As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiry2-(4-Fluorobenzoyl)benzoic acidAppearance:detailed see specifications Storage:Keep away of light, cool place Package:25kg/drum;200kg/drum Application:It is an important raw material and intermediate used in Organic Synthesis, Pharmaceuticals, Agroche
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inquiry2-(4-FLUOROBENZOYL)BENZOIC ACID Application:2-(4-FLUOROBENZOYL)BENZOIC ACID
We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:Powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as primary and sec
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Cerametek Materials (CMT) is your industrial and R&D supplier: 1. Semiconductor materials: Compounds of II, III, IV, V, VI groups such as Metal Sulfides, Selenides, Tellurides, Arsenide, Antimonide, Phosphide... 2. Advanced ceramic and crys
Conditions | Yield |
---|---|
With aluminum (III) chloride at 20℃; Friedel-Crafts Acylation; Heating; | 97% |
With sodium carbonate In dichloromethane at 20℃; for 0.2h; Reagent/catalyst; Solvent; Temperature; Friedel-Crafts Acylation; | 94.6% |
With aluminum (III) chloride at 75℃; for 3h; Friedel Crafts Acylation; | 85% |
phthalic anhydride
4-flourophenylmagnesium bromide
2-(4-fluorobenzoyl)benzoic acid
Conditions | Yield |
---|---|
Stage #1: phthalic anhydride; 4-flourophenylmagnesium bromide In tetrahydrofuran at 30℃; for 1h; Stage #2: With hydrogenchloride In water; toluene at 35℃; for 1h; | 69% |
2-(4-fluorophenyl)-2-oxoacetic acid
benzoic acid
2-(4-fluorobenzoyl)benzoic acid
Conditions | Yield |
---|---|
With palladium(II) trifluoroacetate; silver carbonate In 1,2-dimethoxyethane at 150℃; for 24h; Sealed tube; chemoselective reaction; | 62% |
Conditions | Yield |
---|---|
With hydrogenchloride; aluminium chloride In fluorobenzene; hexane; benzene | 33.5 parts (80.7%) |
With hydrogenchloride; aluminium chloride In fluorobenzene; hexane; benzene | 33.5 parts (80.7%) |
2-(4-fluorobenzoyl)benzoic acid
3-chloro-3-(para-fluorophenyl)-1-(3H)-isobenzofuranone
Conditions | Yield |
---|---|
With thionyl chloride; N,N-dimethyl-formamide In tetrahydrofuran at 20℃; for 4h; Inert atmosphere; | 100% |
With thionyl chloride for 5h; Heating; | |
With thionyl chloride for 2h; Reflux; | |
With thionyl chloride; N,N-dimethyl-formamide In tetrahydrofuran at 20℃; for 4h; Inert atmosphere; |
Conditions | Yield |
---|---|
With sulfuric acid at 85 - 95℃; for 2h; | 88.1% |
Conditions | Yield |
---|---|
With hydrazine hydrate In ethanol for 5h; Heating; | 86% |
2-(4-fluorobenzoyl)benzoic acid
N-[(diphenylphosphinoyl)methyl]-N-methylamine
N-diphenylphosphinoylmethyl-N-methyl-2-(4-fluorobenzoyl)benzamide
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane for 2h; Ambient temperature; | 85% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; sodium acetate; tetra-(n-butyl)ammonium iodide In tetrahydrofuran; water at 80℃; for 12h; | 85% |
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In methanol at 70℃; under 15200 Torr; for 12h; | 83% |
With hydrogen; palladium on activated charcoal In methanol at 70℃; under 15200 Torr; for 12h; | 83% |
With hydrogen; palladium 10% on activated carbon In propylene glycol monomethyl ether at 50℃; for 18h; | 83% |
With sodium hydroxide; coppered zinc | |
With ammonium hydroxide; zinc |
2-(4-fluorobenzoyl)benzoic acid
recorcinol
3-(2,4-dihydroxyphenyl)-3-(4-fluorophenyl)phthalide
Conditions | Yield |
---|---|
With sulfuric acid at 110 - 120℃; for 1h; | 78.9% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl acetamide; chlorobenzene at 185℃; for 17h; Inert atmosphere; | 77% |
2-(4-fluorobenzoyl)benzoic acid
hydroquinone
3-(2,5-dihydroxyphenyl)-3-(4-fluorophenyl)phthalide
Conditions | Yield |
---|---|
With sulfuric acid at 135 - 145℃; for 2h; | 73.3% |
2-(4-fluorobenzoyl)benzoic acid
2-hydrazinyl acetic acid ethyl ester hydrochloride
[4-(4-Fluoro-phenyl)-1-oxo-1H-phthalazin-2-yl]-acetic acid ethyl ester
Conditions | Yield |
---|---|
With TEA In ethanol Heating; | 72% |
Conditions | Yield |
---|---|
With dipotassium peroxodisulfate; silver(I) acetate In [D3]acetonitrile at 130℃; for 1h; Pschorr reaction; Microwave irradiation; | 70% |
Multi-step reaction with 4 steps 1: H2SO4 2: NH3 3: Br2, aq. KOH 4: NaNO2, aq. H2SO4 View Scheme |
2-hydrazinyl-3-(2-(trifluoromethyl)phenyl)-1,8-naphthyridine
2-(4-fluorobenzoyl)benzoic acid
Conditions | Yield |
---|---|
With sulfuric acid In ethanol for 0.25h; Green chemistry; | 70% |
2-(4-fluorobenzoyl)benzoic acid
phenol
3-(4-hydroxyphenyl)-3-(4-fluorophenyl)phthalide
Conditions | Yield |
---|---|
With sulfuric acid at 80 - 90℃; for 5h; | 69.2% |
2-(4-fluorobenzoyl)benzoic acid
L-tryptophanol
Conditions | Yield |
---|---|
In toluene for 23h; Reflux; Inert atmosphere; Dean-Stark; | 65.9% |
2-(4-fluorobenzoyl)benzoic acid
phenylhydrazine
1-oxo-2-phenyl-4-p-fluorophenyl-1,2-dihydrophthalazine
Conditions | Yield |
---|---|
With acetic acid at 100℃; for 2h; | 60% |
In acetic acid for 2h; on a boiling water bath; Yield given; |
3,5-dihydroxyphenol
2-(4-fluorobenzoyl)benzoic acid
3-(2,4,6-trihydroxyphenyl)-3-(4-fluorophenyl)phthalide
Conditions | Yield |
---|---|
With sulfuric acid at 170 - 180℃; for 1h; | 59.3% |
Conditions | Yield |
---|---|
In ethanol Reflux; | 58.7% |
Conditions | Yield |
---|---|
With sulfuric acid at 115 - 125℃; for 0.5h; | 58.5% |
2-(4-fluorobenzoyl)benzoic acid
2-(3,5-dinitro-4-fluorobenzoyl)benzoic acid
Conditions | Yield |
---|---|
With sulfuric acid; nitric acid at 40 - 50℃; for 1h; | 57.5% |
Conditions | Yield |
---|---|
Stage #1: Methyltriphenylphosphonium bromide With sodium t-butanolate In tetrahydrofuran at 0℃; for 0.5h; Inert atmosphere; Stage #2: 2-(4-fluorobenzoyl)benzoic acid In tetrahydrofuran at 0 - 20℃; for 41h; Inert atmosphere; | 57% |
Stage #1: Methyltriphenylphosphonium bromide With potassium tert-butylate In tetrahydrofuran at 0℃; for 0.5h; Wittig Olefination; Inert atmosphere; Stage #2: 2-(4-fluorobenzoyl)benzoic acid In tetrahydrofuran at 0℃; Wittig Olefination; Inert atmosphere; | 17% |
2-(4-fluorobenzoyl)benzoic acid
(2R)-2-amino-3-(1H-indol-3-yl)propan-1-ol
Conditions | Yield |
---|---|
In toluene for 16.5h; Reflux; Inert atmosphere; Dean-Stark; | 56% |
2-(4-fluorobenzoyl)benzoic acid
ethylenediamine
9b-(4-fluorophenyl)-2,3-dihydro-1H-imidazo[2,1-a]isoindol-5(9bH)-one
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene for 4h; Dean-Stark; Inert atmosphere; Reflux; | 55.5% |
In 5,5-dimethyl-1,3-cyclohexadiene Reflux; Dean-Stark; |
2-(4-fluorobenzoyl)benzoic acid
potassium cyanide
1-(4-fluorophenyl)-3-oxo-1,3-dihydro-2-benzofuran-1-carboxamide
Conditions | Yield |
---|---|
With acetic acid at 115 - 125℃; for 48h; | 50% |
2-(4-fluorobenzoyl)benzoic acid
3-methyl-phenol
A
3-(4-fluorophenyl)-3-(2-hydroxy-4-methylphenyl)phthalide
B
3-(4-fluorophenyl)-3-(4-hydroxy-2-methylphenyl)phthalide
Conditions | Yield |
---|---|
With zinc(II) chloride at 115 - 120℃; for 8h; | A 32% B 48% |
Conditions | Yield |
---|---|
With nitric acid; acetic acid at 4 - 20℃; for 3h; | 46% |
methanol
2-(4-fluorobenzoyl)benzoic acid
methyl 2-(4-fluorobenzoyl)benzoate
Conditions | Yield |
---|---|
With sulfuric acid |
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