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Hubei Langyou International Trading Co., Ltd

Advantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best s

China Factory 99% SODIUM PERCHLORATE MONOHYDRATE 7791-07-3

Cas:7791-07-3

Min.Order:10 Gram

Negotiable

Type:Other

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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

Sodium perchlorate monohydrate

Cas:7791-07-3

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Hangzhou Dingyan Chem Co., Ltd

Items Standard Result Appearance White crystalline powder Complies Assay(NaClO4·H2O) 98%mi

High purity Sodium perchlorate monohydrate with high quality and best price cas:7791-07-3

Cas:7791-07-3

Min.Order:1 Metric Ton

FOB Price: $1500.0 / 2000.0

Type:Manufacturers

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality Sodium Perchlorate Monohydrate??? supplier in China

Cas:7791-07-3

Min.Order:0 Metric Ton

Negotiable

Type:Manufacturers

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Sodium Perchlorate Monohydrate

Cas:7791-07-3

Min.Order:1

Negotiable

Type:Other

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Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

Large Stock 99.0% Sodium perchlorate monohydrate 7791-07-3 Producer

Cas:7791-07-3

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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Chemwill Asia Co., Ltd.

Sodium perchlorate monohydrate CAS 7791-07-3 In stock

Cas:7791-07-3

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Manufacturers

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Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

SODIUM PERCHLORATE MONOHYDRATE

Cas:7791-07-3

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

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Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

ClH2NaO5 SODIUM PERCHLORATE MONOHYDRATE 7791-07-3

Cas:7791-07-3

Min.Order:1 Metric Ton

Negotiable

Type:Lab/Research institutions

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Pharmaceutical Grade CAS 7791-07-3 with competitive price

Cas:7791-07-3

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

High purity Sodium perchlorate monohydrate with high quality and best price cas:7791-07-3

Cas:7791-07-3

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Perchloric acid, sodiumsalt, monohydrate (8CI,9CI) 7791-07-3

Cas:7791-07-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Qingdao Beluga Import and Export Co., LTD

SODIUM PERCHLORATE MONOHYDRATE CAS:7791-07-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality org

SODIUM PERCHLORATE MONOHYDRATE CAS:7791-07-3

Cas:7791-07-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Perchloric acid, sodiumsalt, monohydrate (8CI,9CI)

Cas:7791-07-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s

SODIUM PERCHLORATE MONOHYDRATE

Cas:7791-07-3

Min.Order:1 Kilogram

FOB Price: $10.0 / 100.0

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High purity Sodium perchlorate monohydrate

Cas:7791-07-3

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

High purity Sodium perchlorate monohydrate with high quality and best price cas:7791-07-3

Cas:7791-07-3

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

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TaiChem Taizhou Limited

Established in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site

SODIUM PERCHLORATE MONOHYDRATE

Cas:7791-07-3

Min.Order:10 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

Sodium perchlorate monohydrate

Cas:7791-07-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Jiangsu Qianyu Molecular Technology Co., LTD.

Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

Best OfferSODIUM PERCHLORATE MONOHYDRATE

Cas:7791-07-3

Min.Order:0

Negotiable

Type:Trading Company

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EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

High purity Sodium perchlorate monohydrate with high quality and best price cas:7791-07-3

Cas:7791-07-3

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

High purity Sodium perchlorate monohydrate with high quality and best price cas:7791-07-3

Cas:7791-07-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

High purity Sodium perchlorate monohydrate with high quality and best price cas:7791-07-3

Cas:7791-07-3

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

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Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

Perchloric acid sodium salt monohydrate

Cas:7791-07-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Golden Pharma Co., Limited

GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation

SODIUM PERCHLORATE MONOHYDRATE

Cas:7791-07-3

Min.Order:1 Kilogram

Negotiable

Type:Other

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Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

High purity Sodium perchlorate monohydrate with high quality and best price cas:7791-07-3

Cas:7791-07-3

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

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Win-Win chemical Co.Ltd

Stock products, own laboratoryAppearance:white to off-white powder Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

Sodium perchlorate monohydrate cas no. 7791-07-3 98%

Cas:7791-07-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

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GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

Sodium perchlorate 1-hydrate

Cas:7791-07-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

Sodium perchlorate monohydrate

Cas:7791-07-3

Min.Order:0

Negotiable

Type:Other

inquiry

Aecochem Corp.

Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS

Sodium Perchlorate Monohydrate

Cas:7791-07-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Synthetic route

perchloric acid
7601-90-3

perchloric acid

water
7732-18-5

water

sodium hydrogencarbonate
144-55-8

sodium hydrogencarbonate

sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

Conditions
ConditionsYield
In perchloric acid by a react. of HClO4 with NaHCO3; evapn. to incipient crystn.;
sodium perchlorate

sodium perchlorate

sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

Conditions
ConditionsYield
In water crystn. below 52.75°C;
In water crystn. below 52.75°C;
perchloric acid
7601-90-3

perchloric acid

sodium carbonate
497-19-8

sodium carbonate

sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

Conditions
ConditionsYield
In not given neutralization, concg. to satn. concn., hot filtration, cooling the filtrate at stirring; recrystn. from water twice;
In perchloric acid dissoln. of carbonate in HClO4 (72 %), repeated recrystn. (H2O);
In not given neutralization, concg. to satn. concn., hot filtration, cooling the filtrate at stirring; recrystn. from water twice, washing by dry ether, drying in vac. for 10 h at ambient temp.;
In not given neutralization, concg. to satn. concn., hot filtration, cooling the filtrate at stirring; recrystn. from water twice;
In not given neutralization, concg. to satn. concn., hot filtration, cooling the filtrate at stirring; recrystn. from water twice, washing by dry ether, drying in vac. for 10 h at ambient temp.;
sodium carbonate
497-19-8

sodium carbonate

sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

Conditions
ConditionsYield
With aq. HClO4 dry box.;
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

{(NH3)5IrOCHN(CH3)2}(3+)*3ClO4(1-)={(NH3)5IrOCHN(CH3)2}(ClO4)3
88035-85-2

{(NH3)5IrOCHN(CH3)2}(3+)*3ClO4(1-)={(NH3)5IrOCHN(CH3)2}(ClO4)3

{(NH3)5IrOOCH}(2+)*2ClO4(1-)={(NH3)5IrOOCH}(ClO4)2
15646-83-0

{(NH3)5IrOOCH}(2+)*2ClO4(1-)={(NH3)5IrOOCH}(ClO4)2

Conditions
ConditionsYield
With sodium hydroxide In water Kinetics; stirred for 10 min at ambient temp., NaClO4*H2O was added in H2O; cooled, filtered, elem. anal.;100%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

[PdCl(η(3)-CH2C(Me)C(Me)2)]2

[PdCl(η(3)-CH2C(Me)C(Me)2)]2

2-(propane-2-sulfanylmethyl)-pyridine

2-(propane-2-sulfanylmethyl)-pyridine

[Pd(η3-1,1,2-Me3C3H2)(2-isopropylthiomethylpyridine)](ClO4)
460720-55-2

[Pd(η3-1,1,2-Me3C3H2)(2-isopropylthiomethylpyridine)](ClO4)

Conditions
ConditionsYield
In methanol; dichloromethane stirred at room temp. under N2 for 1 h; evapd. in vacuo, residue dissolved in CH2Cl2, treated with activated charcoal, filtered through celite, filtrate was concd., treated with Et2O, ppt. was collected; elem. anal.;99%
4,4'-bipyridine
553-26-4

4,4'-bipyridine

sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

silver(I) acetate
563-63-3

silver(I) acetate

Ag(4,4'-bipyridine)(perchlorate)

Ag(4,4'-bipyridine)(perchlorate)

Conditions
ConditionsYield
In water at 20℃; for 2h; Sealed tube;99%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

cis-{Pt(P(CH3)3)2(μ-OH)}2(NO3)2

cis-{Pt(P(CH3)3)2(μ-OH)}2(NO3)2

di(cis-[bis(trimethylphosphane)(μ-hydroxo)platinum(II)]) nitrate

di(cis-[bis(trimethylphosphane)(μ-hydroxo)platinum(II)]) nitrate

Conditions
ConditionsYield
In not given to Pt-salt NaClO4*H2O added; filtered, washed (H2O), dried in vac., elem. anal.;98%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

tetrakis(acetonitrile)palladium(II) tetrafluoroborate

tetrakis(acetonitrile)palladium(II) tetrafluoroborate

C4H3SC4H2SCHNCH2CH((OC2H4OC2H4)2O)CH2

C4H3SC4H2SCHNCH2CH((OC2H4OC2H4)2O)CH2

acetonitrile
75-05-8

acetonitrile

Pd(2+)*2CH3CN*2BF4(1-)*Na(1+)*ClO4(1-)*C4H3SC4H2SCHNCH2CH((OC2H4OC2H4)2O)CH2=Pd(CH3CN)2(C20H27NO5S2)(BF4)2NaClO4

Pd(2+)*2CH3CN*2BF4(1-)*Na(1+)*ClO4(1-)*C4H3SC4H2SCHNCH2CH((OC2H4OC2H4)2O)CH2=Pd(CH3CN)2(C20H27NO5S2)(BF4)2NaClO4

Conditions
ConditionsYield
In acetonitrile equimol., a soln. of salt added to a soln. of S compd., stirred overnight at room temp.; solvent evapd., residue washed (cold diethyl ether), dried (vac.); elem.anal.;98%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

C21H24N3Pd(1+)*ClO4(1-)

C21H24N3Pd(1+)*ClO4(1-)

triphenylphosphine
603-35-0

triphenylphosphine

C39H39N3PPd(1+)*ClO4(1-)

C39H39N3PPd(1+)*ClO4(1-)

Conditions
ConditionsYield
Stage #1: C21H24N3Pd(1+)*ClO4(1-); triphenylphosphine In dichloromethane for 0.166667h; Inert atmosphere; Schlenk technique;
Stage #2: sodium perchlorate monohydrate In dichloromethane at 20℃; for 1h; Inert atmosphere; Schlenk technique;
98%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

C12H15ClN2Pd

C12H15ClN2Pd

triphenylphosphine
603-35-0

triphenylphosphine

C30H30N2PPd(1+)*ClO4(1-)

C30H30N2PPd(1+)*ClO4(1-)

Conditions
ConditionsYield
In methanol; dichloromethane at 20℃; for 0.5h; Inert atmosphere; Schlenk technique;98%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

bis(η3-allyl-μ-chloropalladium(II))

bis(η3-allyl-μ-chloropalladium(II))

2-<(phenylseleno)methyl>pyridine
76358-92-4

2-<(phenylseleno)methyl>pyridine

Pd(II)(η3-C3H5)(C5H4NCH2SeC6H5) perchlorate

Pd(II)(η3-C3H5)(C5H4NCH2SeC6H5) perchlorate

Conditions
ConditionsYield
In dichloromethane mixed, stirred for 30 min; concd.(vac.), treated with activated charcoal in CH2Cl2, filtered, conctd., pptd.(diethyl ether), elem. anal., IR, NMR;97.6%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

bis(μ-chloro)bis{(1,2,3-η)-3-methyl-2-butenyl}palladium
12288-41-4

bis(μ-chloro)bis{(1,2,3-η)-3-methyl-2-butenyl}palladium

2-(phenyl-thiomethyl)-6-methyl-pyridine

2-(phenyl-thiomethyl)-6-methyl-pyridine

Pd(II)(η1,1-dimethyl-C3H3)(C5H3CH3NCH2SC6H5) perchlorate
404361-92-8

Pd(II)(η1,1-dimethyl-C3H3)(C5H3CH3NCH2SC6H5) perchlorate

Conditions
ConditionsYield
In dichloromethane mixed, stirred for 30 min; concd.(vac.), treated with activated charcoal in CH2Cl2, filtered, conctd., pptd.(diethyl ether), elem. anal., IR, NMR;97.3%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

[Au(C6H4N2C6H5)Cl2]
81033-01-4

[Au(C6H4N2C6H5)Cl2]

[Au(C6H4N2C6H5)(C5H5N)2](2+)*2ClO4(1-)=[Au(C6H4N2C6H5)(C5H5N)2](ClO4)2

[Au(C6H4N2C6H5)(C5H5N)2](2+)*2ClO4(1-)=[Au(C6H4N2C6H5)(C5H5N)2](ClO4)2

Conditions
ConditionsYield
With pyridine In acetone byproducts: NaCl; stirring (1 h, room temp.); evapn., extn. (CH2Cl2), filtration, concn., pptn. on Et2O addn., recrystn. (CH2Cl2/Et2O); elem. anal.;97%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

(η3-allyl)(N,N'-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene)chloropalladium(II)

(η3-allyl)(N,N'-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene)chloropalladium(II)

triphenylphosphine
603-35-0

triphenylphosphine

[Pd(1,3-dimesityl-2,3-dihydroimidazol-2-ylidene)(allyl)(triphenylphosphine)]ClO4

[Pd(1,3-dimesityl-2,3-dihydroimidazol-2-ylidene)(allyl)(triphenylphosphine)]ClO4

Conditions
ConditionsYield
In methanol; dichloromethane byproducts: NaCl; addn. of soln. of P compd. in CH2Cl2 to soln. of Pd complex in CH2Cl2, addn. of soln. of Na compd. in MeOH; filtration, stirring (30 min), evapn., dissolving in CH2Cl2, treatment with activated charcoal, filtration (Celite), concn. under reduced pressure, addn. of Et2O, filtration, washing with Et2O and n-pentane, drying under vacuum, elem. anal.;97%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

bis(η3-allyl-μ-chloropalladium(II))

bis(η3-allyl-μ-chloropalladium(II))

2,6-dimethylphenyl isonitrile
119072-54-7, 2769-71-3

2,6-dimethylphenyl isonitrile

triphenylphosphine
603-35-0

triphenylphosphine

[Pd(2,6-dimethylphenylisocyanide)(triphenylphosphine)(allyl)]ClO4
1269182-47-9

[Pd(2,6-dimethylphenylisocyanide)(triphenylphosphine)(allyl)]ClO4

Conditions
ConditionsYield
In methanol; dichloromethane byproducts: NaCl; addn. of soln. of N compd. in CH2Cl2 to soln. of Pd complex in CH2Cl2, addn. of soln. of PPh3 in CH2Cl2, addn. of Na compd. in MeOH; filtration, stirring (30 min), evapn. under reduced pressure, dissolvingin CH2Cl2, treatment with charcoal, filtration (Celite), concn. under r educed pressure, addn. of Et2O, filtration, washing (Et2O, pentane), drying under vacuum, elem. anal.;97%
N,N-bis(-pyridin-2ylmethyl)benzenamine
301668-92-8

N,N-bis(-pyridin-2ylmethyl)benzenamine

dichloro bis(acetonitrile) palladium(II)
21264-30-2, 90243-59-7, 14592-56-4

dichloro bis(acetonitrile) palladium(II)

sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

N,N-di(2-picolyl)aniline(chloro)PdII perchlorate
1616255-21-0

N,N-di(2-picolyl)aniline(chloro)PdII perchlorate

Conditions
ConditionsYield
In ethanol at 20℃; for 12h;96.8%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

PdCl2(P(C6H5)3)(C4H4N2)

PdCl2(P(C6H5)3)(C4H4N2)

PdCl(P(C6H5)3)2(C4H4N2)(1+)*ClO4(1-)=(PdCl(P(C6H5)3)2(C4H4N2))(ClO4)

PdCl(P(C6H5)3)2(C4H4N2)(1+)*ClO4(1-)=(PdCl(P(C6H5)3)2(C4H4N2))(ClO4)

Conditions
ConditionsYield
With P(C6H5)3 In methanol; dichloromethane Pd complex treated with PPh3; NaClO4*H2O added to the soln.; stirring for 10 min; evapn.; extn. with CH2Cl2 and charcoal; filtration; concn.; addn. of Et2O; elem. anal.;96.3%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

bis(η3-allyl-μ-chloropalladium(II))

bis(η3-allyl-μ-chloropalladium(II))

2-(phenyl-selenomethyl)-6-methyl-pyridine
404361-88-2

2-(phenyl-selenomethyl)-6-methyl-pyridine

Pd(II)(η3-C3H5)(C5H3CH3NCH2SeC6H5) perchlorate

Pd(II)(η3-C3H5)(C5H3CH3NCH2SeC6H5) perchlorate

Conditions
ConditionsYield
In dichloromethane mixed, stirred for 30 min; concd.(vac.), treated with activated charcoal in CH2Cl2, filtered, conctd., pptd.(diethyl ether), elem. anal., IR, NMR;96.2%
perchloric acid
7601-90-3

perchloric acid

water
7732-18-5

water

sodium hydrogencarbonate
144-55-8

sodium hydrogencarbonate

sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

Conditions
ConditionsYield
In perchloric acid by a react. of HClO4 with NaHCO3; evapn. to incipient crystn.;
sodium perchlorate

sodium perchlorate

sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

Conditions
ConditionsYield
In water crystn. below 52.75°C;
In water crystn. below 52.75°C;
perchloric acid
7601-90-3

perchloric acid

sodium carbonate
497-19-8

sodium carbonate

sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

Conditions
ConditionsYield
In not given neutralization, concg. to satn. concn., hot filtration, cooling the filtrate at stirring; recrystn. from water twice;
In perchloric acid dissoln. of carbonate in HClO4 (72 %), repeated recrystn. (H2O);
In not given neutralization, concg. to satn. concn., hot filtration, cooling the filtrate at stirring; recrystn. from water twice, washing by dry ether, drying in vac. for 10 h at ambient temp.;
In not given neutralization, concg. to satn. concn., hot filtration, cooling the filtrate at stirring; recrystn. from water twice;
In not given neutralization, concg. to satn. concn., hot filtration, cooling the filtrate at stirring; recrystn. from water twice, washing by dry ether, drying in vac. for 10 h at ambient temp.;
sodium carbonate
497-19-8

sodium carbonate

sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

Conditions
ConditionsYield
With aq. HClO4 dry box.;
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

{(NH3)5IrOCHN(CH3)2}(3+)*3ClO4(1-)={(NH3)5IrOCHN(CH3)2}(ClO4)3
88035-85-2

{(NH3)5IrOCHN(CH3)2}(3+)*3ClO4(1-)={(NH3)5IrOCHN(CH3)2}(ClO4)3

{(NH3)5IrOOCH}(2+)*2ClO4(1-)={(NH3)5IrOOCH}(ClO4)2
15646-83-0

{(NH3)5IrOOCH}(2+)*2ClO4(1-)={(NH3)5IrOOCH}(ClO4)2

Conditions
ConditionsYield
With sodium hydroxide In water Kinetics; stirred for 10 min at ambient temp., NaClO4*H2O was added in H2O; cooled, filtered, elem. anal.;100%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

[PdCl(η(3)-CH2C(Me)C(Me)2)]2

[PdCl(η(3)-CH2C(Me)C(Me)2)]2

2-(propane-2-sulfanylmethyl)-pyridine

2-(propane-2-sulfanylmethyl)-pyridine

[Pd(η3-1,1,2-Me3C3H2)(2-isopropylthiomethylpyridine)](ClO4)
460720-55-2

[Pd(η3-1,1,2-Me3C3H2)(2-isopropylthiomethylpyridine)](ClO4)

Conditions
ConditionsYield
In methanol; dichloromethane stirred at room temp. under N2 for 1 h; evapd. in vacuo, residue dissolved in CH2Cl2, treated with activated charcoal, filtered through celite, filtrate was concd., treated with Et2O, ppt. was collected; elem. anal.;99%
4,4'-bipyridine
553-26-4

4,4'-bipyridine

sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

silver(I) acetate
563-63-3

silver(I) acetate

Ag(4,4'-bipyridine)(perchlorate)

Ag(4,4'-bipyridine)(perchlorate)

Conditions
ConditionsYield
In water at 20℃; for 2h; Sealed tube;99%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

cis-{Pt(P(CH3)3)2(μ-OH)}2(NO3)2

cis-{Pt(P(CH3)3)2(μ-OH)}2(NO3)2

di(cis-[bis(trimethylphosphane)(μ-hydroxo)platinum(II)]) nitrate

di(cis-[bis(trimethylphosphane)(μ-hydroxo)platinum(II)]) nitrate

Conditions
ConditionsYield
In not given to Pt-salt NaClO4*H2O added; filtered, washed (H2O), dried in vac., elem. anal.;98%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

tetrakis(acetonitrile)palladium(II) tetrafluoroborate

tetrakis(acetonitrile)palladium(II) tetrafluoroborate

C4H3SC4H2SCHNCH2CH((OC2H4OC2H4)2O)CH2

C4H3SC4H2SCHNCH2CH((OC2H4OC2H4)2O)CH2

acetonitrile
75-05-8

acetonitrile

Pd(2+)*2CH3CN*2BF4(1-)*Na(1+)*ClO4(1-)*C4H3SC4H2SCHNCH2CH((OC2H4OC2H4)2O)CH2=Pd(CH3CN)2(C20H27NO5S2)(BF4)2NaClO4

Pd(2+)*2CH3CN*2BF4(1-)*Na(1+)*ClO4(1-)*C4H3SC4H2SCHNCH2CH((OC2H4OC2H4)2O)CH2=Pd(CH3CN)2(C20H27NO5S2)(BF4)2NaClO4

Conditions
ConditionsYield
In acetonitrile equimol., a soln. of salt added to a soln. of S compd., stirred overnight at room temp.; solvent evapd., residue washed (cold diethyl ether), dried (vac.); elem.anal.;98%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

C21H24N3Pd(1+)*ClO4(1-)

C21H24N3Pd(1+)*ClO4(1-)

triphenylphosphine
603-35-0

triphenylphosphine

C39H39N3PPd(1+)*ClO4(1-)

C39H39N3PPd(1+)*ClO4(1-)

Conditions
ConditionsYield
Stage #1: C21H24N3Pd(1+)*ClO4(1-); triphenylphosphine In dichloromethane for 0.166667h; Inert atmosphere; Schlenk technique;
Stage #2: sodium perchlorate monohydrate In dichloromethane at 20℃; for 1h; Inert atmosphere; Schlenk technique;
98%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

C12H15ClN2Pd

C12H15ClN2Pd

triphenylphosphine
603-35-0

triphenylphosphine

C30H30N2PPd(1+)*ClO4(1-)

C30H30N2PPd(1+)*ClO4(1-)

Conditions
ConditionsYield
In methanol; dichloromethane at 20℃; for 0.5h; Inert atmosphere; Schlenk technique;98%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

bis(η3-allyl-μ-chloropalladium(II))

bis(η3-allyl-μ-chloropalladium(II))

2-<(phenylseleno)methyl>pyridine
76358-92-4

2-<(phenylseleno)methyl>pyridine

Pd(II)(η3-C3H5)(C5H4NCH2SeC6H5) perchlorate

Pd(II)(η3-C3H5)(C5H4NCH2SeC6H5) perchlorate

Conditions
ConditionsYield
In dichloromethane mixed, stirred for 30 min; concd.(vac.), treated with activated charcoal in CH2Cl2, filtered, conctd., pptd.(diethyl ether), elem. anal., IR, NMR;97.6%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

bis(μ-chloro)bis{(1,2,3-η)-3-methyl-2-butenyl}palladium
12288-41-4

bis(μ-chloro)bis{(1,2,3-η)-3-methyl-2-butenyl}palladium

2-(phenyl-thiomethyl)-6-methyl-pyridine

2-(phenyl-thiomethyl)-6-methyl-pyridine

Pd(II)(η1,1-dimethyl-C3H3)(C5H3CH3NCH2SC6H5) perchlorate
404361-92-8

Pd(II)(η1,1-dimethyl-C3H3)(C5H3CH3NCH2SC6H5) perchlorate

Conditions
ConditionsYield
In dichloromethane mixed, stirred for 30 min; concd.(vac.), treated with activated charcoal in CH2Cl2, filtered, conctd., pptd.(diethyl ether), elem. anal., IR, NMR;97.3%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

[Au(C6H4N2C6H5)Cl2]
81033-01-4

[Au(C6H4N2C6H5)Cl2]

[Au(C6H4N2C6H5)(C5H5N)2](2+)*2ClO4(1-)=[Au(C6H4N2C6H5)(C5H5N)2](ClO4)2

[Au(C6H4N2C6H5)(C5H5N)2](2+)*2ClO4(1-)=[Au(C6H4N2C6H5)(C5H5N)2](ClO4)2

Conditions
ConditionsYield
With pyridine In acetone byproducts: NaCl; stirring (1 h, room temp.); evapn., extn. (CH2Cl2), filtration, concn., pptn. on Et2O addn., recrystn. (CH2Cl2/Et2O); elem. anal.;97%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

(η3-allyl)(N,N'-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene)chloropalladium(II)

(η3-allyl)(N,N'-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene)chloropalladium(II)

triphenylphosphine
603-35-0

triphenylphosphine

[Pd(1,3-dimesityl-2,3-dihydroimidazol-2-ylidene)(allyl)(triphenylphosphine)]ClO4

[Pd(1,3-dimesityl-2,3-dihydroimidazol-2-ylidene)(allyl)(triphenylphosphine)]ClO4

Conditions
ConditionsYield
In methanol; dichloromethane byproducts: NaCl; addn. of soln. of P compd. in CH2Cl2 to soln. of Pd complex in CH2Cl2, addn. of soln. of Na compd. in MeOH; filtration, stirring (30 min), evapn., dissolving in CH2Cl2, treatment with activated charcoal, filtration (Celite), concn. under reduced pressure, addn. of Et2O, filtration, washing with Et2O and n-pentane, drying under vacuum, elem. anal.;97%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

bis(η3-allyl-μ-chloropalladium(II))

bis(η3-allyl-μ-chloropalladium(II))

2,6-dimethylphenyl isonitrile
119072-54-7, 2769-71-3

2,6-dimethylphenyl isonitrile

triphenylphosphine
603-35-0

triphenylphosphine

[Pd(2,6-dimethylphenylisocyanide)(triphenylphosphine)(allyl)]ClO4
1269182-47-9

[Pd(2,6-dimethylphenylisocyanide)(triphenylphosphine)(allyl)]ClO4

Conditions
ConditionsYield
In methanol; dichloromethane byproducts: NaCl; addn. of soln. of N compd. in CH2Cl2 to soln. of Pd complex in CH2Cl2, addn. of soln. of PPh3 in CH2Cl2, addn. of Na compd. in MeOH; filtration, stirring (30 min), evapn. under reduced pressure, dissolvingin CH2Cl2, treatment with charcoal, filtration (Celite), concn. under r educed pressure, addn. of Et2O, filtration, washing (Et2O, pentane), drying under vacuum, elem. anal.;97%
N,N-bis(-pyridin-2ylmethyl)benzenamine
301668-92-8

N,N-bis(-pyridin-2ylmethyl)benzenamine

dichloro bis(acetonitrile) palladium(II)
21264-30-2, 90243-59-7, 14592-56-4

dichloro bis(acetonitrile) palladium(II)

sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

N,N-di(2-picolyl)aniline(chloro)PdII perchlorate
1616255-21-0

N,N-di(2-picolyl)aniline(chloro)PdII perchlorate

Conditions
ConditionsYield
In ethanol at 20℃; for 12h;96.8%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

PdCl2(P(C6H5)3)(C4H4N2)

PdCl2(P(C6H5)3)(C4H4N2)

PdCl(P(C6H5)3)2(C4H4N2)(1+)*ClO4(1-)=(PdCl(P(C6H5)3)2(C4H4N2))(ClO4)

PdCl(P(C6H5)3)2(C4H4N2)(1+)*ClO4(1-)=(PdCl(P(C6H5)3)2(C4H4N2))(ClO4)

Conditions
ConditionsYield
With P(C6H5)3 In methanol; dichloromethane Pd complex treated with PPh3; NaClO4*H2O added to the soln.; stirring for 10 min; evapn.; extn. with CH2Cl2 and charcoal; filtration; concn.; addn. of Et2O; elem. anal.;96.3%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

bis(η3-allyl-μ-chloropalladium(II))

bis(η3-allyl-μ-chloropalladium(II))

2-(phenyl-selenomethyl)-6-methyl-pyridine
404361-88-2

2-(phenyl-selenomethyl)-6-methyl-pyridine

Pd(II)(η3-C3H5)(C5H3CH3NCH2SeC6H5) perchlorate

Pd(II)(η3-C3H5)(C5H3CH3NCH2SeC6H5) perchlorate

Conditions
ConditionsYield
In dichloromethane mixed, stirred for 30 min; concd.(vac.), treated with activated charcoal in CH2Cl2, filtered, conctd., pptd.(diethyl ether), elem. anal., IR, NMR;96.2%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]

bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]

2-(phenyl-selenomethyl)-6-methyl-pyridine
404361-88-2

2-(phenyl-selenomethyl)-6-methyl-pyridine

Pd(II)(η3-1-phenyl-C3H4)(C5H3CH3NCH2SeC6H5) perchlorate

Pd(II)(η3-1-phenyl-C3H4)(C5H3CH3NCH2SeC6H5) perchlorate

Conditions
ConditionsYield
In dichloromethane mixed, stirred for 30 min; concd.(vac.), treated with activated charcoal in CH2Cl2, filtered, conctd., pptd.(diethyl ether), elem. anal., IR, NMR;96%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

2,2',2''-triaminotriethylamine
4097-89-6

2,2',2''-triaminotriethylamine

1,4-dimethoxybenzene-2,6-dicarboxaldehyde
25224-72-0

1,4-dimethoxybenzene-2,6-dicarboxaldehyde

silver nitrate

silver nitrate

Ag2(C42H54N8O6)(2+)*2ClO4(1-)*4H2O = [Ag2(C42H54N8O6)](ClO4)2*4H2O

Ag2(C42H54N8O6)(2+)*2ClO4(1-)*4H2O = [Ag2(C42H54N8O6)](ClO4)2*4H2O

Conditions
ConditionsYield
In ethanol addn. of the amine in EtOH to the dialdehyde and AgNO3 in EtOH, stirring, filtration, addn. of excess NaClO4*H2O in EtOH; elem. anal.;96%
pyridine
110-86-1

pyridine

sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

[Pt(phpytabn)Cl]

[Pt(phpytabn)Cl]

C25H20N5Pt(1+)*ClO4(1-)

C25H20N5Pt(1+)*ClO4(1-)

Conditions
ConditionsYield
Stage #1: pyridine; [Pt(phpytabn)Cl] In methanol; acetonitrile at 60℃; for 0.75h;
Stage #2: sodium perchlorate monohydrate at 20℃; for 0.5h;
96%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

PdCl2(P(C6H5)3)(C4H4N2)

PdCl2(P(C6H5)3)(C4H4N2)

PdCl(P(C6H5)3)2(C4H4N2)(1+)*ClO4(1-)=(PdCl(P(C6H5)3)2(C4H4N2))(ClO4)

PdCl(P(C6H5)3)2(C4H4N2)(1+)*ClO4(1-)=(PdCl(P(C6H5)3)2(C4H4N2))(ClO4)

Conditions
ConditionsYield
With P(C6H5)3 In methanol; dichloromethane Pd complex treated with PPh3; NaClO4*H2O added to the soln.; stirring for 10 min; evapn.; extn. with CH2Cl2 and charcoal; filtration; concn.; addn. of Et2O; elem. anal.;95.7%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

2-[(phenylsulfanyl)methyl]pyridine
71897-63-7

2-[(phenylsulfanyl)methyl]pyridine

bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]

bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]

Pd(II)(η3-1-phenyl-C3H4)(C5H3CH3NCH2SC6H5) perchlorate
404361-94-0

Pd(II)(η3-1-phenyl-C3H4)(C5H3CH3NCH2SC6H5) perchlorate

Conditions
ConditionsYield
In dichloromethane mixed, stirred for 30 min; concd.(vac.), treated with activated charcoal in CH2Cl2, filtered, conctd., pptd.(diethyl ether), elem. anal., IR, NMR;95.3%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

(ClPd(P(C6H5)3)2C5H3ClN)

(ClPd(P(C6H5)3)2C5H3ClN)

dimethyl sulfate
77-78-1

dimethyl sulfate

PdCl(P(C6H5)3)2C5H3NCH3Cl(1+)*ClO4(1-)=(PdCl(P(C6H5)3)2C5H3NCH3Cl)ClO4
92391-83-8

PdCl(P(C6H5)3)2C5H3NCH3Cl(1+)*ClO4(1-)=(PdCl(P(C6H5)3)2C5H3NCH3Cl)ClO4

Conditions
ConditionsYield
In dichloromethane reflux for 4 h, standing overnight at room temp., concn., pptn. with Et2O, dissoln. in CH2Cl2, addn. of NaClO4*H2O in MeOH; stirring for 10 min;; evapn., extn. with CH2Cl2 and charcoal, filtn., concn. and pptn. with Et2O, elem. anal.;;95%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

bis(1,4,7-trithiacyclononane)cobalt(II) bisperchlorate
97465-54-8

bis(1,4,7-trithiacyclononane)cobalt(II) bisperchlorate

[Co(1,4,7-trithiacyclononane)2](ClO4)3
102573-49-9

[Co(1,4,7-trithiacyclononane)2](ClO4)3

Conditions
ConditionsYield
With Na2S2O8 In water a soln. of Na2S2O8 added to a soln. of Co-complex; NaClO4*H2O added; pptd.; filtered; washed with ethanol and water; air-dried; elem. anal.;95%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

Pd2(C6H4)(O2CCH3)((CH3C5H3N)2)2(1+)*CH3CO2(1-)*3H2O={Pd2(C6H4)(O2CCH3)((CH3C5H3N)2)2}CH3COO*3H2O

Pd2(C6H4)(O2CCH3)((CH3C5H3N)2)2(1+)*CH3CO2(1-)*3H2O={Pd2(C6H4)(O2CCH3)((CH3C5H3N)2)2}CH3COO*3H2O

Pd2(C6H4)(O2CCH3)((CH3C5H3N)2)2(1+)*ClO4(1-)={Pd2(C6H4)(O2CCH3)((CH3C5H3N)2)2}ClO4

Pd2(C6H4)(O2CCH3)((CH3C5H3N)2)2(1+)*ClO4(1-)={Pd2(C6H4)(O2CCH3)((CH3C5H3N)2)2}ClO4

Conditions
ConditionsYield
In methanol addn. of methanolic soln. of NaClO4 to methanolic soln. of Pd compd., stirred for 12 h at ambient temp.; evapn., extn. (CH2Cl2), concn., diln. (hexane); elem. anal.;95%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]

bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]

2-(phenyl-thiomethyl)-6-methyl-pyridine

2-(phenyl-thiomethyl)-6-methyl-pyridine

Pd(II)(η1-phenyl-C3H4)(C5H4NCH2SC6H5) perchlorate
404361-90-6

Pd(II)(η1-phenyl-C3H4)(C5H4NCH2SC6H5) perchlorate

Conditions
ConditionsYield
In dichloromethane mixed, stirred for 30 min; concd.(vac.), treated with activated charcoal in CH2Cl2, filtered, conctd., pptd.(diethyl ether), elem. anal., IR, NMR;95%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

[Pd(1,3-dimesityl-2,3-dihydroimidazol-2-ylidene)(1,1-dimethylallyl)(chloride)]

[Pd(1,3-dimesityl-2,3-dihydroimidazol-2-ylidene)(1,1-dimethylallyl)(chloride)]

2,6-dimethylphenyl isonitrile
119072-54-7, 2769-71-3

2,6-dimethylphenyl isonitrile

[Pd(1,3-dimesityl-2,3-dihydroimidazol-2-ylidene)(1,1-dimethylallyl)(2,6-dimethylisocyanide)]ClO4

[Pd(1,3-dimesityl-2,3-dihydroimidazol-2-ylidene)(1,1-dimethylallyl)(2,6-dimethylisocyanide)]ClO4

Conditions
ConditionsYield
In methanol; dichloromethane byproducts: NaCl; addn. of soln. of CNC6H3Me2 in CH2Cl2 to Pd complex in CH2Cl2, addn. of soln. of Na compd. in MeOH; filtration, stirring for 30 min, evapn. under reduced pressure, dissolving in CH2Cl2, treatment with activated charcoal, filtration (Celite), concn., pptn. by addn. of Et2O, filtration, washing (Et2O, pentane), drying under vacuum, elem. anal.;95%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

[Pd(1,3-dimesitylimidazolidin-2-ylidene)(1,1-dimethylallyl)(chloride)]

[Pd(1,3-dimesitylimidazolidin-2-ylidene)(1,1-dimethylallyl)(chloride)]

2,6-dimethylphenyl isonitrile
119072-54-7, 2769-71-3

2,6-dimethylphenyl isonitrile

[Pd(1,3-dimesitylimidazolidin-2-ylidene)(1,1-dimethylallyl)(2,6-dimethylphenylisocyanide)]ClO4

[Pd(1,3-dimesitylimidazolidin-2-ylidene)(1,1-dimethylallyl)(2,6-dimethylphenylisocyanide)]ClO4

Conditions
ConditionsYield
In methanol; dichloromethane byproducts: NaCl; addn. of soln. of CNC6H3Me2 in CH2Cl2 to Pd complex in CH2Cl2, addn. of soln. of Na compd. in MeOH; filtration, stirring for 30 min, evapn. under reduced pressure, dissolving in CH2Cl2, treatment with activated charcoal, filtration (Celite), concn., pptn. by addn. of Et2O, filtration, washing (Et2O, pentane), drying under vacuum, elem. anal.;95%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

(2-methylallyl)palladium-chloride dimer

(2-methylallyl)palladium-chloride dimer

([1-(phenylthio)methylene-3-mesityl]imidazolyl-2-ene)silverbromide

([1-(phenylthio)methylene-3-mesityl]imidazolyl-2-ene)silverbromide

C23H27N2PdS(1+)*ClO4(1-)

C23H27N2PdS(1+)*ClO4(1-)

Conditions
ConditionsYield
Stage #1: (2-methylallyl)palladium-chloride dimer; ([1-(phenylthio)methylene-3-mesityl]imidazolyl-2-ene)silverbromide In dichloromethane at 20℃; Inert atmosphere;
Stage #2: sodium perchlorate monohydrate In methanol; dichloromethane Inert atmosphere;
95%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

bis(μ-chloro)bis{(1,2,3-η)-3-methyl-2-butenyl}palladium
12288-41-4

bis(μ-chloro)bis{(1,2,3-η)-3-methyl-2-butenyl}palladium

2-<(phenylseleno)methyl>pyridine
76358-92-4

2-<(phenylseleno)methyl>pyridine

Pd(II)(η3-C3H3(CH3)2)(C5H4NCH2SeC6H5) perchlorate

Pd(II)(η3-C3H3(CH3)2)(C5H4NCH2SeC6H5) perchlorate

Conditions
ConditionsYield
In dichloromethane mixed, stirred for 30 min; concd.(vac.), treated with activated charcoal in CH2Cl2, filtered, conctd., pptd.(diethyl ether), elem. anal., IR, NMR;94.7%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

PdCl(1,2-bis(diphenylphosphino)ethane)(C5H4N-C(2))

PdCl(1,2-bis(diphenylphosphino)ethane)(C5H4N-C(2))

chloroacetone
78-95-5

chloroacetone

cis-{PdCl((1-CH2COMe)C5H4N-C2)(dppe)}ClO4
141239-38-5

cis-{PdCl((1-CH2COMe)C5H4N-C2)(dppe)}ClO4

Conditions
ConditionsYield
In acetone Kinetics; reaction with excess chloride; stirred for 24 h at ambient temp.; addn. of perchlorate;; evapn.; extn. (CH2Cl2, charcoal); filtration; concn.; pptn. by addn. of Et2O; repptn. from CH2Cl2/Et2O; elem. anal.;94.4%
dichloro bis(acetonitrile) palladium(II)
21264-30-2, 90243-59-7, 14592-56-4

dichloro bis(acetonitrile) palladium(II)

sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

N,N-di(2-picolyl)benzylamine
26082-96-2

N,N-di(2-picolyl)benzylamine

N,N-di(2-picolyl)benzylamine(chloro)PdII perchlorate
1616255-18-5

N,N-di(2-picolyl)benzylamine(chloro)PdII perchlorate

Conditions
ConditionsYield
In ethanol at 20℃; for 12h;94.2%

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