Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:10378-01-5
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:10378-01-5
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inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for the fine chemicals, ph
CIS-9-HEXADECENOL CAS:10378-01-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interm
Cas:10378-01-5
Min.Order:1 Gram
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:10378-01-5
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:10378-01-5
Min.Order:10 Gram
FOB Price: $100.0
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inquiryHangzhou Fandachem Co.,Ltd, a China-based chemical company, specialize in exporting Palmitoleyl alcohol , CAS NO: 10378-01-5 Please contact us by email freely. We are leading exporter in China. If you really need this cargo, plea
Cas:10378-01-5
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inquiryHigh quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:Beijing or Guangzhou
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen
HANGZHOU TIANYE CHEMICALS Co.LTD , Located in Eastern Science and Innovation Park Hangzhou .We are a high-tech enterprise specialized in technical research and development, production, development and trade of chemical products. We supply Multiple so
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Betterbiochem is specialized in APIs, pharmaceutical intermediates & fine chemicals. 1. The best quality, competitive price. 2. The best service before or after shipment. 3. Rich experience in export operation. 4. Rich experience in
HuBei ipure is a diversified product production and operation enterprise, with API, pharma intermediates, and other fine chemicals as well as R&D and pigments development and sales as one of the large enterprises, with more than 130 acres of pl
Cas:10378-01-5
Min.Order:1 Gram
FOB Price: $1.0 / 2.0
Type:Trading Company
inquiryU-CHEMO Holding Co.,Limited is a very fast developing high-technology enterprise combining with manufacture and sales.U-CHEMO supply high quality products and excellent service to our customers.We make the insect pheromones, censor in the quality con
United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat
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inquiryJoyinchem have been committed to chemical supply for several years and have built good cooperation records with multinational chemical corporations and importers from all over the world. Our services include:-Spot goods-Contract manufacturing-Custom
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inquiryShanghai, Run-Biotech Co., Ltd is a leading domestic pharmaceutical, biopharmaceutical, and health care products R & D outsourcing services company. As an innovation-driven and customer-focused company, Run Biotech provides a broad and integrated por
9-Hexadecen-1-ol, (9Z)- Storage:keep in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/pharma intermediate Transportation:By Sea,by Air,By courier like DHL or Fedx. Port:Shanghai/Shenzhen
Good QualityCompetitive priceFirst-class service Application:pesticide
High quality, Competitive price & Excellent service Application:Chemical,Organic Intermediates
Cas:10378-01-5
Min.Order:0 Metric Ton
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Type:Lab/Research institutions
inquirycis-9-hexadecenoic acid
palmitoleyl alcohol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; Reflux; | 98% |
With lithium aluminium tetrahydride In diethyl ether at 20℃; for 24h; | 97% |
Multi-step reaction with 2 steps 1: 0.19 g / conc. H2SO4 / 6 h / Heating 2: 0.14 g / LiAlH4 / tetrahydrofuran / 24 h / Ambient temperature View Scheme |
9-hexadecyn-1-ol
palmitoleyl alcohol
Conditions | Yield |
---|---|
With hydrogen; ethylendiamine poisoned P-2 Ni In ethanol | 97% |
With hydrogen; Ni-P2 | 88% |
With bis(cyclopentadienyl)titanium dichloride; di-iso-butylmagnesium; ammonium chloride 1.) Et2O, 20 deg C, 30 min, 2.) H2O; Yield given. Multistep reaction; |
(Z)-9-hexadecenoic acid methyl ester
palmitoleyl alcohol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran at -10 - 20℃; for 5h; | 96% |
With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; for 2h; | 92% |
With lithium aluminium tetrahydride In tetrahydrofuran for 24h; Ambient temperature; | 0.14 g |
With lithium aluminium tetrahydride In diethyl ether for 2h; Reflux; | 2.3 g |
9-tetradecyn-1-ol
palmitoleyl alcohol
Conditions | Yield |
---|---|
With hydrogen; P2Ni | 86% |
(Z)-hexadec-9-en-1-yl acetate
palmitoleyl alcohol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In diethyl ether at 20℃; for 5h; | 82% |
With sodium hydroxide In methanol |
palmitoleyl alcohol
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran at 0 - 20℃; for 3h; | 82% |
heptanal
(9-hydroxynonyl)(triphenyl)phosphonium bromide
A
trans-hexadec-9-en-1-ol
B
palmitoleyl alcohol
Conditions | Yield |
---|---|
With sodium hydride; dimethyl sulfoxide In tetrahydrofuran for 0.5h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; |
palmitoleyl alcohol
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In methanol; water at 20℃; for 15h; Yield given; |
2-[((Z)-Hexadec-9-enyl)oxy]-tetrahydro-pyran
palmitoleyl alcohol
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In methanol for 3h; Heating; Yield given; | |
With toluene-4-sulfonic acid In methanol at 20℃; for 16h; |
(Z)-4-undecene-1-ol
palmitoleyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 96 percent / triphenylphosphine, Br2 / CCl4 / 16 h / Ambient temperature 2: 1.) cuprous iodide, 2,2' bipyridyl / 1.) THF, 2 deg C, 10 min, 2.) THF, a) 2 deg C, 2 h, b) RT, 15 h 3: p-toluenesulfonic acid / methanol; H2O / 15 h / 20 °C View Scheme | |
Multi-step reaction with 3 steps 1: 82 percent / PBr3, pyridine / diethyl ether / 1) rt, overnight, 2) reflux, 2 h 2: 1) Mg / 3) Li2CuCl4 / 1) THF, 2) THF, -10 deg C, 30 min, 3) a) 0 to -10 deg C, 6 h, b) rt, overnight 3: p-toluenesulphonic acid / methanol / 3 h / Heating View Scheme |
(Z)-4-undecenal
palmitoleyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 95 percent / diisobutylaluminum hydride / diethyl ether; toluene / 1.5 h / -10 °C 2: 96 percent / triphenylphosphine, Br2 / CCl4 / 16 h / Ambient temperature 3: 1.) cuprous iodide, 2,2' bipyridyl / 1.) THF, 2 deg C, 10 min, 2.) THF, a) 2 deg C, 2 h, b) RT, 15 h 4: p-toluenesulfonic acid / methanol; H2O / 15 h / 20 °C View Scheme |
(Z)-4-undecenyl bromide
palmitoleyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) cuprous iodide, 2,2' bipyridyl / 1.) THF, 2 deg C, 10 min, 2.) THF, a) 2 deg C, 2 h, b) RT, 15 h 2: p-toluenesulfonic acid / methanol; H2O / 15 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: 1) Mg / 3) Li2CuCl4 / 1) THF, 2) THF, -10 deg C, 30 min, 3) a) 0 to -10 deg C, 6 h, b) rt, overnight 2: p-toluenesulphonic acid / methanol / 3 h / Heating View Scheme |
1,1-dimethoxy-8-tosyloxy-(4Z)-octene
palmitoleyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: 63 percent / dilithium tetrachlorocuprate / tetrahydrofuran / 1.) -78 deg C, 2 h, 2.) RT, 15 h 2: 99 percent / 5percent HCl / acetone / 6 h / Ambient temperature 3: 95 percent / diisobutylaluminum hydride / diethyl ether; toluene / 1.5 h / -10 °C 4: 96 percent / triphenylphosphine, Br2 / CCl4 / 16 h / Ambient temperature 5: 1.) cuprous iodide, 2,2' bipyridyl / 1.) THF, 2 deg C, 10 min, 2.) THF, a) 2 deg C, 2 h, b) RT, 15 h 6: p-toluenesulfonic acid / methanol; H2O / 15 h / 20 °C View Scheme |
1,1-dimethoxy-(4Z)-undecene
palmitoleyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 99 percent / 5percent HCl / acetone / 6 h / Ambient temperature 2: 95 percent / diisobutylaluminum hydride / diethyl ether; toluene / 1.5 h / -10 °C 3: 96 percent / triphenylphosphine, Br2 / CCl4 / 16 h / Ambient temperature 4: 1.) cuprous iodide, 2,2' bipyridyl / 1.) THF, 2 deg C, 10 min, 2.) THF, a) 2 deg C, 2 h, b) RT, 15 h 5: p-toluenesulfonic acid / methanol; H2O / 15 h / 20 °C View Scheme |
palmitoleyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: 60.91 percent / aq. NaIO4 / acetonitrile / 0.5 h / 5 °C 2.1: sodium amide / tetrahydrofuran; hexamethylphosphoric acid triamide / 1.5 h / 20 °C 2.2: 91.52 percent / tetrahydrofuran; hexamethylphosphoric acid triamide / -73 - 20 °C 3.1: 92 percent / lithium aluminum hydride / tetrahydrofuran / 2 h / 0 °C View Scheme |
methyl ester of azelaic acid aldehyde
palmitoleyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium amide / tetrahydrofuran; hexamethylphosphoric acid triamide / 1.5 h / 20 °C 1.2: 91.52 percent / tetrahydrofuran; hexamethylphosphoric acid triamide / -73 - 20 °C 2.1: 92 percent / lithium aluminum hydride / tetrahydrofuran / 2 h / 0 °C View Scheme | |
Multi-step reaction with 2 steps 1: 1.) NaNH2 / 1.) THF, RT, 1 h, 2.) THF, from -10 deg C to RT 2: 96 percent / LAH / tetrahydrofuran / 5 h / -10 - 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: potassium carbonate / toluene / 4 h / Reflux 2: lithium aluminium tetrahydride / diethyl ether / 2 h / Reflux View Scheme |
triphenylheptylphosphonium bromide
palmitoleyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium amide / tetrahydrofuran; hexamethylphosphoric acid triamide / 1.5 h / 20 °C 1.2: 91.52 percent / tetrahydrofuran; hexamethylphosphoric acid triamide / -73 - 20 °C 2.1: 92 percent / lithium aluminum hydride / tetrahydrofuran / 2 h / 0 °C View Scheme | |
Multi-step reaction with 2 steps 1: 1.) sodium bis(trimethylsilyl)amide / 1.) THF, from 50 to 55 deg C, 60 min, 2.) THF, a) -78 deg C, 30 min, b) 20 deg C, 12 h 2: 82 percent / LiAlH4 / diethyl ether / 5 h / 20 °C View Scheme |
palmitoleyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: 97.95 percent / aq. H2SO4 / 0.11 h / microwave irradiation 2.1: 60.91 percent / aq. NaIO4 / acetonitrile / 0.5 h / 5 °C 3.1: sodium amide / tetrahydrofuran; hexamethylphosphoric acid triamide / 1.5 h / 20 °C 3.2: 91.52 percent / tetrahydrofuran; hexamethylphosphoric acid triamide / -73 - 20 °C 4.1: 92 percent / lithium aluminum hydride / tetrahydrofuran / 2 h / 0 °C View Scheme |
8-Bromo-1-octene
palmitoleyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 87 percent / NH3 2: 1) 9-BBN, 2) H2O2, AcONa 3: 88 percent / H2 / Ni-P2 View Scheme |
1-octynyllithium
palmitoleyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 87 percent / NH3 2: 1) 9-BBN, 2) H2O2, AcONa 3: 88 percent / H2 / Ni-P2 View Scheme |
hexadec-1-en-9-yne
palmitoleyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1) 9-BBN, 2) H2O2, AcONa 2: 88 percent / H2 / Ni-P2 View Scheme |
10,11-dibromo-undecanoic acid
palmitoleyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: KOH, PEG 400 / 0.5 h / 150 - 200 °C 2: p-TSA / 12 h / Ambient temperature 3: 96 percent / H2, quinoline / 5percent Pd/BaSO4 / hexane / Ambient temperature 4: 84 percent / O3 / CH2Cl2 / -78 °C 5: 1.) NaNH2 / 1.) THF, RT, 1 h, 2.) THF, from -10 deg C to RT 6: 96 percent / LAH / tetrahydrofuran / 5 h / -10 - 20 °C View Scheme |
10-undecenoic acid
palmitoleyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1: 97 percent / Br2 / CCl4 / 1.5 h 2: KOH, PEG 400 / 0.5 h / 150 - 200 °C 3: p-TSA / 12 h / Ambient temperature 4: 96 percent / H2, quinoline / 5percent Pd/BaSO4 / hexane / Ambient temperature 5: 84 percent / O3 / CH2Cl2 / -78 °C 6: 1.) NaNH2 / 1.) THF, RT, 1 h, 2.) THF, from -10 deg C to RT 7: 96 percent / LAH / tetrahydrofuran / 5 h / -10 - 20 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: p-TSA / 12 h / Ambient temperature 2: 96 percent / H2, quinoline / 5percent Pd/BaSO4 / hexane / Ambient temperature 3: 84 percent / O3 / CH2Cl2 / -78 °C 4: 1.) NaNH2 / 1.) THF, RT, 1 h, 2.) THF, from -10 deg C to RT 5: 96 percent / LAH / tetrahydrofuran / 5 h / -10 - 20 °C View Scheme |
9-undecynoic acid methyl ester
palmitoleyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 96 percent / H2, quinoline / 5percent Pd/BaSO4 / hexane / Ambient temperature 2: 84 percent / O3 / CH2Cl2 / -78 °C 3: 1.) NaNH2 / 1.) THF, RT, 1 h, 2.) THF, from -10 deg C to RT 4: 96 percent / LAH / tetrahydrofuran / 5 h / -10 - 20 °C View Scheme |
(Z)-0-undecenoic acid methyl ester
palmitoleyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 84 percent / O3 / CH2Cl2 / -78 °C 2: 1.) NaNH2 / 1.) THF, RT, 1 h, 2.) THF, from -10 deg C to RT 3: 96 percent / LAH / tetrahydrofuran / 5 h / -10 - 20 °C View Scheme |
2-(8-bromooctyloxy)tetrahydropyran
palmitoleyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 1.) LiNH2, HMPTA / 1.) RT, 1 h, 2.) a) 10 deg C, 1 h, b) RT, 15 h, c) 55 deg C, 10 h 2: 85 percent / p-TsOH / methanol; H2O / 18 h / 20 °C 3: 1.) iso-BuMgBr, 2.) Cp2TiCl2 / 1.) diethyl ether, 0 deg C, 15 min, 2.) diethyl ether, RT, 3 h View Scheme | |
Multi-step reaction with 3 steps 1.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -30 - 0 °C / Inert atmosphere 1.2: 16 h / Reflux 2.1: potassium hydroxide; palladium diacetate / N,N-dimethyl-formamide / 16 h / 145 °C / Sealed tube 3.1: toluene-4-sulfonic acid / methanol / 16 h / 20 °C View Scheme |
1,8-Octanediol
palmitoleyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 75 percent / 48percent HBr / Heating 2: 99 percent / p-toluenesulfonic acid 3: 1.) LiNH2, HMPTA / 1.) RT, 1 h, 2.) a) 10 deg C, 1 h, b) RT, 15 h, c) 55 deg C, 10 h 4: 85 percent / p-TsOH / methanol; H2O / 18 h / 20 °C 5: 1.) iso-BuMgBr, 2.) Cp2TiCl2 / 1.) diethyl ether, 0 deg C, 15 min, 2.) diethyl ether, RT, 3 h View Scheme |
8-bromooctanol
palmitoleyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 99 percent / p-toluenesulfonic acid 2: 1.) LiNH2, HMPTA / 1.) RT, 1 h, 2.) a) 10 deg C, 1 h, b) RT, 15 h, c) 55 deg C, 10 h 3: 85 percent / p-TsOH / methanol; H2O / 18 h / 20 °C 4: 1.) iso-BuMgBr, 2.) Cp2TiCl2 / 1.) diethyl ether, 0 deg C, 15 min, 2.) diethyl ether, RT, 3 h View Scheme | |
Multi-step reaction with 4 steps 1.1: toluene-4-sulfonic acid / dichloromethane / 16.5 h / 0 - 20 °C 2.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -30 - 0 °C / Inert atmosphere 2.2: 16 h / Reflux 3.1: potassium hydroxide; palladium diacetate / N,N-dimethyl-formamide / 16 h / 145 °C / Sealed tube 4.1: toluene-4-sulfonic acid / methanol / 16 h / 20 °C View Scheme |
1-tetrahydropyranyloxy-n-9-hexadecyn
palmitoleyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 85 percent / p-TsOH / methanol; H2O / 18 h / 20 °C 2: 1.) iso-BuMgBr, 2.) Cp2TiCl2 / 1.) diethyl ether, 0 deg C, 15 min, 2.) diethyl ether, RT, 3 h View Scheme | |
Multi-step reaction with 2 steps 1: potassium hydroxide; palladium diacetate / N,N-dimethyl-formamide / 16 h / 145 °C / Sealed tube 2: toluene-4-sulfonic acid / methanol / 16 h / 20 °C View Scheme |
palmitoleyl alcohol
(Z)-9-hexadecenal
Conditions | Yield |
---|---|
With pyridinium chlorochromate In dichloromethane at 20℃; for 2h; | 98% |
With pyridinium chlorochromate In dichloromethane for 1.5h; Ambient temperature; | 94% |
With pyridinium chlorochromate | 94% |
palmitoleyl alcohol
(Z)-hexadec-9-enyl bromide
Conditions | Yield |
---|---|
With bromine; triphenylphosphine In benzene at 20℃; for 3h; | 97% |
With carbon tetrabromide; triphenylphosphine In dichloromethane for 16h; Ambient temperature; | 94% |
With carbon tetrabromide; triphenylphosphine In dichloromethane at 20℃; for 16h; | 94% |
palmitoleyl alcohol
Conditions | Yield |
---|---|
With 1H-imidazole; iodine; triphenylphosphine In toluene at 20℃; for 3h; | 89% |
Conditions | Yield |
---|---|
With pyridine for 1h; Ambient temperature; | 85% |
With pyridine for 24h; Ambient temperature; | 68% |
With pyridine for 25h; Ambient temperature; | 0.1 g |
In pyridine at 20℃; for 24h; | 1.4 g |
cholesteryl p-toluenesulfonate
palmitoleyl alcohol
cholesteryl cis-9'-hexadecenyl ether
Conditions | Yield |
---|---|
at 110℃; for 2.5h; | 54.1% |
palmitoleyl alcohol
methanesulfonyl chloride
palmitoleyl methanesulfonate
Conditions | Yield |
---|---|
With pyridine | |
With pyridine at 0 - 20℃; for 24h; |
methanol
palmitoleyl alcohol
Conditions | Yield |
---|---|
With sodium tetrahydroborate; mercury(II) diacetate 1.) 48 h, RT; 2.) glacial acetic acid; Multistep reaction; |
palmitoleyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: 97 percent / PPh3; Br2 / benzene / 3 h / 20 °C 2.1: Mg / tetrahydrofuran / 4 h / Heating 2.2: 12 mg / NaH / diethyl ether / 1.5 h / 0 - 20 °C View Scheme |
palmitoleyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: 97 percent / PPh3; Br2 / benzene / 3 h / 20 °C 2.1: Mg / tetrahydrofuran / 4 h / Heating 2.2: 0.920 g / NaH / diethyl ether / 1.5 h / 0 - 20 °C View Scheme |
palmitoleyl alcohol
(3S,8aR)-5-Bromo-8a-((Z)-heptadec-10-enyl)-3-methyl-8aH-benzo[1,4]dioxine-2,6-dione
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: 97 percent / PPh3; Br2 / benzene / 3 h / 20 °C 2.1: Mg / tetrahydrofuran / 4 h / Heating 2.2: 0.920 g / NaH / diethyl ether / 1.5 h / 0 - 20 °C 3.1: 92 percent / K2CO3 / dimethylformamide / 6 h / 20 °C 4.1: 93 percent / ZnBr; CH3NO2 / 20 °C 5.1: 55 percent / PhIOTMS(OTf); TMSOTf / CH2Cl2 / 0.25 h / 0 °C View Scheme |
palmitoleyl alcohol
2-(2-bromo-6-heptadec-10-enyl-3-hydroxy-phenoxy)-N-methoxy-N-methyl-propionamide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: 97 percent / PPh3; Br2 / benzene / 3 h / 20 °C 2.1: Mg / tetrahydrofuran / 4 h / Heating 2.2: 0.920 g / NaH / diethyl ether / 1.5 h / 0 - 20 °C 3.1: 92 percent / K2CO3 / dimethylformamide / 6 h / 20 °C 4.1: 93 percent / ZnBr; CH3NO2 / 20 °C View Scheme |
palmitoleyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: 97 percent / PPh3; Br2 / benzene / 3 h / 20 °C 2.1: Mg / tetrahydrofuran / 4 h / Heating 2.2: 0.920 g / NaH / diethyl ether / 1.5 h / 0 - 20 °C 3.1: 92 percent / K2CO3 / dimethylformamide / 6 h / 20 °C View Scheme |
palmitoleyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: 97 percent / PPh3; Br2 / benzene / 3 h / 20 °C 2.1: Mg / tetrahydrofuran / 4 h / Heating 2.2: 12 mg / NaH / diethyl ether / 1.5 h / 0 - 20 °C 3.1: 90 percent / HCl / dioxane / 1.25 h / 80 °C View Scheme |
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