Conditions | Yield |
---|---|
In hydrogenchloride | 99% |
L-cysteine hydrochloride monohydrate
Conditions | Yield |
---|---|
In water (argon); 70°C, 2 h; elem. anal.; | 96% |
L-cysteine hydrochloride monohydrate
2,4-Dihydroxybenzaldehyde
(4R)-2-(2,4-dihydroxyphenyl)thiazolidine-4-carboxylic acid
Conditions | Yield |
---|---|
With sodium acetate In ethanol; water at 20℃; for 14h; | 95.8% |
Conditions | Yield |
---|---|
In methanol at 50℃; for 100h; | 95% |
Conditions | Yield |
---|---|
In water mixing of the components in double-distd. water and standing at 4°C overnight; sepn. of the ppt., washing with EtOH and dry Et2O and drying (P2O5, vac.); elem. anal.; | 88.4% |
Conditions | Yield |
---|---|
With sodium acetate In tetrahydrofuran; water at 10 - 60℃; for 37h; pH=4 - 5; Inert atmosphere; | 85% |
Conditions | Yield |
---|---|
In water 70°C, 2 h, addn. of EtOH, stirring (20°C, 12 h); elem. anal.; | 82% |
Conditions | Yield |
---|---|
In water 70°C, 2 h, addn. of EtOH, stirring (20°C, 12 h); elem. anal.; | 80% |
L-cysteine hydrochloride monohydrate
Conditions | Yield |
---|---|
In water 70°C, 2 h, addn. of EtOH, stirring (20°C, 12 h); elem. anal.; | 80% |
L-cysteine hydrochloride monohydrate
Conditions | Yield |
---|---|
In water 70°C, 2 h, addn. of EtOH, stirring (20°C, 12 h); elem. anal.; | 80% |
L-cysteine hydrochloride monohydrate
Conditions | Yield |
---|---|
In water 70°C, 2 h, addn. of EtOH, stirring (20°C, 12 h); elem. anal.; | 80% |
Conditions | Yield |
---|---|
With hydrogenchloride In methanol; water | A n/a B 74.8% |
2,4-dihydroxybenzonitrile
L-cysteine hydrochloride monohydrate
C10H9NO4S
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In methanol | 69% |
ammonium tetrathiotungstate
L-cysteine hydrochloride monohydrate
Conditions | Yield |
---|---|
With HCl; KOH In water dropwise addn. of concd. HCl to aq. W compd. soln. with stirring; addn. of L-cysteine; stirring, several min; adjusting to pH 7 (KOH); heating at 50-60°C, 30 min; addn. of KCl; cooling to room temp.; storage in refrigerator overnight; crystn.; filtration; washing (methanol); recrystn. by dissoln. in hot water; filtration; addn. of KCl; allowing to stand overnight in a refrigerato; crystn.; elem. anal.; | 50% |
water
L-cysteine hydrochloride monohydrate
2-chloro-3-(1H-imidazol-4-yl)propanoic acid
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol for 72h; Inert atmosphere; | 50% |
ammonium tetrathiotungstate
L-cysteine hydrochloride monohydrate
Conditions | Yield |
---|---|
With NH4Cl; HCl; NH3 In water dropwise addn. of HCl to aq. W compd. soln. with stirring; addn. of cysteine; stirring, several min; adjusting pH to 7 (NH3); heating, 50-60°C, 30 min; addn. of NH4Cl; cooling to room temp.; storage in refrigerator overnight; crystn.; filtration; washing (methanol); recrystn.; elem. anal.; | 46% |
4-nitrobenzyl chloride
L-cysteine hydrochloride monohydrate
B
L-2-amino-3-(4-nitrobenzylthio)propionic acid
Conditions | Yield |
---|---|
With hydrogenchloride; sodium hydroxide | A n/a B 45.9% |
ammonium tetrathiotungstate
L-cysteine hydrochloride monohydrate
Conditions | Yield |
---|---|
With NaCl; HCl In water dropwise addn. of HCl to aq. W compd. soln. with stirring; addn. of cysteine; stirring, several min; adjusting pH to 7 (NaOH); heating, 50-60°C, 30 min; addn. of NaCl; cooling to room temp.; storage in refrigerator overnight; crystn.; filtration; washing (methanol); recrystn.; elem. anal.; | 40% |
Conditions | Yield |
---|---|
In water stirred at room temp. for 5 min, heated at 55°C for 2 h (stirring), kept for 2 h at 20°C; filtered, standed for 2 d at 15-20°C, crysts. filtered, washed (cold water), dried (room temp.); elem. anal., TGA; | 37% |
ammonium tetrathiotungstate
L-cysteine hydrochloride monohydrate
Conditions | Yield |
---|---|
With HCl; KOH; KCl In water concd. HCl is added to aq. soln. of W-compd., cysteine compd. is added, pH is adjusted to 7 (KOH), soln. is heated for 20 min, cooled to room temp. and filtered, KCl is added to the filtrate; soln. is kept in refrigerator overnight, crystals are filtered off, washed with MeOH and Et2O and recrystd. from hot H2O, elem. anal.; | 35% |
sodium tungstate (VI) dihydrate
L-cysteine hydrochloride monohydrate
Conditions | Yield |
---|---|
With HCl; KOH In water slow addn. of concd. HCl to aq. soln. of Na2WO4 and Na2S; addn. of L-cysteine; adjusting to pH 7 (KOH); heating at 50-70°C, 20 min; filtration; addn. of KCl; filtration; washing (methanol); recrystn. by dissoln. in hot water; filtration; addn. of KCl; allowing to stand overnight in a refrigerato; crystn.; elem. anal.; | 35% |
L-cysteine hydrochloride monohydrate
Conditions | Yield |
---|---|
In water slow addn. of freshly prepd. NaHSe in H2O to aq. soln. of (NH4)6(Mo7O24)*6H2O; stirring for 24 h; filtering, addn. of HO2CCH(NH2)CH2SH in H2O (pH adjusted to 6 with NaOH); standing for 24 h at room temp., refiltering;; pptn. on addn. of CsCl in H2O; recrystn. from hot H2O; elem. anal.;; | 33.7% |
L-cysteine hydrochloride monohydrate
Conditions | Yield |
---|---|
With AcONH4 In methanol; water slow addn. of aq. cysteine to Tc-complex (in MeOH), pH-adjustment to 7.4(AcONH4), chromy. (celulose, MeOH; then Sephadex LH-20), concn., BaCl2 addn. (pptn.); recrystn. (50% aq. MeOH); elem. anal.; | 33% |
L-cysteine hydrochloride monohydrate
2-Bromoacetyl bromide
(R)-5-oxothiomorpholine-3-carboxylic acid
Conditions | Yield |
---|---|
With sodium carbonate In water for 12h; Ambient temperature; | 15% |
L-cysteine hydrochloride monohydrate
S-guanylsulfanyl-L-cysteine
L-Cysteine hydrochloride monohydratewhite is crystals or crystalline powder with strongly acid taste. L-Cysteine hydrochloride monohydratewhite is very soluble in water.
appearance: white solid.
formula: C3H7NO2S.HCl.H2O.
molecular weight: 175.64 g/mol.
melting point: 176°C.
solubility: soluble in cold water.
L-Cysteine Hydrochloride Monohydrate is widely used in fields of medicine, food processing, biological study, materials of chemical industry and so on.
It's used as raw materials for manufacturing N-Acetyl-L-Cysteine, S-Carboxymethyl
-L-Cysteine and L-Cysteine base etc.
Besides, it is useful to cure liver disease, antioxidant and antidote.
In addition, it is used in cosmetic.
ORAL (LD50): Acute: 3550 mg/kg [Mouse]. 5580 mg/kg[Rat]. 4200 mg/kg [Mouse].
It is very hazardous in case of skin and eye contact, of ingestion, of inhalation.
Repeated or prolonged inhalation of it may lead to chronic respiratory irritation.
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