmosphere;
Stage #2: propargyl bromide In tetrahydrofuran; toluene at 0℃; for 1h; Inert atmosphere; Darkness;
69%
4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

Methacryloyl chloride
920-46-7

Methacryloyl chloride

4-(pyren-1-yl)butyl methacrylate
71254-27-8

4-(pyren-1-yl)butyl methacrylate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 1h; Inert atmosphere;80%
With triethylamine In dichloromethane at 20℃;
With triethylamine In dichloromethane at 0℃; for 2h;
thionyl chloride
7719-09-7

thionyl chloride

[(C5H5)TiCl(C5H4C(CH3)2CH2CO2)]*0.5C7H8

[(C5H5)TiCl(C5H4C(CH3)2CH2CO2)]*0.5C7H8

4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

[(C5H5)TiCl2(C5H4C(CH3)2CH2C(O)O(CH2)4C16H9)]
864767-17-9

[(C5H5)TiCl2(C5H4C(CH3)2CH2C(O)O(CH2)4C16H9)]

Conditions
ConditionsYield
With NaH In dichloromethane Ti complex was reacted with SOCl2 at room temp. for 1 h; heated at 50°C for 2 h in vac.; dissolved in CH2Cl2; transferred to mixt. of NaHand alcohol in CH2Cl2; stirred at room temp. for 16 h; filtered through Celite; crystd. (CH2Cl2/pentane);79%
4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

1,10-dibromodecane
4101-68-2

1,10-dibromodecane

1-[4-(10-bromo-decyloxy)-butyl]-pyrene
244013-58-9

1-[4-(10-bromo-decyloxy)-butyl]-pyrene

Conditions
ConditionsYield
Stage #1: 4-pyrenylbutanol With potassium tert-butylate In toluene at 100℃; for 1h;
Stage #2: 1,10-dibromodecane In toluene for 16h;
79%
3-Thiophene carboxylic acid
88-13-1

3-Thiophene carboxylic acid

4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

4-(pyren-1-yl)butyl thiophene-3-carboxylate

4-(pyren-1-yl)butyl thiophene-3-carboxylate

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0 - 20℃; for 12.5h; Inert atmosphere;79%
thiophen-3-yl-acetic acid
6964-21-2

thiophen-3-yl-acetic acid

4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

4-(pyren-1-yl)butyl 2-(thiophen-3-yl)acetate

4-(pyren-1-yl)butyl 2-(thiophen-3-yl)acetate

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0 - 20℃; for 12.5h; Inert atmosphere;76%
4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

3-mercaptopropionic acid
107-96-0

3-mercaptopropionic acid

4-(pyren-1-yl)butyl 3-mercaptopropionate
1041403-51-3

4-(pyren-1-yl)butyl 3-mercaptopropionate

Conditions
ConditionsYield
With toluene-4-sulfonic acid In benzene Inert atmosphere; Reflux;75%
4-pentynoic acid
6089-09-4

4-pentynoic acid

4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

4-(pyren-1-yl)butyl pent-4-ynoate
1213789-09-3

4-(pyren-1-yl)butyl pent-4-ynoate

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane72%
4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

N-tert-butoxycarbonyl-L-phenylalanine
13734-34-4

N-tert-butoxycarbonyl-L-phenylalanine

Boc-Phe-Pyrene
1400924-49-3

Boc-Phe-Pyrene

Conditions
ConditionsYield
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; ethyl cyanoglyoxylate-2-oxime In N,N-dimethyl-formamide at 0℃; for 2h;71%
4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

2,6-bis(pyrazole-1-yl)pyridine-4-carboxylic acid
600727-96-6

2,6-bis(pyrazole-1-yl)pyridine-4-carboxylic acid

2,6-d-pyrazol-1-yl-isonicotinic acid 4-pyren-1-yl-butyl ester

2,6-d-pyrazol-1-yl-isonicotinic acid 4-pyren-1-yl-butyl ester

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0 - 20℃; for 72h; Inert atmosphere; Schlenk technique;69%
2,6-bis-(bromomethyl)pyridine
7703-74-4

2,6-bis-(bromomethyl)pyridine

4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

2-(bromomethyl)-6-((4-(pyren-1-yl)butoxy)methyl)pyridine

2-(bromomethyl)-6-((4-(pyren-1-yl)butoxy)methyl)pyridine

Conditions
ConditionsYield
Stage #1: 4-pyrenylbutanol With sodium hydride In tetrahydrofuran at 20℃; for 0.5h; Inert atmosphere; Cooling with ice;
Stage #2: 2,6-bis-(bromomethyl)pyridine In tetrahydrofuran at 20℃; for 4h; Inert atmosphere;
68%
With sodium hydride In tetrahydrofuran; mineral oil for 18h; Reflux; Inert atmosphere;62%
4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

allyl bromide
106-95-6

allyl bromide

C23H22O

C23H22O

Conditions
ConditionsYield
With potassium hydride In dichloromethane at 0 - 20℃; for 6h;62%
4-pyrenylbutanol
67000-89-9

4-pyrenylbutanol

C13H16O5S2
1452863-02-3

C13H16O5S2

C53H48O5S2
1452863-03-4

C53H48O5S2

Conditions
ConditionsYield
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 4h;60%

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