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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

4'-FLUORO-[1,1'-BIPHENYL]-4-CARBONITRILE

Cas:10540-31-5

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Pharmaceutical Grade CAS 10540-31-5 with competitive price

Cas:10540-31-5

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

4-(4-Fluorophenyl)benzonitrile

Cas:10540-31-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

[1,1'-Biphenyl]-4-carbonitrile,4'-fluoro-

Cas:10540-31-5

Min.Order:10 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou

4'-Fluoro-[1,1'-biphenyl]-4-carbonitrile

Cas:10540-31-5

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

4-(4-Fluorophenyl)benzonitrile

Cas:10540-31-5

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Antimex Chemical Limied

factory?direct?sale Application:healing drugs

[1,1'-Biphenyl]-4-carbonitrile,4'-fluoro-

Cas:10540-31-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

SAGECHEM LIMITED

10540-31-5 Application:intermediate

4'-fluorobiphenyl-4-carbonitrile

Cas:10540-31-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Chemlyte Solutions

factory?direct?sale Application:Fine chemical intermediates, used as the main raw material for the synthesis of various pesticides, medicines, surfactants, polymer monomers, and antifungal agents

[1,1'-Biphenyl]-4-carbonitrile,4'-fluoro-

Cas:10540-31-5

Min.Order:0

Negotiable

Type:Other

inquiry

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

4-(4-Fluorophenyl)benzonitrile

Cas:10540-31-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

4-(4-Fluorophenyl)benzonitrile

Cas:10540-31-5

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

inquiry

HENAN SUNLAKE ENTERPRISE CORPORATION

Exhibition in shanghai Our Laboratoy Our factory Package & Shipment Appearance: Colorless to light yellow liqui Storage:2-8, cold storage, to

4-(4-Fluorophenyl)benzonitrile

Cas:10540-31-5

Min.Order:100 Gram

Negotiable

Type:Trading Company

inquiry

Chemical Technology Co.,LTD

1. Production capacity: we have three production base with high-tech production equipment and instruments, equipped with professional production personnel, meet your requirements.2. Quality assurance: we have a first-class testing equipment and testi

4-(4-Fluorophenyl)benzonitrile

Cas:10540-31-5

Min.Order:0

Negotiable

Type:Other

inquiry

Capot Chemical Co., Ltd.

At Capot,We can synthesize and purify your complex molecules from 100 gram to 10 tons.Appearance:Clear colorless to light yellow liquid Storage:Dry,Seal and Cool place Package:1G,5G,10G,25G,100G,250G,500G,1KG,5KG,10KG,25KG,50KG,100KG,150KG,200KG. App

4-(4-Fluorophenyl)benzonitrile

Cas:10540-31-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Finetech Industry Limited

FINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the 4-(4-Fluorophenyl)benzonitrile, CAS:10540-31-5 with the most competitive price and th

4-(4-Fluorophenyl)benzonitrile

Cas:10540-31-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shanghai Run-Biotech Co., Ltd.

Shanghai, Run-Biotech Co., Ltd is a leading domestic pharmaceutical, biopharmaceutical, and health care products R & D outsourcing services company. As an innovation-driven and customer-focused company, Run Biotech provides a broad and integrated por

4-(4-Fluorophenyl)benzonitrile

Cas:10540-31-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

GZ HONESTCHEM CO., LTD

R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou

4'-Fluoro-[1,1'-biphenyl]-4-carbonitrile

Cas:10540-31-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shanghai Jingshi Pharmaceutical Technology Co., Ltd.

We promise quality; We deliver goods timely; We test product purity before delivery;We quote price reasonabl;We guarantee after sale service.Appearance:White or off-white crystalline powder Storage:cool and dry area,avoiding light Package:1g/5g/10g/2

4-(4-Fluorophenyl)benzonitrile

Cas:10540-31-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shanghai chamflyer chemicals Co., Ltd

High quality Application:Pharmaceutial

4'-Fluoro-[1,1'-biphenyl]-4-carbonitrile

Cas:10540-31-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Sinofluoro Scientific Co., Ltd

4-(4-Fluorophenyl)benzonitrile

4-(4-Fluorophenyl)benzonitrile

Cas:10540-31-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

NovaChemistry

high purity Application:Drug intermediates Materials intermediates and active molecules

4-(4-Fluorophenyl)benzonitrile

Cas:10540-31-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

4-bromobenzenecarbonitrile
623-00-7

4-bromobenzenecarbonitrile

4-fluoroboronic acid
1765-93-1

4-fluoroboronic acid

4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

Conditions
ConditionsYield
With potassium carbonate; palladium dichloride In ethanol; water at 20℃; for 0.0833333h; Suzuki cross-coupling;99%
With potassium carbonate; polymer-supported Pd catalyst FC 1001 In ethanol at 110℃; for 0.166667h; Suzuki coupling; microwave irradiation;98%
With Ph2P(CH2CH2O)22CH3; triethylamine; palladium dichloride In water at 80℃; for 1h; Suzuki coupling; Inert atmosphere;98%
4-cyanophenyl trifluoromethanesulfonate
66107-32-2

4-cyanophenyl trifluoromethanesulfonate

potassim 4-fluorophenyltrifluoroborate

potassim 4-fluorophenyltrifluoroborate

4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

Conditions
ConditionsYield
With palladium diacetate In ethanol at 95℃; for 0.25h; microwave irradiation;99%
4-Cyanochlorobenzene
623-03-0

4-Cyanochlorobenzene

4-flourophenylmagnesium bromide
352-13-6

4-flourophenylmagnesium bromide

4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

Conditions
ConditionsYield
Stage #1: 4-Cyanochlorobenzene With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate In tetrahydrofuran; toluene Kumada Cross-Coupling; Inert atmosphere; Sealed tube;
Stage #2: 4-flourophenylmagnesium bromide In tetrahydrofuran; toluene at 20℃; for 1.5h; Kumada Cross-Coupling; Inert atmosphere; Sealed tube; chemoselective reaction;
98%
4-bromobenzenecarbonitrile
623-00-7

4-bromobenzenecarbonitrile

potassim 4-fluorophenyltrifluoroborate

potassim 4-fluorophenyltrifluoroborate

4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

Conditions
ConditionsYield
With palladium diacetate; potassium carbonate In methanol for 2h; Suzuki-Miyaura cross-coupling; Heating;96%
With potassium carbonate; palladium diacetate In methanol for 2h; Suzuki reaction; Heating;96%
4-Cyanochlorobenzene
623-03-0

4-Cyanochlorobenzene

4-fluoroboronic acid
1765-93-1

4-fluoroboronic acid

4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

Conditions
ConditionsYield
With C23H20ClFeN3Pd; potassium carbonate In water; N,N-dimethyl-formamide at 80℃; for 4h; Reagent/catalyst; Suzuki-Miyaura Coupling;95%
4-fluoroboronic acid
1765-93-1

4-fluoroboronic acid

4-cyanophenol
767-00-0

4-cyanophenol

4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

Conditions
ConditionsYield
Stage #1: 4-cyanophenol With fluorosulfonyl fluoride; triethylamine In ethanol; water at 20℃; for 4h;
Stage #2: 4-fluoroboronic acid With palladium diacetate; triethylamine In ethanol; water at 20℃; for 6h;
95%
4-cyanophenyl sulfurofluoridate

4-cyanophenyl sulfurofluoridate

4-fluoroboronic acid
1765-93-1

4-fluoroboronic acid

4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

Conditions
ConditionsYield
With palladium diacetate; triethylamine In water at 20℃; for 2h; Suzuki-Miyaura Coupling;94%
2-(4-fluorophenyl)-6-methyl-1,3,6,2-dioxazaborocane-4,8-dione

2-(4-fluorophenyl)-6-methyl-1,3,6,2-dioxazaborocane-4,8-dione

4-cyanobenzene-1-sulfonyl fluoride
33719-37-8

4-cyanobenzene-1-sulfonyl fluoride

4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

Conditions
ConditionsYield
With palladium diacetate; potassium carbonate; diisopropylamine In ethanol; water at 45℃; for 4h;94%
4-iodobenzonitrile
3058-39-7

4-iodobenzonitrile

tributyl(4-fluorophenyl)stannane
17151-47-2

tributyl(4-fluorophenyl)stannane

4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

Conditions
ConditionsYield
With 4,4’‐bis(trimethylammoniummethyl)‐2,2’‐bipyridine; diamminedichloropalladium(II); sodium hydrogencarbonate In water at 110℃; for 3h; Stille Cross Coupling; Sealed tube;93%
4-bromobenzenecarbonitrile
623-00-7

4-bromobenzenecarbonitrile

2-(4-fluorophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
214360-58-4

2-(4-fluorophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

Conditions
ConditionsYield
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate In 1,4-dioxane; water at 90℃; for 12h; Inert atmosphere;92.5%
(4-cyanophenyl)magnesium bromide
412044-48-5

(4-cyanophenyl)magnesium bromide

4-flourophenylmagnesium bromide
352-13-6

4-flourophenylmagnesium bromide

4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

Conditions
ConditionsYield
Stage #1: (4-cyanophenyl)magnesium bromide; 4-flourophenylmagnesium bromide With lithium chloride; manganese(ll) chloride In tetrahydrofuran at -10℃; Inert atmosphere;
Stage #2: With oxygen In tetrahydrofuran at 10 - 20℃;
91%
4-Cyanochlorobenzene
623-03-0

4-Cyanochlorobenzene

2-(4-fluorophenyl)-5,5-dimethyl-1,3,2-dioxaborinane
225916-39-2

2-(4-fluorophenyl)-5,5-dimethyl-1,3,2-dioxaborinane

4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

Conditions
ConditionsYield
With P(t-Bu)3 Palladacycle Gen. 3; potassium trimethylsilonate In tetrahydrofuran at 23℃; for 0.25h; Suzuki-Miyaura Coupling;91%
4-bromobenzenecarbonitrile
623-00-7

4-bromobenzenecarbonitrile

2-(4-fluorophenyl)-6-methyl-1,3,6,2-dioxazaborocane-4,8-dione

2-(4-fluorophenyl)-6-methyl-1,3,6,2-dioxazaborocane-4,8-dione

4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

Conditions
ConditionsYield
With palladium diacetate; diisopropylamine In water at 100℃; for 1h; Suzuki-Miyaura Coupling;88%
4-fluoroboronic acid
1765-93-1

4-fluoroboronic acid

4-[(trifluoromethyl)sulfonyl] benzonitrile
312-21-0

4-[(trifluoromethyl)sulfonyl] benzonitrile

4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

Conditions
ConditionsYield
With potassium phosphate; palladium(II) acetylacetonate; ruphos In 1,4-dioxane; dimethyl sulfoxide at 80℃; for 16h; Suzuki-Miyaura Coupling; Sealed tube; Inert atmosphere;82%
4-Cyanochlorobenzene
623-03-0

4-Cyanochlorobenzene

(4-fluorophenyl)zinc pivalate

(4-fluorophenyl)zinc pivalate

4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

Conditions
ConditionsYield
[1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl) palladium(II) dichloride In tetrahydrofuran at 25℃; for 2h; Negishi Coupling Reaction;80%
4-iodobenzonitrile
3058-39-7

4-iodobenzonitrile

tris(4-fluorophenyl)bismuthane
437-29-6

tris(4-fluorophenyl)bismuthane

4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

Conditions
ConditionsYield
With potassium acetate; palladium diacetate; N-cyclohexyl-cyclohexanamine In N,N-dimethyl-formamide at 35℃; for 2h; Inert atmosphere;78%
zinc(II) cyanide
557-21-1

zinc(II) cyanide

4′-fluoro-[1,1'-biphenyl]-4-yl methanesulfonate

4′-fluoro-[1,1'-biphenyl]-4-yl methanesulfonate

4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

Conditions
ConditionsYield
With dmap; nickel(II) bromide dimethoxyethane; 1,4-di(diphenylphosphino)-butane; zinc In acetonitrile at 80℃; for 12h; Sealed tube; Inert atmosphere;77%
4-Cyanochlorobenzene
623-03-0

4-Cyanochlorobenzene

triallyl(4-fluorophenyl)silane
725735-33-1

triallyl(4-fluorophenyl)silane

4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

Conditions
ConditionsYield
Stage #1: triallyl(4-fluorophenyl)silane With tetrabutyl ammonium fluoride In tetrahydrofuran; water at 20℃; for 1h;
Stage #2: 4-Cyanochlorobenzene With XPhos; bis(η3-allyl-μ-chloropalladium(II)) In tetrahydrofuran; water at 80℃; for 11h;
73%
4-bromobenzenecarbonitrile
623-00-7

4-bromobenzenecarbonitrile

4-fluorophenyhydrazine hydrochloride
823-85-8

4-fluorophenyhydrazine hydrochloride

4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

Conditions
ConditionsYield
With potassium carbonate In acetonitrile at 50℃; for 8h;71%
4-bromobenzenecarbonitrile
623-00-7

4-bromobenzenecarbonitrile

triallyl(4-fluorophenyl)silane
725735-33-1

triallyl(4-fluorophenyl)silane

4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

Conditions
ConditionsYield
Stage #1: triallyl(4-fluorophenyl)silane With tetrabutyl ammonium fluoride In water; dimethyl sulfoxide at 20℃; for 1h;
Stage #2: 4-bromobenzenecarbonitrile With tricyclohexylphosphine; palladium dichloride In water; dimethyl sulfoxide at 80℃; for 18h;
69%
N-(4-cyanophenyl)acetamide
35704-19-9

N-(4-cyanophenyl)acetamide

potassim 4-fluorophenyltrifluoroborate

potassim 4-fluorophenyltrifluoroborate

A

4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

B

4,4'-difluorobiphenyl
398-23-2

4,4'-difluorobiphenyl

Conditions
ConditionsYield
Stage #1: N-(4-cyanophenyl)acetamide With boron trifluoride methanol complex In methanol at 65℃; Inert atmosphere;
Stage #2: With tert.-butylnitrite In methanol at 0℃; for 1h; Inert atmosphere;
Stage #3: potassim 4-fluorophenyltrifluoroborate With palladium diacetate In methanol at 20℃; for 12.25h; Suzuki Coupling; Inert atmosphere;
A 65%
B 10%
4-fluoroboronic acid
1765-93-1

4-fluoroboronic acid

N-methyl-di-4-cyanobenzenesulfonamide

N-methyl-di-4-cyanobenzenesulfonamide

4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

Conditions
ConditionsYield
With potassium phosphate; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II) In 1,4-dioxane at 110℃; Suzuki-Miyaura Coupling; Schlenk technique; Inert atmosphere;51%
C25H16BF3N(1-)*K(1+)

C25H16BF3N(1-)*K(1+)

4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

Conditions
ConditionsYield
With 10-methyl-9-(2,4,6-trimethylphenyl) acridinium tetrafluoroborate; oxygen In acetonitrile at 50℃; for 16h; Inert atmosphere; Irradiation;47%
4-fluoroboronic acid
1765-93-1

4-fluoroboronic acid

1-(methylsulfonyl)-2-(4-cyanophenyl)diazene

1-(methylsulfonyl)-2-(4-cyanophenyl)diazene

4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

Conditions
ConditionsYield
With [2,2]bipyridinyl; (triphenylphosphine)gold(I) chloride; sodium acetate In methanol; acetonitrile for 16h; Suzuki Coupling; Inert atmosphere; Irradiation;37%
4-Fluorobenzoic acid
456-22-4

4-Fluorobenzoic acid

4-bromobenzenecarbonitrile
623-00-7

4-bromobenzenecarbonitrile

4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

Conditions
ConditionsYield
With sodium carbonate In methanol at 150℃; for 1h; Suzuki-Miyaura Coupling; Microwave irradiation;8%
4-fluorobenzenediazonium tetrafluoroborate
459-45-0

4-fluorobenzenediazonium tetrafluoroborate

benzonitrile
100-47-0

benzonitrile

A

4'-fluoro-[1,1'-biphenyl]-3-carbonitrile
10540-33-7

4'-fluoro-[1,1'-biphenyl]-3-carbonitrile

B

4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

C

4'-fluoro-[1,1'-biphenyl]-2-carbonitrile
89346-55-4

4'-fluoro-[1,1'-biphenyl]-2-carbonitrile

Conditions
ConditionsYield
With potassium acetate; 18-crown-6 ether for 1.5h; Ambient temperature; Yield given. Yields of byproduct given;
methanol
67-56-1

methanol

4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

4'-fluoro-N-methyl-[1,1'-biphenyl]-4-carboxamide

4'-fluoro-N-methyl-[1,1'-biphenyl]-4-carboxamide

Conditions
ConditionsYield
With tris(2-diphenylphosphinoethyl)phosphine; potassium tert-butylate; water; caesium carbonate; cobalt(II) bromide In m-xylene at 140℃; for 24h; Green chemistry;97%
4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

4-fluoro-biphenyl
324-74-3

4-fluoro-biphenyl

Conditions
ConditionsYield
With bis(1,5-cyclooctadiene)nickel (0); hydrogen; trimethylaluminum; tricyclohexylphosphine In toluene at 130℃; under 750.075 Torr; for 24h; Schlenk technique;82%
With [1,1'-bis(diphenylphosphino)ferrocene]nickel(II) chloride; ethanol; potassium hexamethylsilazane In toluene at 150℃; for 8h; Inert atmosphere; Molecular sieve;58%
4-cyano-4'-fluorobiphenyl
10540-31-5

4-cyano-4'-fluorobiphenyl

ethylmagnesium bromide
925-90-6

ethylmagnesium bromide

1-(4'-fluoro-[1,1'-biphenyl]-4-yl)cyclopropan-1-amine

1-(4'-fluoro-[1,1'-biphenyl]-4-yl)cyclopropan-1-amine

Conditions
ConditionsYield
Stage #1: 4-cyano-4'-fluorobiphenyl; ethylmagnesium bromide With titanium(IV) isopropylate In diethyl ether at 0 - 20℃; for 1h;
Stage #2: With boron trifluoride diethyl etherate In diethyl ether at 20℃; for 2h;
39.1%

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