As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:87-59-2
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryProduct Description Product website: http://www.finerchem.com Product Name 2,3-Dimethylphenylamine CAS No. 87-59-2 Appearance
Cas:87-59-2
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inquiryhigh quality Appearance:White or off white powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:87-59-2
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inquiryHebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car
Cas:87-59-2
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:87-59-2
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inquiry2,3-Dimethylaniline(2,3-Xylidine) CAS No.: 87-59-2 UN No.:1711 Appearance: Colorless or light brown liquid Assay: ≥99.0% Water (by K Fisher): ≤0.2% [Packing&Storage] 2,3-Dimethylaniline stores in a w
Cas:87-59-2
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
2,3-Dimethylaniline CAS: 87-59-2 Superiority Item Standard Appearance Light yellow or light brown liquid Purity,% 99min Moisture, % 0.2max
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:87-59-2
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inquirySuperior quality, moderate price & quick delivery. Appearance:Brown liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Intermediates Tr
Product name: 2,3-Dimethylaniline CAS No.:87-59-2 Molecule Formula:C8H11N Molecule Weight:121.98 Purity: 99.0% Package: 200kg/drum Description:Colorless to dark red liquid Manufacture Standards:Enterprise Standard
Cas:87-59-2
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:87-59-2
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inquiryProductName:2,3-Dimethylaniline CAS:87-59-2 Molecular Formula:C8H11N Molecular Weight:121.18000 Appearance:Colorless or light brown liquid Assay:≥99.0% Water content:≤0.20% Appearance:Colorless transparent liquid Storage:keep
Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe
Cas:87-59-2
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inquiryCapability on chemical synthesis1. Beijing High-Tech Enterprises2. Strong R&D Team3. 8 years of experiences in R & D of high-tech Catalyst;4. 5000 production techniques, 69 items of national patents, and 360 kinds of products on sales;5. The producti
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Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:87-59-2
Min.Order:1 Kilogram
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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2,3-DimethylanilineAppearance:White powder Storage:Shading, sealed and preserved. Package:25 kg/barrels Application:An organic synthetic intermediate used in the synthesis of medicine. Transportation:By express (Door to door) such as FEDEX, DHL, EMS
1-tert-butyl-N-(2,3-dimethylphenyl)-1,1-dimethylsilanamine
2,3-Dimethylaniline
Conditions | Yield |
---|---|
With silica gel In ethanol; water at 20℃; for 2h; | 100% |
Conditions | Yield |
---|---|
With sodium sulfide; tetrabutylammomium bromide In water; toluene at 80℃; for 0.75h; Zinin reduction; | 96.8% |
Stage #1: 2,3-dimethylnitrobenzene In water at 20℃; for 0.05h; Green chemistry; Stage #2: With glycerol In water at 20℃; for 1.5h; Green chemistry; | 95% |
With sodium tetrahydroborate In water at 60 - 70℃; for 0.133333h; Green chemistry; | 95% |
2-amino-6-methylbenzoic acid methyl ester
2,3-Dimethylaniline
Conditions | Yield |
---|---|
With sodium bis(2-methoxyethoxy)aluminium dihydride In toluene for 3h; Heating; | 75% |
Conditions | Yield |
---|---|
With tris-(2-chloro-ethyl)-amine; trifluorormethanesulfonic acid; trifluoroacetic acid In chloroform at 25℃; for 1h; | A 44% B 30% |
bei der Nitrierung und Hydrierung des Reaktionsprodukts in Gegenwart von Nickel bei 180-190grad; | |
With xenon difluoride; trimethylsilyl isocyanate; trifluorormethanesulfonic acid In dichloromethane at -78℃; |
3,4-dimethylbenzoic acid
A
3,4-Dimethylphenol
B
4-amino-o-xylene
C
2,3-Dimethylaniline
Conditions | Yield |
---|---|
With ammonia; water; copper(II) oxide at 220℃; for 0.5h; | A 3.5% B 43.1% C 0.9% |
2,3-Dimethylaniline
Conditions | Yield |
---|---|
With sodium amalgam |
Methyl fluoride
1-amino-3-methylbenzene
A
2,5-Dimethylaniline
B
4-amino-o-xylene
C
2,3-Dimethylaniline
Conditions | Yield |
---|---|
With oxygen In gaseous matrix at 80℃; Irradiation; | A 29 % Spectr. B 25 % Spectr. C 46 % Spectr. |
Conditions | Yield |
---|---|
In dichloromethane at 21.9℃; Equilibrium constant; |
Conditions | Yield |
---|---|
In dichloromethane at 21.9℃; Equilibrium constant; |
2,3-Dimethylaniline
Conditions | Yield |
---|---|
With iron; acetic acid |
2,3-Dimethylaniline
Conditions | Yield |
---|---|
With iron; acetic acid |
2,3-Dimethylaniline
Conditions | Yield |
---|---|
With acetic acid in mehrere Stufen; |
Conditions | Yield |
---|---|
at 280 - 300℃; bei der Einwirkung auf salzsaures Anilin im Autoklaven; |
hydrogenchloride
4-(2,3-dimethyl-phenylazo)-2,3-dimethyl-aniline
A
1,4-diamino-2,3-dimethylbenzene
B
2,3-Dimethylaniline
N-(2,3-dimethylphenyl)hydroxylamine
A
bis-(2,3-dimethyl-phenyl)-diazene-N-oxide
B
2,3-Dimethylaniline
sulfuric acid
tetramethyl-[1,4]benzoquinone-(2,3-dimethyl-phenylimine)-imine
A
Duroquinone
B
2,3-Dimethylaniline
2,3-dimethyl-6-(trisopropylsilyl)aniline
2,3-Dimethylaniline
Conditions | Yield |
---|---|
With trifluoroacetic acid In hexane for 5h; Heating; | 0.65 g |
2-methoxycarbonyl-3-methyl-6-(trisopropylsilyl)aniline
2,3-Dimethylaniline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 3.85 g / Red-Al / toluene / 3 h / Heating 2: 0.65 g / trifluoroacetic acid / hexane / 5 h / Heating View Scheme |
2-methoxycarbonyl-3-methyl-6,N-bis(trisopropylsilyl)aniline
2,3-Dimethylaniline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 91 percent / KF; HCl; water / methanol / 2 h / Heating 2: 75 percent / Red-Al / toluene / 3 h / Heating View Scheme | |
Multi-step reaction with 3 steps 1: 62 percent / KF; HCl; water / methanol / 2 h / Heating 2: 3.85 g / Red-Al / toluene / 3 h / Heating 3: 0.65 g / trifluoroacetic acid / hexane / 5 h / Heating View Scheme |
Conditions | Yield |
---|---|
With potassium hydroxide; sodium hydroxide |
2,3-Dimethylaniline
trifluoroacetic anhydride
N-(2,3-dimethylphenyl)-2,2,2-trifluoroacetamide
Conditions | Yield |
---|---|
In dichloromethane for 1h; Further stages; | 100% |
With triethylamine In dichloromethane for 1h; Ambient temperature; | 87% |
In diethyl ether | |
In dichloromethane at 0 - 20℃; for 12h; |
2-Bromoacetyl bromide
2,3-Dimethylaniline
2-bromo-N-(2',3'-dimethylphenyl)acetamide
Conditions | Yield |
---|---|
With triethylamine at 0℃; for 1h; Inert atmosphere; | 100% |
With sodium carbonate In water pH=9 - 10; | 99% |
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 1.5h; bromoacetylation; |
di-tert-butyl dicarbonate
2,3-Dimethylaniline
N-tert-butyloxycarbonyl-2,3-dimethylaniline
Conditions | Yield |
---|---|
With sodium carbonate In methanol at 20℃; for 1.5h; | 100% |
In neat (no solvent) at 80℃; for 0.166667h; Green chemistry; chemoselective reaction; | 98% |
at 20℃; for 0.0833333h; Green chemistry; | 95% |
With pyridinium trifluroacetate In neat (no solvent) at 20℃; for 0.3h; Green chemistry; | 93% |
In tetrahydrofuran for 12h; Reflux; |
Conditions | Yield |
---|---|
With tin(ll) chloride; ruthenium trichloride; triphenylphosphine In 1,4-dioxane at 180℃; for 20h; | 99% |
Conditions | Yield |
---|---|
With potassium carbonate In 5,5-dimethyl-1,3-cyclohexadiene | 99% |
N-tert-butoxycarbonyl-L-leucine
2,3-Dimethylaniline
Conditions | Yield |
---|---|
Stage #1: N-tert-butoxycarbonyl-L-leucine With 4-methyl-morpholine; isobutyl chloroformate In tetrahydrofuran at 0℃; for 0.5h; Inert atmosphere; Schlenk technique; Stage #2: 2,3-Dimethylaniline In tetrahydrofuran at 0 - 20℃; Inert atmosphere; Schlenk technique; | 99% |
Conditions | Yield |
---|---|
With Ni2B-Cu2O nanocomposite In neat (no solvent) at 40℃; for 0.0166667h; Reagent/catalyst; | 98% |
In chloroform at 20℃; for 2h; | 88% |
With pyridine at 0 - 20℃; | 80% |
Benzoyl isothiocyanate
2,3-Dimethylaniline
1-benzoyl-3-(2,3-dimethylphenyl)thiourea
Conditions | Yield |
---|---|
In acetone at 20℃; for 1h; | 98% |
In tetrahydrofuran at 60 - 65℃; for 0.166667h; Microwave irradiation; | 92% |
In acetone | 85% |
Conditions | Yield |
---|---|
Stage #1: N-Boc-D-Leu With 4-methyl-morpholine; isobutyl chloroformate In tetrahydrofuran at 0℃; for 0.5h; Inert atmosphere; Schlenk technique; Stage #2: 2,3-Dimethylaniline In tetrahydrofuran at 0 - 20℃; Inert atmosphere; Schlenk technique; | 98% |
Conditions | Yield |
---|---|
With 2'-dicyclohexylphosphanyl-6-hydroxy-biphenyl-3-sulfonic acid; palladium diacetate; sodium t-butanolate In diethylene glycol dimethyl ether at 120℃; for 14h; Buchwald-Hartwig Coupling; Inert atmosphere; | 98% |
benzenesulfonyl chloride
2,3-Dimethylaniline
2,3-dimethyl-N-(phenylsulfonyl)aniline
Conditions | Yield |
---|---|
With pyridine In dichloromethane | 97% |
C10H14O5
2,3-Dimethylaniline
dimethyl (1S,2S,4S,5S)-4-(2,3-dimethylphenylamino)-5-hydroxycyclohexane-1,2-dicarboxylate
Conditions | Yield |
---|---|
With indium(III) bromide In dichloromethane at 20℃; for 15h; | 97% |
Conditions | Yield |
---|---|
at 100℃; under 10343.2 Torr; Microwave irradiation; | 97% |
phenylethane 1,2-diol
2,3-Dimethylaniline
6,7-dimethyl-2-phenyl-1H-indole
Conditions | Yield |
---|---|
With tetrafluoroboric acid diethyl ether; {[(PCy3)(CO)RuH]4(μ-O)(μ-OH)2}; cyclopentene In 1,4-dioxane at 120℃; for 14h; Sealed tube; Schlenk technique; Inert atmosphere; regioselective reaction; | 97% |
Conditions | Yield |
---|---|
With 3-(1,1-dioxido-4-(3-(3-(3-sulfopropyl)-1H-imidazol-3-ium-1-yl)propyl)thiomorpholino-4-ium)propane-1-sulfonate trifluoromethanesulfonate In acetic acid butyl ester at 100℃; for 8h; Green chemistry; | 97% |
chloroacetyl chloride
2,3-Dimethylaniline
2-chloro-N-(2, 3-dimethylphenyl)acetamide
Conditions | Yield |
---|---|
With sodium hydroxide In dichloromethane; water for 18h; | 96% |
With potassium carbonate In acetone at 20℃; | 83% |
In benzene for 5h; Heating; | 60% |
Conditions | Yield |
---|---|
96% |
bromochlorobenzene
2,3-Dimethylaniline
2,3-dimethyl-4',4"-dichlorotriphenylamine
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; sodium t-butanolate In o-xylene for 12h; Inert atmosphere; Reflux; Schlenk technique; | 96% |
3-chlorobenzoyl isothiocyanate
2,3-Dimethylaniline
Conditions | Yield |
---|---|
In tetrahydrofuran at 60 - 65℃; under 760.051 Torr; for 0.025h; Microwave irradiation; | 96% |
potassium methanethiolate
2,3-Dimethylaniline
1,2-dimethyl-3-(methylsulfanyl)benzene
Conditions | Yield |
---|---|
Stage #1: 2,3-Dimethylaniline With sulfuric acid at 50℃; for 0.5h; Stage #2: With sodium nitrite In water at -10 - -5℃; for 1h; Stage #3: potassium methanethiolate In water at 20 - 35℃; for 4h; | 95.8% |
2,3-Dimethylaniline
sodium thiomethoxide
1,2-dimethyl-3-(methylsulfanyl)benzene
Conditions | Yield |
---|---|
Stage #1: 2,3-Dimethylaniline With hydrogenchloride In water at 50℃; for 0.5h; Stage #2: With sodium nitrite In water at -5 - 0℃; for 1h; Stage #3: sodium thiomethoxide In water at 35℃; for 2h; | 95.5% |
2,3-Dimethylaniline
3-nitrobenzenesulphonyl chloride
3-nitro-N-(2,3-dimethylphenyl)benzenesulfonamide
Conditions | Yield |
---|---|
With 4-methyl-morpholine In dichloromethane at 0℃; | 95% |
With 4-methyl-morpholine In dichloromethane at 0℃; for 12h; Acylation; | 95% |
With 4-methyl-morpholine In dichloromethane at 0 - 20℃; Substitution; |
tert-butyldimethylsilyl chloride
2,3-Dimethylaniline
1-tert-butyl-N-(2,3-dimethylphenyl)-1,1-dimethylsilanamine
Conditions | Yield |
---|---|
Stage #1: 2,3-Dimethylaniline With methyllithium In 2-methyltetrahydrofuran; diethyl ether at 0℃; Inert atmosphere; Stage #2: tert-butyldimethylsilyl chloride In 2-methyltetrahydrofuran; diethyl ether at 0 - 20℃; Inert atmosphere; | 95% |
phenylacetylene
2,3-Dimethylaniline
2,3-dimethyl-N-(1-phenylethylidene)benzenamine
Conditions | Yield |
---|---|
With silver trifluoromethanesulfonate; C17H25Cl2N3OPtS In toluene at 120℃; for 12h; Reagent/catalyst; | 95% |
With trifluorormethanesulfonic acid; [(S(CH2CH2C3H2N2(Bn))2-κ3C,C',S)PdBr]Br In toluene at 100℃; for 12h; | 48 %Chromat. |
para-bromotoluene
2,3-Dimethylaniline
2,3,4’,4’’-tetramethyltriphenylamine
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; sodium t-butanolate In o-xylene for 12h; Inert atmosphere; Reflux; Schlenk technique; | 95% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); (RSp,SRp)-tert-butyl([2.2]paracyclophan-4-yl)phosphine oxide; sodium t-butanolate In toluene at 105℃; Buchwald-Hartwig Coupling; | 95% |
With 2'-dicyclohexylphosphanyl-6-methoxy-biphenyl-3-sulfonic acid; palladium diacetate; sodium t-butanolate In diethylene glycol dimethyl ether at 120℃; for 48h; Buchwald-Hartwig Coupling; Inert atmosphere; | 27% |
Conditions | Yield |
---|---|
With 2'-dicyclohexylphosphanyl-6-methoxy-biphenyl-3-sulfonic acid; palladium diacetate; sodium t-butanolate In diethylene glycol dimethyl ether at 120℃; for 96h; Buchwald-Hartwig Coupling; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
Stage #1: ortho-chlorobenzoic acid With sodium carbonate In N,N-dimethyl-formamide at 80℃; for 0.5h; Stage #2: 2,3-Dimethylaniline With manganese(II) acetate In water; N,N-dimethyl-formamide; toluene at 120 - 130℃; Reagent/catalyst; | 94.8% |
Stage #1: ortho-chlorobenzoic acid With sodium carbonate In N,N-dimethyl-formamide at 80℃; for 1.16667h; Stage #2: 2,3-Dimethylaniline With copper In water; N,N-dimethyl-formamide; toluene at 104 - 123℃; | 91.3% |
With copper; sodium carbonate In N,N-dimethyl-formamide at 140℃; for 2h; | 90% |
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