CAS No.463-58-1,Carbonyl sulfide Suppliers

Dayang Chem (Hangzhou) Co.,Ltd.

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Carbonyl sulfide

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Thioxomethanone

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Sulfanylidenemethanone

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Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates

Carbon oxide sulfide(COS)

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Zhuozhou Wenxi import and Export Co., Ltd

Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard

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Antimex Chemical Limied

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Shanghai united Scientific Co.,Ltd.

United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat

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carbonyl sulphide

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Chemical Co.Ltd

Manufacturer,strong R&D,professional team Storage:Store in a cool, dry place. Store in a tightly closed container. Package:according to your requirement Application:ZhiShang Chemical is owned by ZhiShang Group, is a professional new-type chemicals en

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Sigma-Aldrich Chemie GmbH

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Carbonyl sulfide

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Matheson Tri-Gas

CARBONYL SULFIDE

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Estoniya AGA, AO

Carbon oxide sulfide(COS)

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Linde North America Inc.

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Engineered Controls International, Inc

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Specialty Gases of America, Inc

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Synthetic route

: 201230-82-2
carbon monoxide

: 7446-09-5
sulfur dioxide

A: 463-58-1
carbon oxide sulfide

B: 7704-34-9
sulfur

Conditions

Conditions	Yield
With catalyst: La2O3-TiO2 highest activity with 1:1 La:Ti ratio; 500°C, 1 atm, in the presence of N2;	A <1 B 95%
With catalyst: Fe-Al2O3 byproducts: CO2; highest SO2 reduction with 40 % Fe in the catalyst, maximum COS yield at 400°C;
With catalyst: Cu-Al2O3 H2O vapour diminishes catalyst activity;

...Expand

: 7218-04-4, 26117-28-2, 616-91-1
N-Acetylcysteine

: 2-(((3-acetamido-4-methoxy-2-methyl-4-oxobutan-2-yl)disulfanecarbonyl)(methyl)amino)-N-methylethan-1-aminium trifluoroacetate

A: 80-73-9
1,3-dimethyl-2-imidazolidinone

B: 463-58-1
carbon oxide sulfide

C: 5545-17-5, 97247-12-6, 139602-29-2
N,N'-bis(acetyl)cystine

D: C13H25N3O4S2*H(1+)

E: C13H22N2O6S3

F: C13H22N2O6S4

G: C13H22N2O6S5

H: C16H28N2O6S5

I: C16H28N2O6S6

J: 76480-10-9
C16H28N2O6S3

K: 76480-11-0
C16H28N2O6S4

L: 83151-19-3
1-Acetamido-1-(carbomethoxy)-2-methyl-2-propyl Hydrodisulfide

Conditions

Conditions	Yield
With diethylenetriaminopentaacetic acid In aq. buffer at 37℃; pH=7.4;	A 87% B n/a C n/a D n/a E n/a F n/a G n/a H n/a I n/a J n/a K n/a L n/a

...Expand

: 93097-85-9
di-O-isopropyl-S,S-phthaloyl dixanthate (unsymmetrical)

A: 5698-59-9
benzo[c]thiophene-1,3-dione

B: 463-58-1
carbon oxide sulfide

C: 57542-45-7
O,S-diisopropyl xanthate

D: 19357-64-3
Biphthalidyliden

Conditions

Conditions	Yield
at 250℃; for 0.5h; other dixanthate;	A 29% B 82% C 16% D 24%

...Expand

: graphite

: 7446-09-5
sulfur dioxide

A: 75-15-0
carbon disulfide

B: 23550-45-0
disulfur

C: 463-58-1
carbon oxide sulfide

Conditions

Conditions	Yield
byproducts: CO, CO2; at 1400 K, with excess of carbon;	A 81.16% B 10.82% C 8.02%
byproducts: CO, CO2; at 1000 K, with excess of carbon;	A 37.08% B 3.22% C 59.7%

...Expand

: C42H70O35*C11H12OS2

A: 463-58-1
carbon oxide sulfide

B: 59117-56-5
E-(3-phenylallyl) methyl sulfide

Conditions

Conditions	Yield
In neat (no solvent) at 120℃; for 6h; Rate constant; Product distribution;	A n/a B 81%

: 103-72-0
phenyl isothiocyanate

: 215675-49-3
1-cyclohexyl-4,5-diphenylimidazole 3-oxide

A: 463-58-1
carbon oxide sulfide

B: 1-cyclohexyl-4,5-diphenyl-2-(phenylamino)imidazole

Conditions

Conditions	Yield
In dichloromethane at 20℃; for 20h; Cycloaddition; elimination;	A n/a B 81%

...Expand

: 556-61-6
methyl thioisocyanate

: 215675-47-1
1-methyl-4,5-diphenyl-1H-imidazole 3-oxide

A: 463-58-1
carbon oxide sulfide

B: 2-methylamino-1-methyl-4,5-diphenylimidazole

Conditions

Conditions	Yield
In dichloromethane at 20℃; for 20h; Cycloaddition; elimination;	A n/a B 76%

...Expand

: 77420-85-0
1,4-diphenyl-1-ethylxanthyl-2,3-diazabutadiene

A: 463-58-1
carbon oxide sulfide

B: 1456-21-9
diphenyl-[1,3,4]thiadiazole

Conditions

Conditions	Yield
at 240℃; for 20h; sealed tube;	A n/a B 69%

: 103-72-0
phenyl isothiocyanate

: 55738-12-0
1-benzyl-4,5-dimethyl-1H-imidazole 3-oxide

A: 463-58-1
carbon oxide sulfide

B: 1-benzyl-4,5-dimethyl-2-(phenylamino)imidazole

Conditions

Conditions	Yield
In dichloromethane at 20℃; for 20h; Cycloaddition; elimination;	A n/a B 58%

...Expand

: 7218-04-4, 26117-28-2, 616-91-1
N-Acetylcysteine

: C15H19NO5S2

A: 463-58-1
carbon oxide sulfide

B: 39239-85-5
methyl 2-acetamido-3-mercapto-3-methylbutanoate

C: C13H22N2O6S3

D: C16H28N2O6S5

E: C16H28N2O6S6

F: C12H13NO5S

G: C14H22N2O7S3

H: 76480-10-9
C16H28N2O6S3

I: 76480-11-0
C16H28N2O6S4

Conditions

Conditions	Yield
With diethylenetriaminopentaacetic acid; ammonium bicarbonate In aq. buffer at 37℃; pH=7.4; Mechanism; Reagent/catalyst; Solvent;	A n/a B n/a C n/a D n/a E n/a F 53% G n/a H n/a I n/a

...Expand

: 73388-91-7
4-allylthio-3,3,4-triphenyl-2-thietanone

A: 463-58-1
carbon oxide sulfide

B: 2168-78-7
methyl dithiobenzoate

C: 86931-20-6
1-allylthio-1,1,2-triphenylethylene

D: 525-06-4
diphenyl ketene

Conditions

Conditions	Yield
at 170℃; for 1.5h;	A n/a B n/a C 50% D n/a

...Expand

: 73388-91-7
4-allylthio-3,3,4-triphenyl-2-thietanone

A: 463-58-1
carbon oxide sulfide

B: 27249-64-5
allyl dithiobenzoate

C: 86931-20-6
1-allylthio-1,1,2-triphenylethylene

D: 525-06-4
diphenyl ketene

Conditions

Conditions	Yield
at 170℃; for 1.5h;	A n/a B n/a C 50% D n/a

...Expand

: S8(2+)*2AsF6(1-) = S8(AsF6)2

: 201230-82-2
carbon monoxide

: 463-58-1
carbon oxide sulfide

Conditions

Conditions	Yield
In liquid sulphur dioxide	20%

: 7218-04-4, 26117-28-2, 616-91-1
N-Acetylcysteine

: 3-(((3-acetamido-4-methoxy-2-methyl-4-oxobutan-2-yl)disulfanecarbonyl)(methyl)amino)-N-methylpropan-1-aminium trifluoroacetate

A: 7226-23-5
1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone

B: 463-58-1
carbon oxide sulfide

C: 5545-17-5, 97247-12-6, 139602-29-2
N,N'-bis(acetyl)cystine

D: C13H22N2O6S2

E: 76480-10-9
C16H28N2O6S3

Conditions

Conditions	Yield
With diethylenetriaminopentaacetic acid In aq. buffer at 37℃; for 1h; pH=7.4;	A 19.2% B n/a C n/a D n/a E n/a

...Expand

: 7218-04-4, 26117-28-2, 616-91-1
N-Acetylcysteine

: 3-(((3-acetamido-4-methoxy-2-methyl-4-oxobutan-2-yl)disulfanecarbonyl)(methyl)amino)propan-1-aminium trifluoroacetate

A: 463-58-1
carbon oxide sulfide

B: 39239-85-5
methyl 2-acetamido-3-mercapto-3-methylbutanoate

C: 5545-17-5, 97247-12-6, 139602-29-2
N,N'-bis(acetyl)cystine

D: C13H22N2O6S2

E: C13H25N3O4S2*H(1+)

F: 76480-10-9
C16H28N2O6S3

G: 10166-54-8
1-methyltetrahydropyrimidin-2(1H)-one

Conditions

Conditions	Yield
With diethylenetriaminopentaacetic acid In aq. buffer at 37℃; pH=7.4;	A n/a B n/a C n/a D n/a E n/a F n/a G 5.9%

...Expand

: 23550-45-0
disulfur

A: 75-15-0
carbon disulfide

B: 463-58-1
carbon oxide sulfide

Conditions

Conditions	Yield
With carbon monoxide; platinum	A 1% B n/a

: 110-86-1
pyridine

: 2812-74-0
(Propoxy)thiocarbonylchlorid

A: 463-58-1
carbon oxide sulfide

B: 540-54-5
1-Chloropropane

...Expand

: 60-35-5
acetamide

: 75-15-0
carbon disulfide

: 463-58-1
carbon oxide sulfide

Conditions

Conditions	Yield
at 210℃;

: 91-22-5
quinoline

: 2812-74-0
(Propoxy)thiocarbonylchlorid

A: 463-58-1
carbon oxide sulfide

B: 540-54-5
1-Chloropropane

Conditions

Conditions	Yield
at 29℃;

...Expand

: 108-30-5
succinic acid anhydride

: 102-08-9
N,N-diphenylthiourea

A: 83-25-0
N-phenylmaleimide

B: 463-58-1
carbon oxide sulfide

C: 62-53-3
aniline

Conditions

Conditions	Yield
at 150 - 155℃;

...Expand

: 75-15-0
carbon disulfide

: 471-46-5
Oxalamide

: 463-58-1
carbon oxide sulfide

Conditions

Conditions	Yield
at 200℃;

: 75-15-0
carbon disulfide

: 15719-64-9, 15719-76-3, 97762-63-5
methylammonium carbonate

: 463-58-1
carbon oxide sulfide

Conditions

Conditions	Yield
With magnesium oxide

: 75-15-0
carbon disulfide

: 463-58-1
carbon oxide sulfide

Conditions

Conditions	Yield
With kaolin bei Weissglut;
With chlorosulfonic acid at 100℃;
With sulfur trioxide at 100℃;

: 75-44-5
phosgene

: 463-58-1
carbon oxide sulfide

Conditions

Conditions	Yield
With cadmium(II) sulphide at 260 - 280℃;
With magnesium bromide hydrosulfide; benzene unter Kuehlung,dann auf dem Wasserbad;
With hydrogen sulfide at 200℃; unter Druck;

: 85-44-9
phthalic anhydride

: 102-08-9
N,N-diphenylthiourea

A: 520-03-6
N-phenylphthalimide

B: 463-58-1
carbon oxide sulfide

C: 62-53-3
aniline

Conditions

Conditions	Yield
at 170 - 175℃;

...Expand

: 92-52-4
biphenyl

: dithiocarbonic acid O-cyclobutyl ester-S-methyl ester

A: 74-93-1
methylthiol

B: 463-58-1
carbon oxide sulfide

C: 106-99-0
buta-1,3-diene

...Expand

: 108-19-0
BIURET

: 463-58-1
carbon oxide sulfide

Conditions

Conditions	Yield
With hydrogen sulfide oberhalb der Schmelztemperatur;

: 463-58-1
carbon oxide sulfide

: 7722-84-1
dihydrogen peroxide

A: 124-38-9
carbon dioxide

B: 7664-93-9
sulfuric acid

C: 7732-18-5
water

Conditions

Conditions	Yield
With potassium sulfate; potassium hydrogensulfate; potassium peroxomonosulfate In water Kinetics; oxidation of OCS studied in round-bottom Pyrex bulbs, acid-water mixtures introduced into bulbs and degassed, bulb reactors filled with with a gas mixture slightly above 1 atm total pressure with a typical mixing ratio of OCS:Ar:He=40:60:700 Torr; gas chromy. and mass spectroscopy applied for determination of product content;	A 100% B n/a C n/a
With sulfuric acid In water Kinetics; oxidation of OCS studied in round-bottom Pyrex bulbs, acid-water mixtures introduced into bulbs and degassed, bulb reactors filled with with a gas mixture slightly above 1 atm total pressure with a typical mixing ratio of OCS:Ar:He=40:60:700 Torr; gas chromy. and mass spectroscopy applied for determination of product content;	A 100% B n/a C n/a

Yield

With potassium sulfate; potassium hydrogensulfate; potassium peroxomonosulfate In water Kinetics; oxidation of OCS studied in round-bottom Pyrex bulbs, acid-water mixtures introduced into bulbs and degassed, bulb reactors filled with with a gas mixture slightly above 1 atm total pressure with a typical mixing ratio of OCS:Ar:He=40:60:700 Torr; gas chromy. and mass spectroscopy applied for determination of product content;

A 100%
B n/a
C n/a

With sulfuric acid In water Kinetics; oxidation of OCS studied in round-bottom Pyrex bulbs, acid-water mixtures introduced into bulbs and degassed, bulb reactors filled with with a gas mixture slightly above 1 atm total pressure with a typical mixing ratio of OCS:Ar:He=40:60:700 Torr; gas chromy. and mass spectroscopy applied for determination of product content;

A 100%
B n/a
C n/a

...Expand

: 463-58-1
carbon oxide sulfide

: {C6(CH3)6H}Mn(CO)(P(OCH3)3)2

: {C6(CH3)6}Mn(CO)P(OCH3)3P(O)(OCH3)2

Conditions

Conditions	Yield
In tetrahydrofuran byproducts: HC(O)SCH3; inert gas; 2.5 h at room temperature; 40 psi COS;; depressurization; solvent removal in vacuo; chromy.;	100%

: 463-58-1
carbon oxide sulfide

: C36H60GeP3Rh

: C31H45GeOP2RhS

Conditions

Conditions	Yield
In toluene at -70.16 - 19.84℃; for 0.5h;	100%

: 35880-54-7, 61647-76-5, 184490-77-5, 65635-71-4
{ruthenium(0) dicarbonyltris(triphenylphosphine)}

: 463-58-1
carbon oxide sulfide

: 81027-57-8
Ru(CO)2(η2-COS)(PPh3)2

Conditions

Conditions	Yield
In toluene byproducts: PPh3; a suspn. of complex was stirred under atm. of COS for 5 min; dilution with hexane, filtration, washing a solid with hexane, drying in vac.; elem. anal.;	99.6%

: 35880-54-7, 61647-76-5, 184490-77-5, 65635-71-4
{ruthenium(0) dicarbonyltris(triphenylphosphine)}

: 463-58-1
carbon oxide sulfide

: 81011-77-0
Ru(CO)2(η2-CS2)(PPh3)2

Conditions

Conditions	Yield
With carbon disulfide In toluene byproducts: PPh3; a soln. of CS2 was added to a complex and a suspn. was stirred for 10 min, N2 atm.; dilution with hexane, filtration, washing a solid with hexane, drying in vac.;	99%

: 463-58-1
carbon oxide sulfide

: 172655-87-7
[Pd(C5H7N2)2(C5H8N2)2]

: 2Pd(C5H7N2)2(C5H8N2)2*COS = [Pd(C5H7N2)2(C5H8N2)2]2*COS

Conditions

Conditions	Yield
In further solvent(s) reaction with stirring in liquid COS at -78°C;	99%

: N-benzyl-4-methylhexa-2,3-dienamide

: 463-58-1
carbon oxide sulfide

: C15H17NO2S

Conditions

Conditions	Yield
With C15H18N2OS In acetonitrile at 60℃; for 12h; Autoclave;	99%
With C15H18N2OS In acetonitrile at 60℃; for 12h; Schlenk technique; Glovebox; Autoclave; regioselective reaction;	99 %Spectr.

: 463-58-1
carbon oxide sulfide

: 122-60-1
Phenyl glycidyl ether

: 2289-92-1
5-(phenoxymethyl)-1,3-oxathiolan-2-one

Conditions

Conditions	Yield
With 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine at 60℃; under 11251.1 Torr; for 12h; Autoclave; Inert atmosphere; Schlenk technique;	98%

: 463-58-1
carbon oxide sulfide

: 115-19-5
2-methyl-but-3-yn-2-ol

: 126441-98-3
5,5-Dimethyl-4-methylene-[1,3]oxathiolan-2-one

Conditions

Conditions	Yield
With C15H18N2OS In neat (no solvent) at 60℃; under 7500.75 Torr; for 1h; Autoclave;	98%
With C14H16N2OS at 60℃; for 1h; Autoclave;	92%

: 127-66-2
2-Phenyl-3-butyn-2-ol

: 463-58-1
carbon oxide sulfide

: 5-methyl-4-methylene-5-phenyl-1,3-oxathiolan-2-one

Conditions

Conditions	Yield
With C15H18N2OS In neat (no solvent) at 60℃; under 7500.75 Torr; for 1h; Autoclave;	98%
With C9H14N2OS at 50℃; for 2h; Autoclave;	93%

: 463-58-1
carbon oxide sulfide

: 2978-58-7
1,1-dimethylprop-3-ynylamine

: C6H9NOS

Conditions

Conditions	Yield
With C15H18N2OS In dimethyl sulfoxide at 25℃; under 760.051 Torr; chemoselective reaction;	98%
With C13H22N2OS In dimethyl sulfoxide at 25℃; for 24h; Schlenk technique;	90%

: 463-58-1
carbon oxide sulfide

: 827302-78-3
N-benzyl-4-phenyl-2,3-pentadienamide

: C19H17NO2S

Conditions

Conditions	Yield
With C15H18N2OS In acetonitrile at 60℃; for 12h; Autoclave;	98%
With C15H18N2OS In acetonitrile at 60℃; for 12h; Schlenk technique; Glovebox; Autoclave; regioselective reaction;	98 %Spectr.

: 463-58-1
carbon oxide sulfide

: 1606139-16-5
4-phenyl-N-(4-toluenesulfonylmethyl)penta-2,3-dienamide

: C20H19NO4S2

Conditions

Conditions	Yield
With C15H18N2OS In acetonitrile at 60℃; for 12h; Autoclave;	98%
With C15H18N2OS In acetonitrile at 60℃; for 12h; Schlenk technique; Glovebox; Autoclave; regioselective reaction;	98 %Spectr.

: 463-58-1
carbon oxide sulfide

: 1606139-32-5
4-phenyl-N-(4-toluenesulfonylmethyl)buta-2,3-dienamide

: C19H17NO4S2

Conditions

Conditions	Yield
With C15H18N2OS In acetonitrile at 60℃; for 12h; Autoclave;	98%
With C15H18N2OS In acetonitrile at 60℃; for 12h; Schlenk technique; Glovebox; Autoclave; regioselective reaction;	98 %Spectr.

: 463-58-1
carbon oxide sulfide

: N-cyclohexyl-4-methylpenta-2,3-dienamide

: C13H19NO2S

Conditions

Conditions	Yield
With C15H18N2OS In dimethyl sulfoxide at 100℃; for 12h; Autoclave;	98%
With C15H18N2OS In acetonitrile at 100℃; for 12h; Schlenk technique; Glovebox; Autoclave; regioselective reaction;	98 %Spectr.

: 463-58-1
carbon oxide sulfide

: 5876-69-7
2,4-diphenylbut-3-yn-2-ol

: C17H14O2S

Conditions

Conditions	Yield
With C15H18N2OS In neat (no solvent) at 60℃; under 7500.75 Torr; for 1h; Autoclave; diastereoselective reaction;	98%

: 463-58-1
carbon oxide sulfide

: 1504-58-1
3-Phenyl-2-propyn-1-ol

: 126441-96-1
4-[1-Phenyl-meth-(Z)-ylidene]-[1,3]oxathiolan-2-one

Conditions

Conditions	Yield
With C15H18N2OS In neat (no solvent) at 60℃; under 7500.75 Torr; for 1h; Autoclave; diastereoselective reaction;	98%

: 463-58-1
carbon oxide sulfide

: 1719-19-3
2-Methyl-4-phenyl-3-butyn-2-ol

: (Z)-4-benzylidene-5,5-dimethyl-1,3-oxathiolan-2-one

Conditions

Conditions	Yield
With C15H18N2OS In neat (no solvent) at 60℃; under 7500.75 Torr; for 1h; Reagent/catalyst; Temperature; Autoclave; diastereoselective reaction;	98%

: 463-58-1
carbon oxide sulfide

: 143767-97-9
2-methyl-4-phenylbut-3-yn-2-amine

: C12H13NOS

Conditions

Conditions	Yield
With C15H18N2OS In dimethyl sulfoxide at 25℃; under 760.051 Torr; chemoselective reaction;	98%

: 1197-51-9
N-propargylbenzylamine

: 463-58-1
carbon oxide sulfide

: C11H11NOS

Conditions

Conditions	Yield
With C15H18N2OS In dimethyl sulfoxide at 25℃; under 760.051 Torr; chemoselective reaction;	98%

: 463-58-1
carbon oxide sulfide

: 2450-71-7
Propargylamine

: C4H5NOS

Conditions

Conditions	Yield
With C15H18N2OS In dimethyl sulfoxide at 25℃; under 760.051 Torr; chemoselective reaction;	98%

: 463-58-1
carbon oxide sulfide

: C16H12N2O3

: C17H12N2O4S

Conditions

Conditions	Yield
With C15H18N2OS In dimethyl sulfoxide at 60℃; under 760.051 Torr; for 12h;	98%

: 463-58-1
carbon oxide sulfide

: 15448-47-2
(R)-propylene oxide

: (R)-propylene monothiocarbonate

Conditions

Conditions	Yield
Stage #1: (R)-propylene oxide With triethylamine; Quinine In ethanol at 16℃; for 0.25h; Stage #2: carbon oxide sulfide In ethanol at 20℃; for 20h; Reagent/catalyst; Temperature;	97.5%

: 503-30-0
trimethylene oxide

: 463-58-1
carbon oxide sulfide

: trimethylene monothiocarbonate

Conditions

Conditions	Yield
With bentonite-supported ionic liquid catalyst at 60℃; under 22502.3 Torr; for 6h; Temperature; Pressure; Autoclave;	97.4%

: 463-58-1
carbon oxide sulfide

: 137-07-5
2-amino-benzenethiol

: 934-34-9
2(3H)-Benzothiazolone

Conditions

Conditions	Yield
With triethylamine In tetrahydrofuran 1) 25-30 deg C, 24 h, 2) reflux, 2 h;	97%
With sodium hydroxide In N,N-dimethyl-formamide at 25℃; under 3750.38 Torr; for 1.5h;	87%

: 463-58-1
carbon oxide sulfide

: 1,3-bis(cyclohexyl)imidazolium tetrafluoroborate

: 1346137-08-3
1,3-dicyclohexylimidazolium-2-thiocarboxylate

Conditions

Conditions	Yield
Stage #1: 1,3-bis(cyclohexyl)imidazolium tetrafluoroborate With potassium hexamethylsilazane In tetrahydrofuran; toluene at 20℃; for 0.5h; Inert atmosphere; Stage #2: carbon oxide sulfide In tetrahydrofuran; toluene at 20℃; for 2h; Inert atmosphere;	97%

: 463-58-1
carbon oxide sulfide

: 1141-88-4
2-Aminophenyl disulfide

: 934-34-9
2(3H)-Benzothiazolone

Conditions

Conditions	Yield
With sodiumsulfide nonahydrate In N,N-dimethyl-formamide at 25℃; under 3750.38 Torr; for 1.5h; Reagent/catalyst; Solvent; Temperature; Autoclave;	97%
With sodium hydroxide In N,N-dimethyl-formamide at 25℃; under 3750.38 Torr; for 1.5h; Reagent/catalyst; Solvent; Pressure;	94%

: 463-58-1
carbon oxide sulfide

: 4-ethyl-N-(prop-2-yn-1-yl)hexa-2,3-dienamide

: C12H15NO2S

Conditions

Conditions	Yield
With C15H18N2OS In acetonitrile at 60℃; for 12h; Autoclave;	97%
With C15H18N2OS In acetonitrile at 60℃; for 12h; Schlenk technique; Glovebox; Autoclave; regioselective reaction;	97 %Spectr.

: 463-58-1
carbon oxide sulfide

: 1595281-23-4
1,3-bis(1,3-diisopropyl-4,5-dimethyl-1H-imidazol-2(3H)-ylidene)-2-isopropylguanidiniumtetrafluoroborate

: C27H47N7OS

Conditions

Conditions	Yield
Stage #1: 1,3-bis(1,3-diisopropyl-4,5-dimethyl-1H-imidazol-2(3H)-ylidene)-2-isopropylguanidiniumtetrafluoroborate With potassium hexamethylsilazane In tetrahydrofuran at 25℃; for 2h; Glovebox; Inert atmosphere; Stage #2: carbon oxide sulfide In hexane at 25℃; under 760.051 Torr; for 2h;	97%