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inquiryWe are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white crystalline powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use
Dodecanoic acid,12-amino- cas 693-57-2Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
Conditions | Yield |
---|---|
With Acidovorax sp.T31 ω-laurolactam hydrolase; water In toluene at 35℃; for 17h; pH=7; aq. phosphate buffer; Enzymatic reaction; | 99.7% |
With hydrogenchloride | |
With potassium phosphate buffer In toluene at 30℃; for 2h; pH=7.0; | 10 mmol |
With whole cells or crude cell extract of recombinant E.coli BL21 (DE3) (pCom10_T31) In ethanol for 0.5h; pH=7.4; aq. buffer; Enzymatic reaction; | 99 %Chromat. |
Conditions | Yield |
---|---|
With ethanol; titanium(IV) oxide for 2.5h; Irradiation; | A n/a B 89% C n/a |
12-oxododecanoic acid oxime
12-Aminododecanoic acid
Conditions | Yield |
---|---|
With hydrogen; platinum(IV) oxide In methanol under 2280 Torr; for 1.5h; | 87% |
12-nitrododecanoic acid
12-Aminododecanoic acid
Conditions | Yield |
---|---|
With ammonium formate; palladium on activated charcoal In methanol at 80℃; for 0.5h; | 85% |
Conditions | Yield |
---|---|
Pseudomonas K95 | 55% |
Pseudomonas K95 | 49% |
methyl 12-aminododecanoate
A
2-azacyclotridecanone
B
12-Aminododecanoic acid
Conditions | Yield |
---|---|
With whole-cells or crude cell extract of recombinant E.coli BL21 (DE3) (pCom10_T31) In ethanol for 0.5h; pH=10; aq. buffer; Enzymatic reaction; | A 13% B n/a |
12-aminododecanoic acid ethyl ester
12-Aminododecanoic acid
Conditions | Yield |
---|---|
With hydrogenchloride |
12-Aminododecanoic acid
Conditions | Yield |
---|---|
With sulfuric acid und Erhitzen des Reaktionsprodukts mit konz. wss. HCl auf 180grad; |
Conditions | Yield |
---|---|
With hydrogenchloride |
ω-Amino-7-oxo-laurinsaeure
12-Aminododecanoic acid
Conditions | Yield |
---|---|
With potassium hydroxide; hydrazine hydrate |
Conditions | Yield |
---|---|
In water-d2 at 24.85℃; pH=7.3; Equilibrium constant; Decomposition; |
Conditions | Yield |
---|---|
In water-d2 at 24.85℃; pH=7.3; Equilibrium constant; Decomposition; |
12-Aminododecanoic acid
Conditions | Yield |
---|---|
With sulfuric acid anschliessend mit konz. Salzsaeure bei 180grad; |
sulfuric acid
A
1-nonadecanamine (n-nonadecylamine)
B
Arachidic acid
C
12-Aminododecanoic acid
Conditions | Yield |
---|---|
Erhitzen des Rektionsprodukts mit konz. HCl auf 180grad; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 0.92 mg / hydroxylamine hydrochloride, aq. NaOH / ethanol / 0.17 h / 100 °C 2: 87 percent / H2 / PtO2 / methanol / 1.5 h / 2280 Torr View Scheme |
cis-12,13-epoxystearic acid
12-Aminododecanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 73 percent / HIO4 / H2O; 2-methyl-propan-2-ol / 5 h 2: 0.92 mg / hydroxylamine hydrochloride, aq. NaOH / ethanol / 0.17 h / 100 °C 3: 87 percent / H2 / PtO2 / methanol / 1.5 h / 2280 Torr View Scheme |
(+/-)-cis-12,13-epoxy-9(Z)-octadecenoic acid
12-Aminododecanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 93 percent / H2 / PtO2 / methanol / 0.75 h / 2280 Torr 2: 73 percent / HIO4 / H2O; 2-methyl-propan-2-ol / 5 h 3: 0.92 mg / hydroxylamine hydrochloride, aq. NaOH / ethanol / 0.17 h / 100 °C 4: 87 percent / H2 / PtO2 / methanol / 1.5 h / 2280 Torr View Scheme |
7-[5-(acetylamino-methyl)-thiophen-2-yl]-heptanoic acid ethyl ester
12-Aminododecanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aq. HCl / Raney-Ni / methanol 2: aq. HCl View Scheme |
2-(syn-2-Oxo-cyclohexyliden)-1-aza-cycloheptan
12-Aminododecanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aq. NaOH / Heating 2: N2H4*H2O, KOH View Scheme |
methyl 12-aminododecanoate
12-Aminododecanoic acid
Conditions | Yield |
---|---|
With whole-cells of recombinant E.coli BL21 (DE3) (pCom10_T31) In ethanol pH=7.4; aq. buffer; Enzymatic reaction; |
methyl n-dodecanoate
A
12-hydroxydodecanoic acid
B
methyl 12-hydroxydodecanoate
C
1,12-dodecanedioic acid
D
12-methoxy-12-oxododecanoic acid
E
methyl 12-aminododecanoate
F
12-Aminododecanoic acid
Conditions | Yield |
---|---|
With NADH In aq. phosphate buffer Kinetics; Microbiological reaction; | |
Multi-step reaction with 2 steps 1: NADH / aq. phosphate buffer / Microbiological reaction 2: NADH / aq. phosphate buffer / Microbiological reaction View Scheme |
methyl 11-formylundecanoate
A
12-hydroxydodecanoic acid
B
methyl 12-hydroxydodecanoate
C
1,12-dodecanedioic acid
D
12-methoxy-12-oxododecanoic acid
E
methyl 12-aminododecanoate
F
12-Aminododecanoic acid
Conditions | Yield |
---|---|
With NADH In aq. phosphate buffer Kinetics; Microbiological reaction; |
Conditions | Yield |
---|---|
With L-alanin; sodium hydroxide In aq. buffer at 35℃; for 2h; pH=8 - 9.5; Enzymatic reaction; | |
With pyridoxal 5'-phosphate; MATITNHMPTAELQALDAAHHLHPFSANNALGEEGTRVITRARGVWLNDSEGEEILDAMAGLWCVNIGYGRDELAEVAARQMRELPYYNTFFKTTHVPAIALAQKLAELAPGDLNHVFFAGGGSEANDTNIRMVRTYWQNKGQPEKTVIISRKNAYHGSTVASSALGGMAGMHAQSGLIPDVHHINQPNWWAEGGDMDPEEFGLARARELEEAILELGENRVAAFIAEPVQGAGGVIVAPDSYWPEIQRICDKYDILLIADEVICGFGRTGNWFGTQTMGIRPHIMTIAKGLSSGYAPIGGSIVCDEVAHVIGKDEFNHGYTYSGHPVAAAVALENLRILEEENILDHVRNVAAPYLKEKWEALTDHPLVGEAKIVGMMASIALTPNKASRAKFASEPGTIGYICRERCFANNLIMRHVGDRMIISPPLVITPAEIDEMFVRIRKSLDEAQAEIEKQGLMKSA; MIKAYAALEANGKLQPFEYDPGALGANEVEIEVQYCGVCHSDLSMINNEWGISNYPLVPGHEVVGTVAAMGEGVNHVEVGDLVGLGWHSGYCMTCHSCLSGYHNLCATAESTIVGHYGGFGDRVRAKGVSVVKLPKGIDLASAGPLFCGGITVFSPMVELSLKPTAKVAVIGIGGLGHLAVQFLRAWGCEVTAFTSSARKQTEVLELGAHHILDSTNPEAIASAEGKFDYIISTVNLKLDWNLYISTLAPQGHFHFVGVVLEPLDLNLFPLLMGQRSVSASPVGSPATIATMLDFAVRHDIKPVVEQFSFDQINEAIAHLESGKAHYRVVLSHSKN; nicotinamide adenine dinucleotide phosphate; benzylamine In dimethyl sulfoxide at 37℃; for 24h; pH=8; Reagent/catalyst; pH-value; Solvent; Microbiological reaction; Enzymatic reaction; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: ozone / 2.5 h / 5 °C / Molecular sieve 1.2: 0.5 h / 10 - 20 °C 2.1: ammonia; hydrogen / isopropyl alcohol / 60 °C / 36961.4 Torr View Scheme |
12-Aminododecanoic acid
Conditions | Yield |
---|---|
With ammonia; hydrogen In isopropyl alcohol at 60℃; under 36961.4 Torr; | |
With ammonia; hydrogen In isopropyl alcohol at 60℃; under 36961.4 Torr; |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: hydrogen bromide / toluene / 1 h / 18 °C / Industrial scale 2: sodium carbonate / N,N-dimethyl acetamide / 1.5 h / 130 °C / Inert atmosphere 3: hydrogen / 0.67 h / 90 - 110 °C / 18751.9 Torr View Scheme |
Conditions | Yield |
---|---|
With hydrogen at 90 - 110℃; under 18751.9 Torr; for 0.666667h; Temperature; | |
With ammonium hydroxide; Ru/SiC; hydrogen In propan-1-ol; water at 110℃; under 26252.6 Torr; for 1.5h; Autoclave; | 9.7 g |
methyl 12-hydroxydodecanoate
A
methyl 12-aminododecanoate
B
12-Aminododecanoic acid
Conditions | Yield |
---|---|
With pyridoxal 5'-phosphate; MATITNHMPTAELQALDAAHHLHPFSANNALGEEGTRVITRARGVWLNDSEGEEILDAMAGLWCVNIGYGRDELAEVAARQMRELPYYNTFFKTTHVPAIALAQKLAELAPGDLNHVFFAGGGSEANDTNIRMVRTYWQNKGQPEKTVIISRKNAYHGSTVASSALGGMAGMHAQSGLIPDVHHINQPNWWAEGGDMDPEEFGLARARELEEAILELGENRVAAFIAEPVQGAGGVIVAPDSYWPEIQRICDKYDILLIADEVICGFGRTGNWFGTQTMGIRPHIMTIAKGLSSGYAPIGGSIVCDEVAHVIGKDEFNHGYTYSGHPVAAAVALENLRILEEENILDHVRNVAAPYLKEKWEALTDHPLVGEAKIVGMMASIALTPNKASRAKFASEPGTIGYICRERCFANNLIMRHVGDRMIISPPLVITPAEIDEMFVRIRKSLDEAQAEIEKQGLMKSA; MIKAYAALEANGKLQPFEYDPGALGANEVEIEVQYCGVCHSDLSMINNEWGISNYPLVPGHEVVGTVAAMGEGVNHVEVGDLVGLGWHSGYCMTCHSCLSGYHNLCATAESTIVGHYGGFGDRVRAKGVSVVKLPKGIDLASAGPLFCGGITVFSPMVELSLKPTAKVAVIGIGGLGHLAVQFLRAWGCEVTAFTSSARKQTEVLELGAHHILDSTNPEAIASAEGKFDYIISTVNLKLDWNLYISTLAPQGHFHFVGVVLEPLDLNLFPLLMGQRSVSASPVGSPATIATMLDFAVRHDIKPVVEQFSFDQINEAIAHLESGKAHYRVVLSHSKN; nicotinamide adenine dinucleotide phosphate; benzylamine In dimethyl sulfoxide at 37℃; for 24h; pH=8; Microbiological reaction; Enzymatic reaction; |
undec-10-enenitrile
12-Aminododecanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: acetylacetonatodicarbonylrhodium(l); hydrogen; 1,2-bis-(diphenylphosphino)ethane / toluene / 2 h / 100 °C / 15001.5 Torr / Autoclave 2: oxygen / toluene / 24 h / 20 °C 3: hydrogen; Ru/SiC; ammonium hydroxide / propan-1-ol; water / 1.5 h / 110 °C / 26252.6 Torr / Autoclave View Scheme | |
Multi-step reaction with 3 steps 1: acetylacetonatodicarbonylrhodium(l); hydrogen; 6,6'-[[3,3',5,5'-tetrakis(1,1-dimethylethyl)-[1,1'-biphenyl]-2,2'-diyl]bis(oxy)]bis-dibenzo [d,f][1,3,2]-dioxaphosphepine / toluene / 24 h / 120 °C / 15001.5 Torr / Autoclave 2: oxygen / toluene / 24 h / 20 °C 3: hydrogen; Ru/SiC; ammonium hydroxide / propan-1-ol; water / 1.5 h / 110 °C / 26252.6 Torr / Autoclave View Scheme |
1-adamantyl isocyanate
12-Aminododecanoic acid
12-(3-adamantan-1-yl-ureido)dodecanoic acid
Conditions | Yield |
---|---|
In 1,2-dichloro-ethane for 6h; Heating; | 100% |
In chloroform for 10h; Heating / reflux; | 100% |
In hexane at 20℃; | 39% |
In chloroform | 2.66 g (100%) |
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane |
di-tert-butyl dicarbonate
12-Aminododecanoic acid
N-(tert-butyloxycarbonyl)-12-aminododecanoic acid
Conditions | Yield |
---|---|
With triethylamine In dichloromethane | 99% |
With sodium hydroxide In water | 97% |
With triethylamine In methanol at 60℃; for 1h; | 96% |
Conditions | Yield |
---|---|
With hydrogenchloride at 50℃; for 4h; | 99% |
With thionyl chloride at 20℃; Reflux; | 98% |
With thionyl chloride at 0 - 20℃; for 9h; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
In methanol for 4h; Reflux; | 99% |
Conditions | Yield |
---|---|
With triethylamine In methanol for 4h; Reflux; | 99% |
maleic anhydride
12-Aminododecanoic acid
12-(3-carboxyacryloylamino)dodecanoic acid
Conditions | Yield |
---|---|
With lutidine In diethylene glycol dimethyl ether | 98% |
With acetic acid Ambient temperature; | 85% |
In acetic acid |
phthalic anhydride
12-Aminododecanoic acid
12-(1,3-dioxoisoindolin-2-yl)dodecanoic acid
Conditions | Yield |
---|---|
With triethylamine In toluene for 1.5h; Heating; | 98% |
With triethylamine In toluene for 12h; Heating; | 80% |
In toluene Heating; | 36% |
at 150℃; for 0.75h; Yield given; |
12-Aminododecanoic acid
methyl 12-aminododecanoate
Conditions | Yield |
---|---|
With hydrogenchloride; sodium hydrogencarbonate In methanol; water | 98% |
With sulfuric acid; sodium carbonate In methanol | 95% |
With sulfuric acid In methanol for 24h; Reflux; | 70% |
trifluoroacetic acid-methyl ester
12-Aminododecanoic acid
12-(2,2,2-trifluoroacetamido)dodecanoic acid
Conditions | Yield |
---|---|
With triethylamine In methanol for 18h; | 97% |
With triethylamine In methanol at 20℃; for 18h; | 92% |
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
12-Aminododecanoic acid
N,N’-di(1-carboxylundecyl)-3,4,9,10-perylenetetracarboxyldiimide
Conditions | Yield |
---|---|
With 1H-imidazole at 120℃; for 1h; Schlenk technique; Inert atmosphere; | 96% |
In 1-methyl-pyrrolidin-2-one | |
In 1-methyl-pyrrolidin-2-one at 110℃; for 24h; Inert atmosphere; |
Methacryloyl chloride
12-Aminododecanoic acid
12-(methacrylolamino)dodecanoic acid
Conditions | Yield |
---|---|
With sodium hydrogencarbonate; 4-methoxy-phenol In acetone for 1h; Heating; | 95% |
In 1,4-dioxane; water | 73% |
Stage #1: 12-Aminododecanoic acid With sodium hydroxide In water for 0.5h; Stage #2: Methacryloyl chloride In water at -5 - 0℃; for 1.25h; Stage #3: With hydrogenchloride In water pH=<= 3; |
Conditions | Yield |
---|---|
Stage #1: ethanol With acetyl chloride at 20℃; for 1h; Stage #2: 12-Aminododecanoic acid at 20℃; for 0.25h; | 94% |
With sulfuric acid Reflux; |
Conditions | Yield |
---|---|
With thionyl chloride at 0 - 20℃; for 12h; | 93% |
With thionyl chloride at 0 - 20℃; for 2.33333h; |
Conditions | Yield |
---|---|
With sodium hydrogencarbonate; triethylamine In acetone at 20℃; for 1h; | 92% |
With sodium hydrogencarbonate In water; acetone at 20℃; for 5h; | 60% |
succinimidyl 4-azido-2,3,5,6-tetrafluorobenzoate
12-Aminododecanoic acid
12-[N-(4-azido-2,3,5,6-tetrafluorobenzoyl)]amidododecanoic acid
Conditions | Yield |
---|---|
In 1,4-dioxane at 50 - 60℃; for 4h; | 90% |
(fluorenylmethoxy)carbonyl chloride
12-Aminododecanoic acid
9-fluorenylmethoxycarbonyl-12-aminododecanoic acid
Conditions | Yield |
---|---|
With sodium hydroxide In 1,4-dioxane; water | 90% |
With sodium carbonate In 1,4-dioxane at 0 - 20℃; | 78.3% |
With sodium carbonate In 1,4-dioxane; water at 0 - 20℃; |
Conditions | Yield |
---|---|
In ethyl acetate | 90% |
4-chloro-2H-1-benzopyran-2-one
12-Aminododecanoic acid
Conditions | Yield |
---|---|
With copper(l) iodide; potassium carbonate In water at 80℃; Ullmann Condensation; Microwave irradiation; | 90% |
2,2,2-trichloro-1,1-dimethylethoxychloroformate
12-Aminododecanoic acid
12-(2,2,2-trichloro-1,1-dimethyl-ethoxycarbonylamino)-dodecanoic acid
Conditions | Yield |
---|---|
With sodium hydroxide In 1,4-dioxane at 20℃; for 0.166667h; Acylation; | 88.7% |
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; | 88% |
Conditions | Yield |
---|---|
Stage #1: 12-Aminododecanoic acid With sodium hydroxide In methanol Stage #2: pyridine-2-carbaldehyde In methanol at 20℃; for 12h; | 87% |
diisopropyl hydrogenphosphonate
12-Aminododecanoic acid
12-(diisopropoxy-phosphorylamino)-dodecanoic acid
Conditions | Yield |
---|---|
With triethylamine In tetrachloromethane; ethanol; water at 0 - 20℃; | 87% |
NBD chloride
12-Aminododecanoic acid
12-((7-nitrobenzo[c][1,2,5]oxadiazol-4-yl)amino)dodecanoic acid
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water; acetonitrile at 65℃; for 2h; | 87% |
With sodium hydrogencarbonate In methanol at 0 - 50℃; for 3.5h; | 81% |
With sodium hydrogencarbonate In methanol; water at 50℃; for 1.5h; | 64% |
Stage #1: 12-Aminododecanoic acid With sodium hydrogencarbonate In ethanol; water at 37℃; for 0.166667h; Inert atmosphere; Stage #2: NBD chloride In ethanol; water at 37℃; Inert atmosphere; | 56% |
With sodium hydrogencarbonate In methanol at 50℃; for 3h; | 36% |
12-Aminododecanoic acid
1,6,7,12-tetrachloro-perylene-3,4,9,10-tetracarboxylic acid dianhydride
Conditions | Yield |
---|---|
With propionic acid at 140℃; for 36h; Inert atmosphere; Schlenk technique; | 87% |
In 1-methyl-pyrrolidin-2-one at 20 - 65℃; for 1.5h; |
Conditions | Yield |
---|---|
With acetic acid at 20℃; for 2.5h; | 86% |
Conditions | Yield |
---|---|
With thionyl chloride at -10 - 20℃; | 86% |
With thionyl chloride | |
With acetyl chloride at 0℃; for 3h; Inert atmosphere; Reflux; |
Conditions | Yield |
---|---|
Stage #1: 12-Aminododecanoic acid With potassium hydroxide In 1,4-dioxane for 0.0833333h; Stage #2: 2,4-Dinitrofluorobenzene In 1,4-dioxane for 18h; | 86% |
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