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Cas:10193-99-4
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inquiryPentaerythritol
mercaptoacetic acid
3-[(sulfanylacetyl)oxy]-2,2-bis{[(sulfanylacetyl)oxy]methyl}propyl sulfanylacetate
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene Heating; | 52% |
With toluene-4-sulfonic acid In toluene at 110 - 120℃; for 4h; | |
With toluene-4-sulfonic acid In toluene at 130℃; for 9h; Dean-Stark; Inert atmosphere; | 76 %Chromat. |
Pentaerythritol
Dipentaerythritol
mercaptoacetic acid
3-[(sulfanylacetyl)oxy]-2,2-bis{[(sulfanylacetyl)oxy]methyl}propyl sulfanylacetate
Conditions | Yield |
---|---|
toluene-4-sulfonic acid In water; toluene at 104 - 121℃; for 5h; Product distribution / selectivity; Heating / reflux; |
Pentaerythritol
mercaptoacetic acid
A
pentaerythritol tris(thioglycolate)
B
3-[(sulfanylacetyl)oxy]-2,2-bis{[(sulfanylacetyl)oxy]methyl}propyl sulfanylacetate
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene at 130℃; for 9h; Dean-Stark; Inert atmosphere; | A 79 %Chromat. B 20 %Chromat. |
3-[(sulfanylacetyl)oxy]-2,2-bis{[(sulfanylacetyl)oxy]methyl}propyl sulfanylacetate
di(n-butyl)tin oxide
Conditions | Yield |
---|---|
In toluene at 110℃; for 29h; Dean-Stark; | 96% |
3-[(sulfanylacetyl)oxy]-2,2-bis{[(sulfanylacetyl)oxy]methyl}propyl sulfanylacetate
pentaerythritol tetracetate
Conditions | Yield |
---|---|
With di-tert-butyl peroxide; triethyl phosphite In acetonitrile at 20℃; UV-irradiation; | 94% |
With di-tert-butyl peroxide; triethyl phosphite In acetonitrile at 25℃; for 6h; Irradiation; | 94% |
3-[(sulfanylacetyl)oxy]-2,2-bis{[(sulfanylacetyl)oxy]methyl}propyl sulfanylacetate
Conditions | Yield |
---|---|
With di-tert-butyl peroxide; water-d2; ethydiphenylphosphine oxide In dichloromethane at 20℃; for 10h; Solvent; Irradiation; Green chemistry; | 94% |
4-(diphenylamino)benzaldehyde N-2,3-epoxypropyl-N-phenylhydrazone
3-[(sulfanylacetyl)oxy]-2,2-bis{[(sulfanylacetyl)oxy]methyl}propyl sulfanylacetate
Conditions | Yield |
---|---|
triethylamine In tetrahydrofuran for 12h; Heating / reflux; | 73% |
C20H19NO4
3-[(sulfanylacetyl)oxy]-2,2-bis{[(sulfanylacetyl)oxy]methyl}propyl sulfanylacetate
C93H96N4O24S4
Conditions | Yield |
---|---|
tributyl-amine In dichloromethane at 20℃; for 72h; | 72% |
MoCl(CO)2(1,10-phenanthroline)(η(3)-CH2C(COCl)C=CH2)
dichloromethane
3-[(sulfanylacetyl)oxy]-2,2-bis{[(sulfanylacetyl)oxy]methyl}propyl sulfanylacetate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane (N2); addn. of amine to a soln. of molybdenum complex in CH2Cl2, addn. of a soln. of thiol in CH2Cl2, stirring for 3 h; filtration, washing with cold CH2Cl2, recrystn. (CH2Cl2/petrol); elem. anal.; | 46% |
3-[(sulfanylacetyl)oxy]-2,2-bis{[(sulfanylacetyl)oxy]methyl}propyl sulfanylacetate
1-chloroacetophenone
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 18h; | 45% |
3-[(sulfanylacetyl)oxy]-2,2-bis{[(sulfanylacetyl)oxy]methyl}propyl sulfanylacetate
propargyl alcohol methyl ether
Conditions | Yield |
---|---|
With tripropylborane In methanol; hexane; benzene at 20℃; | 42% |
3-[(sulfanylacetyl)oxy]-2,2-bis{[(sulfanylacetyl)oxy]methyl}propyl sulfanylacetate
hex-1-yne
Conditions | Yield |
---|---|
With tripropylborane In methanol; hexane; benzene at 20℃; | 25% |
3-[(sulfanylacetyl)oxy]-2,2-bis{[(sulfanylacetyl)oxy]methyl}propyl sulfanylacetate
Conditions | Yield |
---|---|
at 20℃; for 336h; Michael Addition; | 23% |
3-[(sulfanylacetyl)oxy]-2,2-bis{[(sulfanylacetyl)oxy]methyl}propyl sulfanylacetate
1,3-Phenylene diisocyanate
Conditions | Yield |
---|---|
With Zerec UN (acidic phosphate ester); BioSorb 583 (UV absorber); dibutyltin chloride at 10 - 120℃; for 18h; Product distribution / selectivity; Heating / reflux; |
C10H10ClNO5S
3-[(sulfanylacetyl)oxy]-2,2-bis{[(sulfanylacetyl)oxy]methyl}propyl sulfanylacetate
C53H56N4O28S8
Conditions | Yield |
---|---|
With triethylamine In 1,2-dimethoxyethane; tert-butyl methyl ether at 0℃; for 3h; |
3-[(sulfanylacetyl)oxy]-2,2-bis{[(sulfanylacetyl)oxy]methyl}propyl sulfanylacetate
(E)-1-((1RS,2SR)-2,6,6-trimethylcyclohex-3-enyl)but-2-en-1-one
Conditions | Yield |
---|---|
at 20℃; for 336h; |
3-[(sulfanylacetyl)oxy]-2,2-bis{[(sulfanylacetyl)oxy]methyl}propyl sulfanylacetate
(E)-1-((1RS,2SR)-2,6,6-trimethylcyclohex-3-enyl)but-2-en-1-one
Conditions | Yield |
---|---|
at 20℃; for 192h; |
3-[(sulfanylacetyl)oxy]-2,2-bis{[(sulfanylacetyl)oxy]methyl}propyl sulfanylacetate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: toluene / 29 h / 110 °C / Dean-Stark 2: [2,2]bipyridinyl / chloroform / Reflux View Scheme |
3-[(sulfanylacetyl)oxy]-2,2-bis{[(sulfanylacetyl)oxy]methyl}propyl sulfanylacetate
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide |
3-[(sulfanylacetyl)oxy]-2,2-bis{[(sulfanylacetyl)oxy]methyl}propyl sulfanylacetate
Conditions | Yield |
---|---|
With triethylamine In ethyl acetate at 50℃; for 10h; Temperature; |
hexamethylene glycol diacrylate
3-[(sulfanylacetyl)oxy]-2,2-bis{[(sulfanylacetyl)oxy]methyl}propyl sulfanylacetate
Conditions | Yield |
---|---|
With triethylamine In ethyl acetate at 50℃; for 10h; Temperature; |
3-[(sulfanylacetyl)oxy]-2,2-bis{[(sulfanylacetyl)oxy]methyl}propyl sulfanylacetate
2-((acryloyloxy)methyl)-2-ethylpropane-1,3-diyl diacrylate
Conditions | Yield |
---|---|
With triethylamine In ethyl acetate at 50℃; for 10h; Temperature; Michael Addition; Green chemistry; |
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