HANGZHOU THINK CHEMICAL CO., LTD. (THINKCHEM) is an integrative corporation of trade, research and contract manufacture. With about ten years of business experiences on the marketing & distribution, thinkchem specializes in exp
Cas:976-71-6
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Min.Order:1 Kilogram
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Type:Trading Company
inquiryItems Standard Result Appearance Yellow Powder Complies Identification Corresponds to the retenti
Cas:976-71-6
Min.Order:1 Kilogram
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Type:Trading Company
inquiryCanrenone is an active metabolite of spironolactone that acts as an MCR antagonist, inhibiting aldosterone biosynthesis. it also blocks ouabain effects. Specification Analysis Test
1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; ...... Appearance:Yellow crystalline powder Storage:Store at RT Package:1kg/foi
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Type:Trading Company
inquiryHebei yanxi chemical co., LTD is a professional research, development and production enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low carbon environmental protection safety
Good products, good service. We have professional sales team working on sales service for 15 years. Good products can win good market but can not stand long without good service. We have strict sales regulation and service procedure to make sure yo
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Min.Order:50 Kilogram
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Type:Trading Company
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Cas:976-71-6
Min.Order:1 Gram
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Type:Manufacturers
inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api, intermedi
Shanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
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Min.Order:1 Kilogram
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Type:Manufacturers
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Product Name: Canrenone Synonyms: 11614r.p;17-(2-Carboxyethyl)17-hydroxy-3-oxoandrosta-4,6-dienelactone;17-(2-Carboxyethyl)17-hydroxyandrosta-4,6-dien-3-onelactone;17-hydroxy-3-oxo-,gamma-lactone,(17-alpha)-pregna-6-diene-21-carboxylicacid;17-Hydr
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Min.Order:1 Kilogram
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Min.Order:1 Kilogram
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Min.Order:1 Kilogram
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Min.Order:1 Kilogram
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Type:Lab/Research institutions
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Cas:976-71-6
Min.Order:1 Kilogram
FOB Price: $470.0 / 500.0
Type:Trading Company
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Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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Min.Order:1 Kilogram
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Type:Lab/Research institutions
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Min.Order:1 Kilogram
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Type:Trading Company
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Type:Lab/Research institutions
inquiryLorcaserin(856681-05-5)is an orally administered agent and a selective 5-HT2C receptor agonist for the treatment of obesity. It had been approved for marketing in US by FDA on 27 June in 2012. In clinical studies, lorcaserin h
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Cas:976-71-6
Min.Order:5 Gram
Negotiable
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:976-71-6
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Conditions | Yield |
---|---|
With mercury dichloride In ethanol Ambient temperature; | 95% |
With sodium methylate In tetrahydrofuran at 20℃; for 18h; Elimination; | 72% |
With potassium dihydrogenphosphate In ethanol at 40℃; Rate constant; Kinetics; Thermodynamic data; var. buffers, pH, temp., ionic strengh, spironolactone and buffer conc.; energy of activation; |
canrenone
Conditions | Yield |
---|---|
With NH2SO4 In methanol for 0.0833333h; Heating; | 92% |
With hydrogenchloride In chloroform for 8h; Heating; | 86% |
With acetic acid for 0.5h; Heating; |
canrenone
Conditions | Yield |
---|---|
With chloranil In methanol; water; 1,2-dichloro-ethane at 20℃; for 1h; | 84% |
canrenone
Conditions | Yield |
---|---|
Stage #1: 17β-hydroxy-3-ethoxy-17α-pregn-3,5-diene-21-carboxylic acid-γ-lactone With chloranil In methanol; dichloromethane; water at 20℃; for 1h; Stage #2: With sodium thiosulfate In methanol; water at 20℃; for 1h; | 83% |
Conditions | Yield |
---|---|
With chloranil In tert-butyl alcohol Heating; | 70% |
With chloranil; toluene-4-sulfonic acid; xylene |
Conditions | Yield |
---|---|
With mercury dichloride In ethanol for 2h; Heating; | A 38% B 54% |
C22H32O3
canrenone
Conditions | Yield |
---|---|
Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 98 percent / trimethyl orthoformate, p-toluenesulfonic acid / methanol / 3 h / 50 °C 2: H2, triphenylphosphine, rhodium acetate dimer / ethyl acetate / 20 h / 80 °C / 9000.7 Torr 3: 100 percent / N-methylmorpholine N-oxide (NMO), RuCl2(Ph3P)3 / dimethylformamide / 0.17 h 4: 97 percent / 6 N HCl / tetrahydrofuran / 0.5 h 5: 70 percent / p-chloranil / 2-methyl-propan-2-ol / Heating View Scheme |
17α-ethynyl-17β-hydroxy-5-androsten-3-one ethylene ketal
canrenone
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: H2, triphenylphosphine, rhodium acetate dimer / ethyl acetate / 20 h / 80 °C / 9000.7 Torr 2: 100 percent / N-methylmorpholine N-oxide (NMO), RuCl2(Ph3P)3 / dimethylformamide / 0.17 h 3: 97 percent / 6 N HCl / tetrahydrofuran / 0.5 h 4: 70 percent / p-chloranil / 2-methyl-propan-2-ol / Heating View Scheme |
5'-hydroxyspiro-5-en-3-one
canrenone
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 100 percent / N-methylmorpholine N-oxide (NMO), RuCl2(Ph3P)3 / dimethylformamide / 0.17 h 2: 97 percent / 6 N HCl / tetrahydrofuran / 0.5 h 3: 70 percent / p-chloranil / 2-methyl-propan-2-ol / Heating View Scheme |
C24H34O4
canrenone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 97 percent / 6 N HCl / tetrahydrofuran / 0.5 h 2: 70 percent / p-chloranil / 2-methyl-propan-2-ol / Heating View Scheme |
3-(3-oxo-7α-thio-17β-hydroxy-4-androsten-17α-yl)propionic acid γ-lactone
methyl iodide
A
canrenone
B
7-Thiomethylspirolactone
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 20℃; for 2h; |
3-(3-oxo-7α-thio-17β-hydroxy-4-androsten-17α-yl)propionic acid γ-lactone
canrenone
Conditions | Yield |
---|---|
With sodium methylate; methyl iodide In methanol at 20℃; for 1h; |
SPIRONOLACTONE
A
3-(3-oxo-7α-thio-17β-hydroxy-4-androsten-17α-yl)propionic acid γ-lactone
B
canrenone
Conditions | Yield |
---|---|
With sodium hypochlorite; octabromotetrakis(2,6-dichlorophenyl)porphyrin Fe(III)Cl In water; acetonitrile at 80℃; for 0.833333h; Microwave irradiation; | |
With curvularia lunata Microbiological reaction; |
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: potassium hydroxide / tetrahydrofuran / 6.5 h / 15 - 20 °C / Inert atmosphere 2: 5%-palladium/activated carbon; hydrogen / ethanol / 5 h / 20 - 30 °C / Inert atmosphere 3: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium bromide; sodium hypochlorite; tetrabutyl-ammonium chloride / dichloromethane / 6 h / 10 - 15 °C 4: pyridine; sodium acetate; acetic acid; N-Bromosuccinimide / acetone; water / 2 h / -2 - 2 °C 5: lithium carbonate; lithium bromide / N,N-dimethyl-formamide / 3 h / 100 - 105 °C View Scheme |
canrenone
Conditions | Yield |
---|---|
With lithium carbonate; lithium bromide In N,N-dimethyl-formamide at 100 - 105℃; for 3h; | 7.8 g |
17,23-dihydroxy-21,24-dinor-17βH-chol-4-en-20-yn-3-one
canrenone
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 5%-palladium/activated carbon; hydrogen / ethanol / 5 h / 20 - 30 °C / Inert atmosphere 2: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium bromide; sodium hypochlorite; tetrabutyl-ammonium chloride / dichloromethane / 6 h / 10 - 15 °C 3: pyridine; sodium acetate; acetic acid; N-Bromosuccinimide / acetone; water / 2 h / -2 - 2 °C 4: lithium carbonate; lithium bromide / N,N-dimethyl-formamide / 3 h / 100 - 105 °C View Scheme |
17α-(3-hydroxypropyl)-17β-hydroxy-4-androsten-3-one
canrenone
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium bromide; sodium hypochlorite; tetrabutyl-ammonium chloride / dichloromethane / 6 h / 10 - 15 °C 2: pyridine; sodium acetate; acetic acid; N-Bromosuccinimide / acetone; water / 2 h / -2 - 2 °C 3: lithium carbonate; lithium bromide / N,N-dimethyl-formamide / 3 h / 100 - 105 °C View Scheme |
SPIRONOLACTONE
A
3-(17β-hydroxy-3-oxo-1,4,6-androstadien-17α-yl)propionic acid γ-lactone
B
canrenone
Conditions | Yield |
---|---|
With gibberella fujikuroi for 240h; Microbiological reaction; |
SPIRONOLACTONE
A
15α-hydroxycanrenone
E
3-(3-oxo-7α-thio-17β-hydroxy-4-androsten-17α-yl)propionic acid γ-lactone
F
3-(17β-hydroxy-3-oxo-1,4,6-androstadien-17α-yl)propionic acid γ-lactone
G
canrenone
Conditions | Yield |
---|---|
With aspergillus alliaceus Microbiological reaction; |
SPIRONOLACTONE
A
15α-hydroxycanrenone
E
3-(17β-hydroxy-3-oxo-1,4,6-androstadien-17α-yl)propionic acid γ-lactone
F
canrenone
Conditions | Yield |
---|---|
With fusarium lini Microbiological reaction; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: lithium bromide; C30H31Cl3N3(1+)*BF4(1-); triethylamine / 1,2-dichloro-ethane / 5 h / 20 °C / Inert atmosphere; Sealed tube 2: chloranil / 1,2-dichloro-ethane; methanol; water / 1 h / 20 °C View Scheme |
canrenone
Conditions | Yield |
---|---|
With acetic acid In water; toluene at 0 - 100℃; for 24h; pH=7.1; Temperature; pH-value; Autoclave; Inert atmosphere; | 33.1 g |
canrenone
Conditions | Yield |
---|---|
With methanesulfonyl chloride; triethylamine In dichloromethane at 0℃; for 4h; Temperature; Reagent/catalyst; Solvent; Inert atmosphere; | 8.6 g |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: iodine; mercury dichloride; magnesium / diethyl ether / 0.5 h / 40 °C 1.2: 2.5 h / 0 - 20 °C 2.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / 0 °C 2.2: 2 h / 0 - 20 °C 2.3: 1 h / 0 - 20 °C 3.1: Dess-Martin periodane / dichloromethane / 4 h / 0 - 20 °C 4.1: chloranil / tert-butyl alcohol / 3 h / 80 °C View Scheme |
21,24-dinor-3β,17β-dihydroxy-chol-5-en-22-yne
canrenone
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / 0 °C 1.2: 2 h / 0 - 20 °C 1.3: 1 h / 0 - 20 °C 2.1: Dess-Martin periodane / dichloromethane / 4 h / 0 - 20 °C 3.1: chloranil / tert-butyl alcohol / 3 h / 80 °C View Scheme |
3β,17β-Dihydroxy-5-androsten-17α-propanoic Acid γ-Lactone
canrenone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Dess-Martin periodane / dichloromethane / 4 h / 0 - 20 °C 2: chloranil / tert-butyl alcohol / 3 h / 80 °C View Scheme |
canrenone
Conditions | Yield |
---|---|
With chloranil In tert-butyl alcohol at 80℃; for 3h; | 7.9 mg |
formic acid
canrenone
A
C22H27ClO3
B
7α-Chlor-6β-(formyloxy)-17β-hydroxy-3-oxo-4,6-pregnadien-21-carbonsaeure-γ-lacton
Conditions | Yield |
---|---|
With tert-butylhypochlorite for 1h; Ambient temperature; Title compound not separated from byproducts; | A n/a B 91% |
canrenone
4-(t-butyldimethylsilyloxy)-benzyl mercaptan
3-oxo-17α-pregna-4-ene-7α-[4-(t-butyldimethylsilyloxy)-benzylthia]-21,17-carbolactone
Conditions | Yield |
---|---|
With sodium at 45℃; for 0.75h; Addition; | 91% |
canrenone
11α-hydroxyl canrenone
Conditions | Yield |
---|---|
With D-glucose; peptone In water | 90% |
With D-glucose In water for 72h; | 80% |
With D-glucose In water for 72h; | 80% |
N,N-dimethyl(methylene)ammonium chloride
canrenone
Conditions | Yield |
---|---|
In acetonitrile for 24h; Ambient temperature; | 86% |
canrenone
[4-(2-piperidin-1-yl-ethoxy)-phenyl]-methanethiol
Conditions | Yield |
---|---|
With sodium at 45℃; for 1h; Addition; | 82% |
canrenone
Conditions | Yield |
---|---|
With Nocardia farcinica NCAIM (P)-B 001342 9α-hydroxylase; 13-ethyl-10,11α-dihydroxy-4-gonene-3,17-dione In methanol; water; N,N-dimethyl-formamide at 30℃; for 16h; Enzymatic reaction; | 82% |
With dipotassium hydrogenphosphate; D-glucose; sodium chloride In methanol; water at 26℃; for 5 - 48h; Conversion of starting material; | |
With dipotassium hydrogenphosphate; D-glucose; sodium chloride In methanol; water at 26℃; for 5 - 48h; Conversion of starting material; |
Conditions | Yield |
---|---|
Stage #1: tiolacetic acid With trifluoromethylsulfonic anhydride In tetrahydrofuran Stage #2: canrenone In tetrahydrofuran at 20℃; for 1h; | 76% |
With trimethylsilyl trifluoromethanesulfonate In tetrahydrofuran at 20℃; for 3h; | 60% |
In water at 20℃; for 2h; Michael addition; |
Conditions | Yield |
---|---|
With sodium at 60℃; for 24h; Addition; | 74% |
Conditions | Yield |
---|---|
titanium tetrachloride In dichloromethane at -70℃; | A 73% B 15% |
Conditions | Yield |
---|---|
With sodium at 60℃; for 24h; Addition; | 72% |
Conditions | Yield |
---|---|
With pyridine for 24h; Heating; | 70% |
Conditions | Yield |
---|---|
With ethanol; boron trifluoride diethyl etherate In nitromethane at -19℃; for 17h; | A 69.5% B 19.8% |
canrenone
Conditions | Yield |
---|---|
With pyridinium hydrobromide perbromide In acetic acid for 1.5h; Ambient temperature; | 69% |
Conditions | Yield |
---|---|
With piperidine at 10℃; | 69% |
With piperidine In methanol at 20℃; for 20h; |
Conditions | Yield |
---|---|
With trimethylsilyl trifluoromethanesulfonate In tetrahydrofuran for 1h; Ambient temperature; Yields of byproduct given; | A n/a B 64% |
With trimethylsilyl trifluoromethanesulfonate In tetrahydrofuran for 1h; Ambient temperature; Yield given; | A n/a B 64% |
Conditions | Yield |
---|---|
With sodium at 60℃; for 24h; Addition; | 62% |
Conditions | Yield |
---|---|
With sodium at 60℃; for 24h; Addition; | 59% |
Conditions | Yield |
---|---|
With sodium at 60℃; for 24h; Addition; | 59% |
1-hexene
canrenone
A
(+)-7α-hexyl-17-hydroxy-3-oxo-17α-pregn-4-ene-21-carboxylic acid γ-lactone
B
(+)-7β-hexyl-17-hydroxy-3-oxo-17α-pregn-4-ene-21-carboxylic acid γ-lactone
Conditions | Yield |
---|---|
Stage #1: 1-hexene With Schwartz's reagent In dichloromethane at 20℃; for 0.666667h; Inert atmosphere; Schlenk technique; Stage #2: canrenone With chloro-trimethyl-silane; copper(I) trifluoromethanesulfonate benzene In diethyl ether; dichloromethane at 20℃; for 15h; Inert atmosphere; Schlenk technique; diastereoselective reaction; | A 59% B 21% |
Stage #1: 1-hexene With Schwartz's reagent In dichloromethane at 20℃; for 0.666667h; Inert atmosphere; Stage #2: With C36H30CuNO2P(1+)*CF3O3S(1-) In diethyl ether; dichloromethane at 20℃; for 0.166667h; Inert atmosphere; Stage #3: canrenone With chloro-trimethyl-silane In diethyl ether; dichloromethane at 20℃; for 15h; Inert atmosphere; | A 59% B 21% |
canrenone
γ-lactone of 17α-pregna-4,6-diene-3β,17β-diol-20-carboxylic acid
Conditions | Yield |
---|---|
With sodium tetrahydroborate In methanol | 56% |
canrenone
Conditions | Yield |
---|---|
With 2,6-di-tert-butyl-4-methyl-phenol; 3-chloro-benzenecarboperoxoic acid In chloroform for 1.66667h; Heating; | 53% |
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