CAS No.7204-46-8,N,N-DIETHYLTHIOUREA Suppliers

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N,N-diethylthiourea cas 7204-46-8Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

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Thiourea, N,N-diethyl-Appearance:Off white to slight yellow solid Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediates Transportation:By Sea,by Air,By courier

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N,N-diethylthiourea

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UkrOrgSynthesis Ltd.

N,N-diethylthiourea

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Synthetic route

: 351425-47-3
N,N-Diethyl-1H-benzotriazole-1-carboximidamide

: 7204-46-8
1,1-diethylthiourea

Conditions

Conditions	Yield
With hydrogen sulfide In tetrahydrofuran at 20℃; for 1h;	92%

: 58328-36-2
N,N-diethyl-N'-benzoyl-thiourea

: 7204-46-8
1,1-diethylthiourea

Conditions

Conditions	Yield
With hydrazine at 25℃; for 0.166667h;	89%
With water

: sodium thiocyanate

: 541-41-3
chloroformic acid ethyl ester

: 109-89-7
diethylamine

: 7204-46-8
1,1-diethylthiourea

Conditions

Conditions	Yield
Stage #1: sodium thiocyanate; chloroformic acid ethyl ester With pyridine In acetonitrile at 5 - 20℃; Inert atmosphere; Stage #2: diethylamine In acetonitrile at 5 - 20℃; Inert atmosphere; Stage #3: With hydrazine hydrate In water at 50℃; for 4h; Inert atmosphere;	66%

...Expand

: 1147550-11-5
ammonium thiocyanate

: 109-89-7
diethylamine

: 7204-46-8
1,1-diethylthiourea

Conditions

Conditions	Yield
In water at 80 - 90℃;	61%

: C5H11ClN2*ClH

: 7204-46-8
1,1-diethylthiourea

Conditions

Conditions	Yield
With LiAlHSH In tetrahydrofuran at 0℃; for 3h;	55%

: 109-89-7
diethylamine

: 532-55-8
Benzoyl isothiocyanate

: 7204-46-8
1,1-diethylthiourea

Conditions

Conditions	Yield
With hydrazine hydrate In 1,2-dichloro-ethane at 20℃; for 6h;	54%

: 617-83-4
Diethylcyanamide

: 7204-46-8
1,1-diethylthiourea

Conditions

Conditions	Yield
With pyridine; hydrogen sulfide; triethylamine
With hydrogen sulfide; ammonia
With O,O-Diethyl hydrogen phosphorodithioate In diethyl ether

: 3487-55-6
diethylammonium thiocyanate

: 7204-46-8
1,1-diethylthiourea

Conditions

Conditions	Yield
at 105℃; Geschwindigkeit der Isomerisierung;

: 14327-03-8
N,N-Diethyl-N'-tert.-butyl-thioharnstoff

: 7204-46-8
1,1-diethylthiourea

Conditions

Conditions	Yield
With hydrogenchloride Heating;

: 66365-41-1
triphenylphosphine thiocyanogen

: 109-89-7
diethylamine

: 7204-46-8
1,1-diethylthiourea

Conditions

Conditions	Yield
(i) MeCN, CH2Cl2, (ii) H2O; Multistep reaction;
In dichloromethane; acetonitrile

: 333-20-0
potassium thioacyanate

: 109-89-7
diethylamine

: 7204-46-8
1,1-diethylthiourea

Conditions

Conditions	Yield
(i) ClCO2Et, acetone, (ii) /BRN= 605268/, (iii) aq. HCl; Multistep reaction;

: 132625-72-0
C8H16N2O2S

: 7204-46-8
1,1-diethylthiourea

Conditions

Conditions	Yield
With hydrogenchloride at 80℃; for 8h; Yield given;

: 3282-30-2
pivaloyl chloride

: 109-89-7
diethylamine

: 7204-46-8
1,1-diethylthiourea

Conditions

Conditions	Yield
With sodium hydroxide In hydrogenchloride; acetone

: ammonium thiocyanate

: 109-89-7
diethylamine

: 7204-46-8
1,1-diethylthiourea

Conditions

Conditions	Yield
In water at 80 - 90℃;

: 7204-46-8
1,1-diethylthiourea

: 532-27-4
1-chloroacetophenone

: 75654-98-7
2-diethylamino-4-phenylthiazole

Conditions

Conditions	Yield
In isopropyl alcohol for 1h; Heating; Reflux;	97%

: 7204-46-8
1,1-diethylthiourea

: 107-14-2
chloroacetonitrile

: Diethyl-(4-imino-4,5-dihydro-thiazol-2-yl)-amine; hydrochloride

Conditions

Conditions	Yield
In ethanol for 1h; Heating;	92%

: 18829-56-6
(E)-2-Nonenal

: 7204-46-8
1,1-diethylthiourea

: 104504-02-1
4-methyl-N-(tosyloxy)benzenesulfonamide

: 1353053-43-6
(R)-N-(1-(2-(diethylamino)thiazol-5-yl)heptyl)-4-methylbenzenesulfonamide

Conditions

Conditions	Yield
Stage #1: (E)-2-Nonenal; 4-methyl-N-(tosyloxy)benzenesulfonamide With (S)-2-{bis[3,5-bis(trifluoromethyl)phenyl][(trimethylsilanyl)oxy]methyl}pyrrolidine; sodium acetate In toluene at 20℃; for 24h; Stage #2: 1,1-diethylthiourea In toluene at 60℃; for 1.5h;	92%

...Expand

: 7204-46-8
1,1-diethylthiourea

: 99-94-5
p-Toluic acid

: N-(diethylcarbamothioyl)-4-methylbenzamide

Conditions

Conditions	Yield
With potassium fluoride on basic alumina; N,N-dimethyl-formamide at 20 - 105℃; for 0.0666667h; Product distribution; Further Variations:; Reagents; Temperatures; heating instead of irradiation; Acylation; Irradiation;	85%
With potassium fluoride on basic alumina; N,N-dimethyl-formamide at 20 - 105℃; for 0.0666667h; Acylation; Irradiation;	85%

: 3739-94-4
2,6-Pyridinedicarbonyl dichloride

: 7204-46-8
1,1-diethylthiourea

: N2,N6-bis(diethylcarbamothioyl)pyridine-2,6-dicarboxamide

Conditions

Conditions	Yield
With triethylamine In tetrahydrofuran at 40℃; for 1h;	78%
With triethylamine In acetone at 20 - 60℃; for 3h;	68%
With triethylamine In tetrahydrofuran at 0 - 50℃; for 2h; Inert atmosphere;	7.27 g
In N,N-dimethyl-formamide

: 7204-46-8
1,1-diethylthiourea

: 4637-24-5
N,N-dimethyl-formamide dimethyl acetal

: C8H17N3S

Conditions

Conditions	Yield
In dichloromethane for 2h;	77%

: 7204-46-8
1,1-diethylthiourea

A: 617-83-4
Diethylcyanamide

B: 3,5-bis(diethylamino)-1,2,4-thiadiazole

Conditions

Conditions	Yield
With diethoxydisulfane In tetrachloromethane for 7h; Heating;	A 5% B 75%

: 7204-46-8
1,1-diethylthiourea

: 70-11-1
α-bromoacetophenone

: 75654-98-7
2-diethylamino-4-phenylthiazole

Conditions

Conditions	Yield
In ethanol for 0.666667h; Heating;	75%

: 7204-46-8
1,1-diethylthiourea

: 5469-26-1
1-Bromopinacolon

: 83893-94-1
(4-tert-Butyl-thiazol-2-yl)-diethyl-amine

Conditions

Conditions	Yield
In ethanol for 0.666667h; Heating;	65%

: 7204-46-8
1,1-diethylthiourea

: 65739-39-1
2,2′-bipyridine-6,6′-dicarbonyl dichloride

: 2,2′-bipyridine-6,6′-dicarbonyl bis(N,N-diethylthiourea)

Conditions

Conditions	Yield
Stage #1: 1,1-diethylthiourea; 2,2′-bipyridine-6,6′-dicarbonyl dichloride With triethylamine In tetrahydrofuran at 20℃; for 1h; Stage #2: With triethylamine In tetrahydrofuran at 50℃; for 0.75h;	65%

: 24238-62-8
3-(2-bromoacetyl)-4-hydroxy-2H-chromen-2-one

: 7204-46-8
1,1-diethylthiourea

: 944548-98-5
3-(2-diethylamino-thiazol-4-yl)-4-hydroxychromen-2-one

Conditions

Conditions	Yield
In ethanol Hantzsch reaction; Reflux;	63.34%
In ethanol Reflux;

: 7204-46-8
1,1-diethylthiourea

: 78-95-5
chloroacetone

: 164397-12-0
diethyl-(4-methyl-thiazol-2-yl)-amine

Conditions

Conditions	Yield
In ethanol for 0.666667h; Heating;	60%
With water

: 7204-46-8
1,1-diethylthiourea

: 534-07-6
1,3-Dichloroacetone

: 4-(chloromethyl)-N,N-diethylthiazol-2-amine

Conditions

Conditions	Yield
In ethanol at 80℃; for 16h;	53%
In acetone

: 7204-46-8
1,1-diethylthiourea

: 57375-25-4
3-bromorifamicin S

: 113102-19-5
2'-(N,N-diethylamino)rifamycin P

Conditions

Conditions	Yield
In methanol for 1.5h; Ambient temperature;	49%

: 18829-56-6
(E)-2-Nonenal

: 7204-46-8
1,1-diethylthiourea

: 1353053-42-5
(R)-1-(2-(diethylamino)thiazol-5-yl)heptan-1-ol

Conditions

Conditions	Yield
Stage #1: (E)-2-Nonenal With (S)-2-{bis[3,5-bis(trifluoromethyl)phenyl][(trimethylsilanyl)oxy]methyl}pyrrolidine; dihydrogen peroxide In water; toluene at 20℃; for 24h; Stage #2: 1,1-diethylthiourea In water; toluene at 20℃; for 3h; enantioselective reaction;	45%

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