CAS No.534-07-6,1,3-Dichloroacetone Suppliers

Hunan Russell Chemicals Technology Co.,Ltd

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1,3-Dichloroacetone, 96% 534-07-6

Cas:534-07-6

Min.Order:0

Negotiable

Type:Trading Company

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Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

Amadis Chemical offer CAS#534-07-6;CAT#A829568

Cas:534-07-6

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

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Pure Chemistry Scientific Inc.

1,3-Dichloroacetone Application:80016991

1,3-Dichloroacetone

Cas:534-07-6

Min.Order:1 Gram

FOB Price: $500.0

Type:Trading Company

inquiry

Synthetic route

: 816-39-7
1,3-dibromoroacetone

: 534-07-6
1,3-Dichloroacetone

Conditions

Conditions	Yield
With potassium chloride In water at 20 - 60℃; for 0.333333h;	98%

: 53535-68-5
bromo-3-chloro-propanone

: 1001-58-7
3-mercaptopropionitrile

A: 1-bromo-3-(2-cyanoethylthio)propanone

B: 534-07-6
1,3-Dichloroacetone

Conditions

Conditions	Yield
	A 94% B n/a

...Expand

: 96-23-1
1,3-Dichloro-2-propanol

: 534-07-6
1,3-Dichloroacetone

Conditions

Conditions	Yield
With periodic acid In acetonitrile at 20℃; for 3h; Reagent/catalyst; Solvent; Temperature;	80%
With chromic acid
With chromium(III) oxide; sulfuric acid

: 593-71-5
Chloroiodomethane

: 105-39-5
chloroacetic acid ethyl ester

: 534-07-6
1,3-Dichloroacetone

Conditions

Conditions	Yield
With methyllithium; lithium bromide In tetrahydrofuran; diethyl ether at -78℃; for 0.333333h;	60%
Yield given. Multistep reaction;

: 55549-51-4
2,4-Dichlor-3-aminocrotonsaeurenitril

: 534-07-6
1,3-Dichloroacetone

Conditions

Conditions	Yield
With hydrogenchloride for 72h;	58%

: 82313-45-9
(Z)-1,3-Dichlor-2,4,4-trimorpholino-1,3-butadien-1-carbonitril

: 534-07-6
1,3-Dichloroacetone

Conditions

Conditions	Yield
With hydrogenchloride at 60 - 70℃; for 10h; 2) Et2O, heating;	15%

: 186581-53-3, 908094-01-9
diazomethane

: 75-44-5
phosgene

: 60-29-7
diethyl ether

: 534-07-6
1,3-Dichloroacetone

...Expand

: 186581-53-3, 908094-01-9
diazomethane

: 75-44-5
phosgene

: 534-07-6
1,3-Dichloroacetone

Conditions

Conditions	Yield
With diethyl ether

: 78-88-6
2,3-Dichloroprop-1-ene

: 534-07-6
1,3-Dichloroacetone

Conditions

Conditions	Yield
With hypochloric acid

: 53535-68-5
bromo-3-chloro-propanone

A: 816-39-7
1,3-dibromoroacetone

B: 534-07-6
1,3-Dichloroacetone

Conditions

Conditions	Yield
beim partielle Disproportionierung;

: 463-49-0
1,2-propanediene

: 534-07-6
1,3-Dichloroacetone

Conditions

Conditions	Yield
With hypochloric acid

: 108-20-3
di-isopropyl ether

: 534-07-6
1,3-Dichloroacetone

Conditions

Conditions	Yield
With chlorine at -20℃; im Licht;

: 6305-40-4
1,3-diiodopropan-2-one

: 534-07-6
1,3-Dichloroacetone

Conditions

Conditions	Yield
With silver(I) chloride

: 20485-53-4
1-chloro-3-diazopropan-2-one

: 534-07-6
1,3-Dichloroacetone

Conditions

Conditions	Yield
With hydrogenchloride
With hydrogenchloride In diethyl ether for 4h; Heating; Yield given;

: 67-64-1
acetone

: 534-07-6
1,3-Dichloroacetone

Conditions

Conditions	Yield
With chlorine; nickel dichloride

: 67-64-1
acetone

A: 513-88-2
1,1-Dichloroacetone

B: 534-07-6
1,3-Dichloroacetone

Conditions

Conditions	Yield
With iron(III) chloride at 45℃; bei der Chlorierung;
With chlorine In tetrachloromethane Product distribution; 1.) below 40 deg C, 2.) room temperature, 0.5 h;	A 67 % Chromat. B 33 % Chromat.
With chlorine; acetic acid
With hydrogenchloride; chlorine
With antimonypentachloride; chlorine

: 106-89-8
epichlorohydrin

A: 96-23-1
1,3-Dichloro-2-propanol

B: 534-07-6
1,3-Dichloroacetone

Conditions

Conditions	Yield
With disulfur dichloride beim Siedetemperatur;
With disulfur dichloride

: 2881-95-0
α,α-Bis-Chlormethyl-α-hydroxy-essigsaeure-anhydrosulfit

: 534-07-6
1,3-Dichloroacetone

Conditions

Conditions	Yield
In chlorobenzene Heating;

: 463-49-0
1,2-propanediene

A: 60367-21-7
dichloride of 1-chloro-2-propene-2-phosphonic acid

B: 40632-73-3
dichloride of 2-chloro-2-propene-1-phosphonic acid

C: 534-07-6
1,3-Dichloroacetone

Conditions

Conditions	Yield
With oxygen; phosphorus trichloride Product distribution;

...Expand

: 96-23-1
1,3-Dichloro-2-propanol

A: 921-03-9
1,1,3-trichloroacetone

B: 534-07-6
1,3-Dichloroacetone

Conditions

Conditions	Yield
With ruthenium(IV) oxide; sodium chloride In water; ethyl acetate at 5℃; Product distribution; other organic solvents;	A 1 % Chromat. B 62 % Chromat.

: 82598-72-9
1,3-dichloro-2,2-propanediol

: 534-07-6
1,3-Dichloroacetone

Conditions

Conditions	Yield
With dehydration at 25℃; Rate constant; Equilibrium constant; Thermodynamic data; ΔH(excit.), ΔS(excit.), ΔG(excit.); isotope effects;
With water In acetonitrile Equilibrium constant; various temperatures (15-46 deg C), isotope effect;

: 110-63-4
Butane-1,4-diol

: 67-64-1
acetone

A: 513-88-2
1,1-Dichloroacetone

B: 2-Chloromethyl-2-methyl-[1,3]dioxepane

C: 77416-10-5
2,2-Bis(chloromethyl)-1,3-dioxacycloheptane

D: 146774-72-3
2-dichloromethyl-2-methyl-1,3-dioxepane

E: 78-95-5
chloroacetone

F: 534-07-6
1,3-Dichloroacetone

Conditions

Conditions	Yield
With chlorine Product distribution; 1.) 20-50 deg C, 2.) room temperature, 0.5 h;	A n/a B n/a C 28.3 % Chromat. D 13.8 % Chromat. E n/a F n/a

...Expand

: 110-63-4
Butane-1,4-diol

: 67-64-1
acetone

A: 513-88-2
1,1-Dichloroacetone

B: 77416-10-5
2,2-Bis(chloromethyl)-1,3-dioxacycloheptane

C: 146774-72-3
2-dichloromethyl-2-methyl-1,3-dioxepane

D: 534-07-6
1,3-Dichloroacetone

Conditions

Conditions	Yield
With chlorine 1) 20-50 deg C; 2) room temp., 0.5 h; Further byproducts given. Yields of byproduct given;	A n/a B 28.3 % Chromat. C n/a D n/a

...Expand

: 67-64-1
acetone

A: 513-88-2
1,1-Dichloroacetone

B: 78-95-5
chloroacetone

C: 534-07-6
1,3-Dichloroacetone

Conditions

Conditions	Yield
With hydrogenchloride at 23 - 25℃; electrochemical; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
With hydrogenchloride at 23 - 25℃; electrochemical; Yield given. Yields of byproduct given;
With hydrogenchloride at 22 - 25℃; Product distribution; function of current and concentration;

...Expand

: 106-89-8
epichlorohydrin

disulfur dichloride: disulfur dichloride

A: 96-23-1
1,3-Dichloro-2-propanol

B: 534-07-6
1,3-Dichloroacetone

...Expand

α.γ-dichloro-acetoacetic acid ester: α.γ-dichloro-acetoacetic acid ester

: 534-07-6
1,3-Dichloroacetone

Conditions

Conditions	Yield
With sulfuric acid

chloro-ethoxy-acetoacetic acid ester: chloro-ethoxy-acetoacetic acid ester

: 534-07-6
1,3-Dichloroacetone

Conditions

Conditions	Yield
With hydrogenchloride

symm.glycerol chlorohydrin: symm.glycerol chlorohydrin

: 534-07-6
1,3-Dichloroacetone

: 6294-89-9
hydrazinecarboxylic acid methyl ester

: 534-07-6
1,3-Dichloroacetone

: 87595-89-9
methyl 2-[2-chloro-1-(chloromethyl)ethylidene]-1-hydrazinecarboxylate

Conditions

Conditions	Yield
In diethyl ether for 15h; Ambient temperature;	100%
In methanol at 23℃; for 4h;	54%
for 3h; Ambient temperature; Yield given;
In methanol at 23℃; for 4h;

: 534-07-6
1,3-Dichloroacetone

: O-(1-E-cinnamyl)hydroxylamine hydrochloride

: 215599-97-6
(E)-1,3-dichloroacetone O-(3-phenyl-2-propenyl)oxime

Conditions

Conditions	Yield
In methanol at 40℃; for 2h;	100%

: 534-07-6
1,3-Dichloroacetone

: 1-morpholino-3-(morpholinomethylene)thiourea

: 373602-92-7
bis-(2-morpholin-4-yl-thiazol-5-yl)-methanone

Conditions

Conditions	Yield
Stage #1: 1,3-Dichloroacetone; 1-morpholino-3-(morpholinomethylene)thiourea In acetonitrile for 2h; Heating; Stage #2: With triethylamine In acetonitrile	100%

: 534-07-6
1,3-Dichloroacetone

: 682353-67-9
1,3-diazido-propan-2-one

Conditions

Conditions	Yield
With sodium azide In acetone at 20℃;	100%
With sodium azide In acetone at 20℃; for 12h;	96%
With sodium azide In acetone at 20℃; for 12h;	96%

: 85102-68-7
2-N-piperidino-5-methyl-1,3-dithiolium-4-thiolate

: 534-07-6
1,3-Dichloroacetone

: 1,3-bis(5-methyl-2-piperidinio-1,3-dithiol-4-ylsulfanyl)propan-2-one dichloride

Conditions

Conditions	Yield
In acetone	100%

: 6258-60-2
p-methoxybenzylmercaptan

: 534-07-6
1,3-Dichloroacetone

: 1,3-bis-(4-methoxy-benzylsulfanyl)-propan-2-one

Conditions

Conditions	Yield
With sodium methylate In ethanol for 1.5h; Heating;	100%

: 2362-64-3
p-methoxythiobenzamide

: 534-07-6
1,3-Dichloroacetone

: 4-methoxy-thiobenzimidic acid 3-chloro-2-oxo-propyl ester hydrochloride

Conditions

Conditions	Yield
In acetone at 20℃; for 72h;	100%

: 78950-30-8
4-cyanobenzothioamide

: 534-07-6
1,3-Dichloroacetone

: 873009-61-1
C11H7ClN2S

Conditions

Conditions	Yield
In ethanol for 3h; Heating / reflux;	100%

: 534-07-6
1,3-Dichloroacetone

: 196811-66-2
4-(tert-butoxycarbonyl)piperazine-1-thiocarboxamide

: 4-(4-chloromethylthiazol-2-yl)piperazine-1-carboxylic acid tert-butyl ester

Conditions

Conditions	Yield
With sodium hydrogencarbonate In ethyl acetate; 1,2-dichloro-ethane	100%

: 6967-89-1
naphthalene-2-carbothioamide

: 534-07-6
1,3-Dichloroacetone

: 1094428-16-6
4-(chloromethyl)-2-(naphthalen-6-yl)thiazole

Conditions

Conditions	Yield
In ethanol Heating;	100%

: 1424835-11-9
6-fluoronaphthalene-2-carbothioamide

: 534-07-6
1,3-Dichloroacetone

: 1424835-28-8
4-(chloromethyl)-2-(2-fluoronaphthalen-6-yl)thiazole

Conditions

Conditions	Yield
In ethanol Heating;	100%

: 534-07-6
1,3-Dichloroacetone

: 122-52-1
triethyl phosphite

: 81431-81-4
3-chloro-2-<(diethoxyphosphoryl)oxy>-1-propene

Conditions

Conditions	Yield
at 100℃;	99%
In dichloromethane for 166h; Ambient temperature;	98%
at 60 - 100℃; for 3h;	98.9%
at 50℃;

: 534-07-6
1,3-Dichloroacetone

: 35433-52-4
1,3-dichloroacetone oxime

Conditions

Conditions	Yield
With sulfuric acid; hydroxylamine hydrochloride In ethanol at 20℃; for 2h; Inert atmosphere;	99%
With hydroxylamine

: 95-14-7
1,2,3-Benzotriazole

: 534-07-6
1,3-Dichloroacetone

: 1,3-bis-(benzotriazol-1-yl)propan-2-one

Conditions

Conditions	Yield
In benzene for 48h; Heating;	99%

: 617-86-7
triethylsilane

: 534-07-6
1,3-Dichloroacetone

: 7531-61-5
((1,3-dichloropropan-2-yl)oxy)triethylsilane

Conditions

Conditions	Yield
Stage #1: 1,3-Dichloroacetone With C8H10BiCl2N; C4H6AgN2(1+)*C24H12BCl8(1-) In dichloromethane-d2 at 25℃; Stage #2: triethylsilane In dichloromethane at 25℃;	99%
With C24H36AlN2O2(1+)*C24H12BCl8(1-) In benzene-d6 for 15h; Inert atmosphere; Schlenk technique; Glovebox;	98 %Spectr.

: 96-45-7
N,N'-ethylenethiourea

: 534-07-6
1,3-Dichloroacetone

: 3-(chloromethyl)-5,6-dihydroimidazo[2,1-b]thiazole hydrochloride

Conditions

Conditions	Yield
In acetonitrile at 80℃; Inert atmosphere;	99%

: 534-07-6
1,3-Dichloroacetone

: 2227-79-4
benzenecarbothioamide

: 4771-31-7
2-phenyl-4-chloromethylthiazole

Conditions

Conditions	Yield
In ethanol for 4h; Reflux;	98%
In ethanol for 2h; Reflux;	90%
Stage #1: 1,3-Dichloroacetone; benzenecarbothioamide In acetone Inert atmosphere; Reflux; Stage #2: With sulfuric acid for 0.5h; Inert atmosphere;	85%

: 534-07-6
1,3-Dichloroacetone

: 603-35-0
triphenylphosphine

: 13605-65-7
(3-chloro-2-oxopropyl)triphenylphosphonium chloride

Conditions

Conditions	Yield
In tetrahydrofuran for 24h; Reflux;	98%
In benzene at 20℃; for 6h;	98%
In tetrahydrofuran at 70℃; for 5h;	97%

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 534-07-6
1,3-Dichloroacetone

: 188125-86-2
1,3-dichloro-2-propanone O-benzyloxime

Conditions

Conditions	Yield
In ethanol Ambient temperature;	98%
In ethanol at 20℃; for 24h;	2.32 g

: 62-55-5
thioacetamide

: 534-07-6
1,3-Dichloroacetone

: 39238-07-8
4-(chloromethyl)-2-methyl-1,3-thiazole

Conditions

Conditions	Yield
In acetone	97%
at 20 - 50℃; for 20h;	93%
	92.9%

: 582-25-2
Potassium benzoate

: 534-07-6
1,3-Dichloroacetone

: 38982-27-3
1,3-Dibenzoyl-1,3-dihydroxyacetone

Conditions

Conditions	Yield
5,11,17,23,29,35-Hexa-p-tert-butyl-37,38,39,40,41,42-hexakis-(3,6,9-trioxadecyloxy)calix<6>arene In water; acetonitrile at 65℃; for 6h;	97%
With ethanol

: 126-30-7
2,2-Dimethyl-1,3-propanediol

: 534-07-6
1,3-Dichloroacetone

: 133961-12-3
2,2-bis-(chloromethyl)-5,5-dimethyl-1,3-dioxane

Conditions

Conditions	Yield
With toluene-4-sulfonic acid In benzene Heating;	97%
With toluene-4-sulfonic acid In benzene for 19h; Heating;	97%
With toluene-4-sulfonic acid In benzene for 18h; Heating;	97%

: 72505-21-6
4-trifluoromethylbenzthioamide

: 534-07-6
1,3-Dichloroacetone

: 135873-35-7
4-chloromethyl-2-[4-(trifluoromethyl)phenyl]thiazole

Conditions

Conditions	Yield
In toluene Reflux;	97%
In toluene at 80℃; for 4h;	62%
With thionyl chloride; sodium hydrogencarbonate 1.) 1,2-dichloroethane; Multistep reaction;
In 1,2-dichloro-ethane at 130 - 140℃; for 5h; Sealed tube;

: 534-07-6
1,3-Dichloroacetone

: 603-35-0
triphenylphosphine

: 13605-66-8
1-chloro-3-(triphenylphosphoranylidene)acetone

Conditions

Conditions	Yield
Stage #1: 1,3-Dichloroacetone; triphenylphosphine In tetrahydrofuran for 4h; Heating; Stage #2: With sodium carbonate In methanol at 20℃; for 0.5h;	97%
Stage #1: 1,3-Dichloroacetone; triphenylphosphine In tetrahydrofuran for 24h; Heating; Stage #2: With sodium hydrogencarbonate In water Further stages.;	92%
In tetrahydrofuran for 24h; Heating;	91%

: 17356-08-0
thiourea

: 534-07-6
1,3-Dichloroacetone

: 4-(chloromethyl)thiazol-2-amine hydrochloride

Conditions

Conditions	Yield
In acetone at 20 - 25℃; for 72h;	97%

: 534-07-6
1,3-Dichloroacetone

: 149-73-5
trimethyl orthoformate

: 6626-57-9
1,3-dichloroacetone dimethyl acetal

Conditions

Conditions	Yield
With Amberlyst 15 In dichloromethane	96%

: 534-07-6
1,3-Dichloroacetone

: 18435-67-1
o-methoxycarbonyl-α-diazoacetophenone

: 10,10-Bis-chloromethyl-1-methoxy-11,12-dioxa-tricyclo[7.2.1.02,7]dodeca-2(7),3,5-trien-8-one

Conditions

Conditions	Yield
With copper acetylacetonate In benzene for 1h; Heating;	96%

: 16982-21-1
ethyl 2-amino-2-thioxoacetate

: 534-07-6
1,3-Dichloroacetone

: 100960-16-5
4-(chloromethyl)thiazole-2-carboxylic acid-ethyl ester

Conditions

Conditions	Yield
In toluene at 110℃; for 2h;	96%
In ethanol Heating / reflux;	37%
In ethanol for 15h; Heating;
In toluene for 2h; Inert atmosphere; Reflux;
In toluene Reflux;

: 591-51-5
phenyllithium

: 534-07-6
1,3-Dichloroacetone

: 87234-28-4
1,3-dichloro-2-hydroxy-2-phenylpropane

Conditions

Conditions	Yield
Stage #1: phenyllithium With cerium(III) chloride In tetrahydrofuran; diethyl ether; cyclohexane at -78℃; for 0.666667h; Stage #2: 1,3-Dichloroacetone In tetrahydrofuran; diethyl ether; cyclohexane at -78℃; for 0.166667h;	96%

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