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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

Chloral

Cas:75-87-6

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Trichloroacetaldehyde

Cas:75-87-6

Min.Order:1

Negotiable

Type:Other

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Chloral, anhydrous

Cas:75-87-6

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At presen

Chloral Hydrocarbons halides

Cas:75-87-6

Min.Order:1 Kilogram

FOB Price: $80.0 / 100.0

Type:Trading Company

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:75-87-6

Cas:75-87-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

Trichloroacetaldehyde

Cas:75-87-6

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Chloral

Cas:75-87-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

Trichloroethanal

Cas:75-87-6

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

moderate price & quick delivery Appearance:colourless oily liquid with a pungent odour Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Mai

Chloral

Cas:75-87-6

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Henan Tianfu Chemical Co., Ltd.

Chloral Chemical Properties Melting point -57.5°C Boiling point 94-98 °C density 1.51 g/mL

75-87-6 Chloral

Cas:75-87-6

Min.Order:1 Metric Ton

FOB Price: $20.0

Type:Lab/Research institutions

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

Trichloroethanal

Cas:75-87-6

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Xi'an yuanfar international trade company

best quality, best price and best service. Appearance:A colorless, oily liquid Application:Mainly used in the production of insecticides DDT, trichlorfon, dichlorvos and herbicide trichloroacetaldehyde urea, medicine for the production of chlora

low price\high quality97%\Chloral

Cas:75-87-6

Min.Order:0 Metric Ton

Negotiable

Type:Trading Company

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

Chloral

Cas:75-87-6

Min.Order:0

Negotiable

Type:Other

inquiry

GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier

Chloral

Cas:75-87-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates

trichloroacetaldehyde

Cas:75-87-6

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

DB BIOTECH CO., LTD

Q1: Are you a manufacturer Answer: Yes, we are factory founded on 2012.Q2: How to contact with us Click "contact supplier" And then send us message the product you interest in, you will get reply within 12 hours.Q3:Which kind of payment terms do you

Chloral

Cas:75-87-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

Chloral

Cas:75-87-6

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Enke Pharma-tech Co.,Ltd. (Cangzhou, China )

Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city?in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api,?intermediat

2,2,2-Trichloroacetaldehyde

Cas:75-87-6

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard

factory directly supply CAS 75-87-6 with competitive price

Cas:75-87-6

Min.Order:1 Kilogram

FOB Price: $112.0

Type:Trading Company

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

Acetaldehyde,2,2,2-trichloro-

Cas:75-87-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hubei Langyou International Trading Co., Ltd

75-87-6 Chloral Application:75-87-6 Chloral

75-87-6 Chloral

Cas:75-87-6

Min.Order:0

Negotiable

Type:Other

inquiry

Wuhan ZeShanCheng Biomedical Technology Co., Ltd.

1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highl

trichloroacetaldehyde

Cas:75-87-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hangzhou ZeErRui Chemical Co., Ltd.

Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home an

Chloral manufacture

Cas:75-87-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

SAGECHEM LIMITED

75-87-6 Application:intermediate

2,2,2-trichloroacetaldehyde

Cas:75-87-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hunan Longxianng Runhui Trading Co.,Ltd

75-87-6 ChloralAppearance:powder Storage:room tempurature Package:As required Application:medical Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport to airport) or by sea LCL/FCL for large amount.

75-87-6 Chloral

Cas:75-87-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hunan Russell Chemicals Technology Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

Trichloroethanal 75-87-6

Cas:75-87-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

HENAN SUNLAKE ENTERPRISE CORPORATION

Chloral Basic information

75-87-6 C2HCl3O Chloral

Cas:75-87-6

Min.Order:5 Gram

Negotiable

Type:Trading Company

inquiry

Shanlong Biotechnology (hebei) Co., Ltd.

Why Choose Us: 1.Own chemical factory 2.Abundant professional production experience 3.Sample is free of charge and in stock with fast delivery 4.Price,quality&service,we care that all your cares 5.Prompt reply keep in touch to sa

Chloral Grasex cas 75-87-6

Cas:75-87-6

Min.Order:1 Kilogram

FOB Price: $44.0 / 52.0

Type:Trading Company

inquiry

Shaanxi Mingqi Chemical Co., Ltd

Known for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers. Our advantages:1, High quality with competitive price:1) Standard:BP/USP/EP/Enterprise standard2) All Purity≥99%3) We are manufacturer

trichloroacetaldehyde factory

Cas:75-87-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Xi'an Harmonious Natural Bio-Technology Co., Ltd.

Before-Sale Service:---Any inquiries will be replied within 12 hours.---Golden Manufactory under?ISO/GMP?with?large stock.---Dedication to quality,We?have?strict?quality?control?system.?---OEM/ODM Available.---Sample is available for your evaluation

Gmp factory supply trichloroacetaldehyde in high quality

Cas:75-87-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

trichloroethylene epoxide
16967-79-6

trichloroethylene epoxide

chloral
75-87-6

chloral

Conditions
ConditionsYield
With sulfuric acid at 100℃; for 2h;100%
iron(III) chloride at 60℃; for 1h; sealed tube; Yield given;
chloral hydrate
302-17-0

chloral hydrate

chloral
75-87-6

chloral

Conditions
ConditionsYield
With phosphorus pentoxide; sulfuric acid99%
With diethyl ether; water; chlorine at 80℃;
With sulfuric acid
Trichloroacetyl chloride
76-02-8

Trichloroacetyl chloride

chloral
75-87-6

chloral

Conditions
ConditionsYield
With sodium tris(tert-butoxo)aluminium hydride In tetrahydrofuran; diethylene glycol dimethyl ether at -78℃; for 1h;91%
With ammonium hydroxide; formic acid In diethyl ether; chloroform for 0.75h; Ambient temperature;76%
Stage #1: trifluoroacetyl chloride With aluminium hydride In tetrahydrofuran at 20℃; for 1h; Metallation;
Stage #2: With pyridinium chlorochromate In tetrahydrofuran; dichloromethane at 20℃; for 6h; Oxidation;
95 % Chromat.
1,2,2,2-Tetrachloroethyl tert-Butyl Carbonate
98015-52-2

1,2,2,2-Tetrachloroethyl tert-Butyl Carbonate

L-proline
147-85-3

L-proline

A

1-(tert-butoxycarbonyl)-L-proline
15761-39-4

1-(tert-butoxycarbonyl)-L-proline

B

chloral
75-87-6

chloral

Conditions
ConditionsYield
With triethylamine In 1,4-dioxane; water at 20℃; for 5h; Product distribution; var. amines, other 1-chloroalkyl carbonate, other basic reagent and time;A 91%
B n/a
paracetaldehyde
123-63-7

paracetaldehyde

A

2-chloroethanal
107-20-0

2-chloroethanal

B

2,2-dichloroacetaldehyde
79-02-7

2,2-dichloroacetaldehyde

C

chloral
75-87-6

chloral

Conditions
ConditionsYield
With antimony(III) chloride; chlorine at 10 - 80℃; for 18h; Product distribution; var. catalysts, var. time;A 0.7%
B 71.3%
C 2.6%
5-(p-methoxyphenyl)-2-trichloromethyl-1,3,4-oxathiazole
73501-02-7

5-(p-methoxyphenyl)-2-trichloromethyl-1,3,4-oxathiazole

propynoic acid ethyl ester
623-47-2

propynoic acid ethyl ester

A

ethyl 3-(p-methoxyphenyl)isothiazole-4-carboxylate
76162-57-7

ethyl 3-(p-methoxyphenyl)isothiazole-4-carboxylate

B

ethyl 3-(p-methoxyphenyl)isothiazole-5-carboxylate
76162-58-8

ethyl 3-(p-methoxyphenyl)isothiazole-5-carboxylate

C

chloral
75-87-6

chloral

D

4-methoxybenzonitrile
874-90-8

4-methoxybenzonitrile

E

S

S

Conditions
ConditionsYield
In 1,3,5-trimethyl-benzene at 161℃; for 19h;A 17%
B 13%
C n/a
D 68%
E n/a
Trichloroethylene
79-01-6

Trichloroethylene

chloral
75-87-6

chloral

Conditions
ConditionsYield
With tetrachloromethane; chlorine monoxide at -20℃;
With hypochloric acid
Trichloroethylene
79-01-6

Trichloroethylene

A

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

B

chloral
75-87-6

chloral

Conditions
ConditionsYield
With oxygen Umsetzung der bis 107grad siedenden Anteile des Reaktionsprodukts mit Metallchloriden wie SbCl5,FeCl3 oder AlCl3;
1,1,1-trichloro-2,2-diethoxy-ethane
599-97-3

1,1,1-trichloro-2,2-diethoxy-ethane

chloral
75-87-6

chloral

Conditions
ConditionsYield
With sulfuric acid at 150℃;
at 200℃;
(2,2,2-trichloro-1-hydroxyethyl)urea
2000-40-0

(2,2,2-trichloro-1-hydroxyethyl)urea

A

chloral
75-87-6

chloral

B

isocyanuric acid
108-80-5

isocyanuric acid

Conditions
ConditionsYield
at 150℃;
2,2-diacetoxy-1,1,1-trichloro-ethane
24298-56-4

2,2-diacetoxy-1,1,1-trichloro-ethane

A

acetic anhydride
108-24-7

acetic anhydride

B

chloral
75-87-6

chloral

Conditions
ConditionsYield
at 210 - 290℃; Kinetics;
2-(2,2,2-trichloro-1-hydroxy-ethyl)-acetoacetic acid ethyl ester
75456-97-2

2-(2,2,2-trichloro-1-hydroxy-ethyl)-acetoacetic acid ethyl ester

A

ethyl acetoacetate
141-97-9

ethyl acetoacetate

B

chloral
75-87-6

chloral

Conditions
ConditionsYield
Erhitzen;
N,N'-bis-(2,2,2-trichloro-1-hydroxy-ethyl)-oxalamide
75457-07-7

N,N'-bis-(2,2,2-trichloro-1-hydroxy-ethyl)-oxalamide

A

Oxalamide
471-46-5

Oxalamide

B

chloral
75-87-6

chloral

N,N'-(1,3-bis-trichloromethyl-2-oxa-propanediyl)-bis-carbamic acid dimethyl ester
198283-38-4

N,N'-(1,3-bis-trichloromethyl-2-oxa-propanediyl)-bis-carbamic acid dimethyl ester

chloral
75-87-6

chloral

Conditions
ConditionsYield
at 200℃;
benzyl 2,2,2-trichloroacetate
26827-38-3

benzyl 2,2,2-trichloroacetate

A

benzaldehyde
100-52-7

benzaldehyde

B

chloral
75-87-6

chloral

Conditions
ConditionsYield
at 220℃;
3-acridin-9-yl-1,1,1-trichloro-propan-2-ol
91025-27-3

3-acridin-9-yl-1,1,1-trichloro-propan-2-ol

A

9-methyl-acridine
611-64-3

9-methyl-acridine

B

chloral
75-87-6

chloral

Conditions
ConditionsYield
beim Erhitzen;
trichloro-acetic acid phenethyl ester
71965-07-6

trichloro-acetic acid phenethyl ester

A

phenylacetaldehyde
122-78-1

phenylacetaldehyde

B

chloral
75-87-6

chloral

Conditions
ConditionsYield
at 240℃;
N-phenyl-N'-(2,2,2-trichloro-1-hydroxy-ethyl)-oxalamide
859068-72-7

N-phenyl-N'-(2,2,2-trichloro-1-hydroxy-ethyl)-oxalamide

A

oxanilic acid
500-72-1

oxanilic acid

B

chloral
75-87-6

chloral

chloral allyl hemiacetal
1873-15-0

chloral allyl hemiacetal

benzyl chloride
100-44-7

benzyl chloride

A

vinyl benzoate
583-04-0

vinyl benzoate

B

chloral
75-87-6

chloral

ethanol
64-17-5

ethanol

1-[(E)-benzylideneamino]-2,2,2-trichloroethanol
43180-42-3

1-[(E)-benzylideneamino]-2,2,2-trichloroethanol

phenyl isothiocyanate
103-72-0

phenyl isothiocyanate

A

benzaldehyde
100-52-7

benzaldehyde

B

chloral
75-87-6

chloral

C

monophenylthiourea
103-85-5

monophenylthiourea

acetaldehyde
75-07-0

acetaldehyde

chloral
75-87-6

chloral

Conditions
ConditionsYield
With water Chlorieren;
With hydrogenchloride; chlorine
With antimony(III) chloride; chlorine
With chlorine at 250℃; under 760.051 Torr; Industry scale;
2-pyrrolidinon
616-45-5

2-pyrrolidinon

chloral
75-87-6

chloral

2,2,2-trichloro-1-(2-oxo-1-aza-1-cyclopentyl)ethanol
7042-60-6

2,2,2-trichloro-1-(2-oxo-1-aza-1-cyclopentyl)ethanol

Conditions
ConditionsYield
In benzene for 2h; Heating;100%
piperidin-2-one
675-20-7

piperidin-2-one

chloral
75-87-6

chloral

1-(2,2,2-Trichloro-1-hydroxy-ethyl)-piperidin-2-one
65101-81-7

1-(2,2,2-Trichloro-1-hydroxy-ethyl)-piperidin-2-one

Conditions
ConditionsYield
In benzene for 2h; Heating;100%
L-Tartaric acid
87-69-4

L-Tartaric acid

chloral
75-87-6

chloral

Conditions
ConditionsYield
With sulfuric acid for 0.5h; Ambient temperature;100%
2,2,2-tribromo-1,3,2-benzodioxaphosphole
3712-44-5

2,2,2-tribromo-1,3,2-benzodioxaphosphole

chloral
75-87-6

chloral

5-bis(1-bromo-2',2',2'-trichloroethoxy)-2,3-benzo-1,4,6-trioxa-7-bromo-8,8,8-trichloro-5-phospha<4>octane
127955-64-0, 135819-35-1

5-bis(1-bromo-2',2',2'-trichloroethoxy)-2,3-benzo-1,4,6-trioxa-7-bromo-8,8,8-trichloro-5-phospha<4>octane

Conditions
ConditionsYield
In dichloromethane at -40 - 25℃; for 4h;100%
With bromine In dichloromethane - 60 to 20 deg C;
2,2,3,3-Tetrafluoropropyl difluorophosphite
131570-94-0

2,2,3,3-Tetrafluoropropyl difluorophosphite

chloral
75-87-6

chloral

bis(1-bromo-2,2,2-trichloroethoxy)difluoro(2,2,3,3-tetrafluoropropoxy)phosphorane
131570-92-8, 135819-38-4, 135819-39-5

bis(1-bromo-2,2,2-trichloroethoxy)difluoro(2,2,3,3-tetrafluoropropoxy)phosphorane

Conditions
ConditionsYield
With bromine In dichloromethane 1.) CH2Cl2, -60 deg C, 2.a) to 15 deg C, 6 h, b) 10-15 deg C;100%
chloral
75-87-6

chloral

2-(2,2,3,3-Tetrafluoro-propoxy)-[1,3,2]dioxaphosphinane
115044-89-8

2-(2,2,3,3-Tetrafluoro-propoxy)-[1,3,2]dioxaphosphinane

1,1,3-trihydroperfluoropropyl-2,2-dichlorovinyl-3-chloropropyl phosphate
115045-01-7

1,1,3-trihydroperfluoropropyl-2,2-dichlorovinyl-3-chloropropyl phosphate

Conditions
ConditionsYield
In dichloromethane at 50℃; for 0.5h;100%
chloral
75-87-6

chloral

N-hydroxybenzenecarboximidamide
613-92-3

N-hydroxybenzenecarboximidamide

O-(2,2,2-Trichloro-1-hydroxyethyl)benzamidoxime
111321-11-0

O-(2,2,2-Trichloro-1-hydroxyethyl)benzamidoxime

Conditions
ConditionsYield
In diethyl ether for 4h; Heating;100%
chloral
75-87-6

chloral

tris(2,2,2-trifluoroethoxy)dicyanophosphorane

tris(2,2,2-trifluoroethoxy)dicyanophosphorane

tris(2,2,2-trofluoroethoxy)bis(1-cyano-2,2,2-trichloroethoxy)phosphorane

tris(2,2,2-trofluoroethoxy)bis(1-cyano-2,2,2-trichloroethoxy)phosphorane

Conditions
ConditionsYield
In dichloromethane at 0 - 10℃;100%
chloral
75-87-6

chloral

dibenzylamine
103-49-1

dibenzylamine

N,N-dibenzylformamide
5464-77-7

N,N-dibenzylformamide

Conditions
ConditionsYield
In chloroform at 10 - 15℃; for 12h;100%
tributyltin methoxide
1067-52-3

tributyltin methoxide

chloral
75-87-6

chloral

1.1.1-Trichlor-2-methoxy-2--ethan
14630-16-1

1.1.1-Trichlor-2-methoxy-2--ethan

Conditions
ConditionsYield
In neat (no solvent) addn. of tributyltin alkoxide to aldehyde (1:1 mole ratio) at 33°C; proved by NMR;100%
In neat (no solvent) addn. of tributyltin alkoxide to aldehyde (1:1 mole ratio) at 33°C; proved by NMR;100%
1:1.1;85-100
tributyltin ethoxide
682-00-8

tributyltin ethoxide

chloral
75-87-6

chloral

2.2.2-Trichlor-1-ethoxy-1-(tributyl-stannoxy)-ethan
21001-96-7

2.2.2-Trichlor-1-ethoxy-1-(tributyl-stannoxy)-ethan

Conditions
ConditionsYield
In tetrachloromethane addn. of tributyltin alkoxide to aldehyde (1:1 mole ratio) at 33°C; proved by NMR;100%
In tetrachloromethane addn. of tributyltin alkoxide to aldehyde (1:1 mole ratio) at 33°C; proved by NMR;100%
tri-n-butyl(cyanomethyl)stannane
17729-59-8

tri-n-butyl(cyanomethyl)stannane

chloral
75-87-6

chloral

<1-Trichlormethyl-2-cyanethoxy>-tributylzinn
17981-10-1

<1-Trichlormethyl-2-cyanethoxy>-tributylzinn

Conditions
ConditionsYield
at room temp. for 16 h;100%
at room temp. for 16 h;100%
1,1-diphenyl-N-(tributylstannyl)methanimine
34982-42-8

1,1-diphenyl-N-(tributylstannyl)methanimine

chloral
75-87-6

chloral

(C4H9)3SnOCH(CCl3)NC(C6H5)2
34982-49-5

(C4H9)3SnOCH(CCl3)NC(C6H5)2

Conditions
ConditionsYield
100%
100%
(N-tributylstannyl)benzenesulfonamide

(N-tributylstannyl)benzenesulfonamide

chloral
75-87-6

chloral

N-(1-Tributylstannyloxy-2-trichlor-ethyl)-benzolsulfonamid

N-(1-Tributylstannyloxy-2-trichlor-ethyl)-benzolsulfonamid

Conditions
ConditionsYield
In neat (no solvent) 1:1.2 mole ratio of (C4H9)3Sn-amine and CCl3CHO at room temp or 55°C; proved by NMR;100%
In tetrachloromethane 1:1.2 mole ratio of (C4H9)3Sn-amine and CCl3CHO at room temp or 55°C; proved by NMR;100%
In tetrachloromethane 1:1.2 mole ratio of (C4H9)3Sn-amine and CCl3CHO at room temp or 55°C; proved by NMR;100%
In neat (no solvent) 1:1.2 mole ratio of (C4H9)3Sn-amine and CCl3CHO at room temp or 55°C; proved by NMR;100%
2-(3,4-dichlorophenyl)-4,4-dimethylsemicarbazide hydrochloride

2-(3,4-dichlorophenyl)-4,4-dimethylsemicarbazide hydrochloride

chloral hydrate
302-17-0

chloral hydrate

A

2-(3,4-dichlorophenyl)-4,4-dimethylsemicarbazone

2-(3,4-dichlorophenyl)-4,4-dimethylsemicarbazone

B

chloral
75-87-6

chloral

Conditions
ConditionsYield
In waterA 66%
B n/a
5-(p-methoxyphenyl)-2-trichloromethyl-1,3,4-oxathiazole
73501-02-7

5-(p-methoxyphenyl)-2-trichloromethyl-1,3,4-oxathiazole

dimethyl acetylenedicarboxylate
762-42-5

dimethyl acetylenedicarboxylate

A

chloral
75-87-6

chloral

B

4-methoxybenzonitrile
874-90-8

4-methoxybenzonitrile

C

dimethyl 3-(p-methoxyphenyl)isothiazole-4,5-dicarboxylate
59291-73-5

dimethyl 3-(p-methoxyphenyl)isothiazole-4,5-dicarboxylate

D

S

S

Conditions
ConditionsYield
In 1,3,5-trimethyl-benzene at 161℃; for 18h;A n/a
B 33%
C 60%
D n/a
thirane
420-12-2

thirane

2,2-dimethyl-4-trichloromethyl-1,3,2-dioxagermenate
96287-65-9

2,2-dimethyl-4-trichloromethyl-1,3,2-dioxagermenate

A

2,2-Dimethyl-2-germa-1-oxa-3-thia-cyclopentan
86553-73-3

2,2-Dimethyl-2-germa-1-oxa-3-thia-cyclopentan

B

chloral
75-87-6

chloral

Conditions
ConditionsYield
at 100°C;;A 45%
B n/a
at 20°C;;A <1
B n/a
oxirane
75-21-8

oxirane

2,2-dimethyl-4-trichloromethyl-1,3,2-dioxagermenate
96287-65-9

2,2-dimethyl-4-trichloromethyl-1,3,2-dioxagermenate

A

dimethyl-2,2 germa-2 dioxolane-1,3
5865-67-8

dimethyl-2,2 germa-2 dioxolane-1,3

B

chloral
75-87-6

chloral

Conditions
ConditionsYield
at 100°C;;A 15%
B n/a
at 20°C;;A <1
B n/a
tetrachloromethane
56-23-5

tetrachloromethane

formaldehyd
50-00-0

formaldehyd

chloral
75-87-6

chloral

Conditions
ConditionsYield
With sulfuryl dichloride at 300℃;
With sulfuryl dichloride at 300℃;
chloral ethyl hemiacetal
515-83-3

chloral ethyl hemiacetal

A

ethanol
64-17-5

ethanol

B

chloral
75-87-6

chloral

Conditions
ConditionsYield
at 157℃;
at 198℃;
ethanol
64-17-5

ethanol

(4-acetylamino-phenoxy)-acetic acid-(2,2,2-trichloro-1-hydroxy-ethylamide)

(4-acetylamino-phenoxy)-acetic acid-(2,2,2-trichloro-1-hydroxy-ethylamide)

A

(4-acetylamino-phenoxy)-acetic acid amide
6033-85-8

(4-acetylamino-phenoxy)-acetic acid amide

B

chloral
75-87-6

chloral

ethanol
64-17-5

ethanol

chloral
75-87-6

chloral

Conditions
ConditionsYield
Chlorierung;
With water; chlorine Bildung des krystallisierten Chloralhydrats;
Chlorieren;
ethyl-(1,2,2,2-tetrachloro-ethyl)-ether
36458-82-9

ethyl-(1,2,2,2-tetrachloro-ethyl)-ether

chloral
75-87-6

chloral

Conditions
ConditionsYield
With sulfuric acid durch Destillieren;
With water at 100℃;
chloral
75-87-6

chloral

acetyl chloride
75-36-5

acetyl chloride

1-azido-2,2,2-trichloroethyl acetate

1-azido-2,2,2-trichloroethyl acetate

Conditions
ConditionsYield
With hydrogen azide In chloroform at -50 - 20℃; for 48h;100%
chloral
75-87-6

chloral

1,3-Dibutyl-2-ethoxy-4,5-dimethyl-2,3-dihydro-1H-[1,3,2]diazaphosphole
141968-97-0

1,3-Dibutyl-2-ethoxy-4,5-dimethyl-2,3-dihydro-1H-[1,3,2]diazaphosphole

1,3-dibutyl-2-[(2,2-dichlorovinyl)oxy]-4,5-dimethyl-Δ4-1,3,2λ5-diazaphospholine 2-oxide

1,3-dibutyl-2-[(2,2-dichlorovinyl)oxy]-4,5-dimethyl-Δ4-1,3,2λ5-diazaphospholine 2-oxide

Conditions
ConditionsYield
In diethyl ether for 24h;99.6%
p-toluidine
106-49-0

p-toluidine

chloral
75-87-6

chloral

2-hydroxyimino-N-p-tolyl-acetamide
1132-40-7

2-hydroxyimino-N-p-tolyl-acetamide

Conditions
ConditionsYield
With hydroxyammonium sulfate; sodium sulfate In water at 60 - 80℃; for 2h;99%
With hydroxylamine hydrochloride; sodium sulfate In water for 0.05h; Condensation; substitution; microwave irradiation;82%
With hydrogenchloride; hydroxylamine hydrochloride; sodium sulfate In water at 90℃; for 0.166667h;27%
4-chloro-aniline
106-47-8

4-chloro-aniline

chloral
75-87-6

chloral

N-(4-chlorophenyl)-2-(hydroxyimino)ethanamide
65798-06-3, 17122-56-4

N-(4-chlorophenyl)-2-(hydroxyimino)ethanamide

Conditions
ConditionsYield
With hydroxyammonium sulfate; sodium sulfate In water at 70 - 80℃; for 3h;99%
With hydroxylamine
With hydrogenchloride; hydroxylamine hydrochloride; sodium sulfate In water at 85℃; for 2.5h;
With hydrogenchloride; hydroxylamine hydrochloride; sodium sulfate In water for 1h; Reflux;
With hydroxylamine hydrochloride; sodium sulfate In water
phenoxymethylpenicillin sulfoxide
4888-90-8

phenoxymethylpenicillin sulfoxide

tert-butylisonitrile
119072-55-8, 7188-38-7

tert-butylisonitrile

chloral
75-87-6

chloral

Penicillin-V-sulfoxid-1'-tert-butylaminocarbonyl-2',2',2'-trichlorethylester
65538-81-0

Penicillin-V-sulfoxid-1'-tert-butylaminocarbonyl-2',2',2'-trichlorethylester

Conditions
ConditionsYield
In tetrahydrofuran; dichloromethane Ambient temperature;99%
1,2,3,6-tertahydrophthalimide
85-40-5

1,2,3,6-tertahydrophthalimide

chloral
75-87-6

chloral

N-(1-Hydroxy-2,2,2-trichloroethyl)-cis-4-cyclohexene-1,2-dicarboximide

N-(1-Hydroxy-2,2,2-trichloroethyl)-cis-4-cyclohexene-1,2-dicarboximide

Conditions
ConditionsYield
In ethanol for 2.5h; Addition; Heating;99%
chloral
75-87-6

chloral

(5E)-2-methyl-6-phenylhex-5-en-3-yn-2-ol
82565-66-0

(5E)-2-methyl-6-phenylhex-5-en-3-yn-2-ol

(E)-1,1,1-Trichloro-6-phenyl-hex-5-en-3-yn-2-ol

(E)-1,1,1-Trichloro-6-phenyl-hex-5-en-3-yn-2-ol

Conditions
ConditionsYield
Stage #1: (5E)-2-methyl-6-phenylhex-5-en-3-yn-2-ol With (o,o'-biphenylenedioxy)methylaluminium In hexane; dichloromethane at 20℃; for 0.5h;
Stage #2: chloral In hexane; dichloromethane at 20℃; for 5h; Meerwein-Ponndorf-Verley alkynylation;
99%
5-bromo-2-pyridinecarboxamide
90145-48-5

5-bromo-2-pyridinecarboxamide

chloral
75-87-6

chloral

5-bromo-N-(2,2,2-trichloro-1-hydroxyethyl)picolinamide
1265593-67-6

5-bromo-N-(2,2,2-trichloro-1-hydroxyethyl)picolinamide

Conditions
ConditionsYield
In 1,4-dioxane at 100℃;99%
In 1,4-dioxane at 100℃;
4-acryloyloxy-2,2,6,6-tetramethylpiperidine-1-oxyl
21270-85-9

4-acryloyloxy-2,2,6,6-tetramethylpiperidine-1-oxyl

chloral
75-87-6

chloral

4-(2-((trichloromethyl)hydroxymethyl)acryloyloxy)-2,2,6,6-tetramethylpiperidine-1-oxyl
1414365-14-2

4-(2-((trichloromethyl)hydroxymethyl)acryloyloxy)-2,2,6,6-tetramethylpiperidine-1-oxyl

Conditions
ConditionsYield
With Quinuclidine; methanol In tetrahydrofuran at 20℃; for 26h; Morita-Baylis-Hillman Alkylation; Inert atmosphere;99%
methylene bis phosphonate de diethyle
63366-56-3

methylene bis phosphonate de diethyle

chloral
75-87-6

chloral

methylenebis(O-ethyl-O-β,β-dichlorovinylphosphonate)
123146-93-0

methylenebis(O-ethyl-O-β,β-dichlorovinylphosphonate)

Conditions
ConditionsYield
In diethyl ether 1) -70 deg C, 2) RT;98%
chloral
75-87-6

chloral

1-methyl-6-phenyl-1H-imidazo[1,2-a]imidazole
37162-79-1

1-methyl-6-phenyl-1H-imidazo[1,2-a]imidazole

2,2,2-Trichloro-1-(7-methyl-2-phenyl-7H-imidazo[1,2-a]imidazol-3-yl)-ethanol
74944-14-2

2,2,2-Trichloro-1-(7-methyl-2-phenyl-7H-imidazo[1,2-a]imidazol-3-yl)-ethanol

Conditions
ConditionsYield
In benzene for 15h; Ambient temperature;98%
chloral
75-87-6

chloral

3-(Methyl-propoxy-phosphinoyloxy)-thiopropionimidic acid propyl ester

3-(Methyl-propoxy-phosphinoyloxy)-thiopropionimidic acid propyl ester

O-propyl-O-<3(N-1-hydroxy-2,2,2-trichloroethyl)imino-3-propylthio>propylmethylphosphonate

O-propyl-O-<3(N-1-hydroxy-2,2,2-trichloroethyl)imino-3-propylthio>propylmethylphosphonate

Conditions
ConditionsYield
In 1,4-dioxane at 15 - 25℃; for 2h;98%
chloral
75-87-6

chloral

3-bromo-1-adamantyl-2'-adamantylphosphine oxide
118154-04-4

3-bromo-1-adamantyl-2'-adamantylphosphine oxide

3-bromo-1-adamantyl-2'-adamantyl-2",2",2"-trichloro-1"-hydroxyethylphosphine oxide

3-bromo-1-adamantyl-2'-adamantyl-2",2",2"-trichloro-1"-hydroxyethylphosphine oxide

Conditions
ConditionsYield
at 80℃; for 2h;98%
chloral
75-87-6

chloral

perfluorobutanoyl diisopropyl phosphite
157402-29-4

perfluorobutanoyl diisopropyl phosphite

diisopropyl 1-perfluorobutanoyloxy-2,2,2-trichloroethylphosphonate

diisopropyl 1-perfluorobutanoyloxy-2,2,2-trichloroethylphosphonate

Conditions
ConditionsYield
at 20℃;98%
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