Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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inquiryDayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
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inquiry- Analysis tests Standard Results Appearance White crystalline powder conforms H-NMR S
Cas:1062580-52-2
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inquiryProduct Description Product Name (3R,4R)-N,4-Dimethyl-1-(phenylmethyl)-3-piperidinamine hydrochloride CAS No. 1062580-52-2 Assay ≥99% Appearance White powder Capacity 50mt/year
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inquiry(3R,4R)-N,4-Dimethyl-1-(phenylmethyl)-3-piperidinamine hydrochloride CAS No.:1062580-52-2 Name: (3R,4R)-N,4-Dimethyl-1-(phenylmethyl)-3-piperidinamine hydrochloride Molecular Structure Molecular Formula: C14
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api, intermedi
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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inquiryName:CIS-N-BENZYL-3-METHYLAMINO-4-METHYL-PIPERIDINE BIS-(HYDROCHLORIDE) CAS NO:1062580-52-2 Grade:Medical scientific research and export Molecular formula:C14H22N2·2(HCl) Molecular weight:291.26 Product Quality 12 years of chemical ra
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:1062580-52-2
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inquiryName: (3R,4R)-N,4-Dimethyl-1-(phenylmethyl)-3-piperidinamine hydrochloride Synonyms: (3R,4R)-1-Benzyl-N,4-dimethylpiperidin-3-amine dihydrochloride CAS:1062580-52-2 MF: C14H22N2·2(HCl) Appearance: white powder Storage:Store in cool and dr
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:White Crystalline Powder Storage:Store in sealed conta
Cas:1062580-52-2
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiryHangzhou Huarong Pharm Co., Ltd. established since 2009 , has been always focusing on supplying products and services to our clients in the field of small molecule drug. Huarong Pharm has built platforms for the research, development and manufac
Cas:1062580-52-2
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inquiryProduct Name: (3R,4R)-1-benzyl-N,4-dimethylpiperidin-3-amine dihydrochloride Synonyms: CIS-N-BENZYL-3-METHYLAMINO-4-METHYL-PIPERIDINE BIS-(HYDROCHLORIDE);cis-1-Benzyl-N,4-dimethylpiperidin-3-amine dihydrochloride;cis-1-Benzyl-4-methyl-3-(methyl
Cas:1062580-52-2
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry(3R,4R)-1-benzyl-N,4-dimethylpiperidin-3-amine dihydrochloride CAS:1062580-52-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediate
Cas:1062580-52-2
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:1062580-52-2
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:1062580-52-2
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inquiryProduct Name: CIS-N-BENZYL-3-METHYLAMINO-4-METHYL-PIPERIDINE BIS-(HYDROCHLORIDE) Synonyms: (3R,4R)-1-苄基-N,4-二甲基哌啶-3-胺二盐酸盐;CIS-N-BENZYL-3-METHYLAMINO-4-METHYL-PIPERIDINE BIS-(HYDROCHLORIDE);cis-1-Benzyl-N,4-dimethylpiperidin-3-amine dihydrochlorid
Cas:1062580-52-2
Min.Order:100 Gram
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:1062580-52-2
Min.Order:4 Kilogram
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
Cas:1062580-52-2
Min.Order:1 Gram
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:1062580-52-2
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:1062580-52-2
Min.Order:10 Gram
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:1062580-52-2
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inquiryN-(3R,4R)-(1-benzyl-4-methylpiperidin-3-yl)-methylamine
N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol at 0 - 5℃; pH=3 - 4; | 94% |
With hydrogenchloride In n-heptane; isopropyl alcohol at 20℃; for 0.666667h; Reflux; | 60% |
1-benzyl-4-methyl-piperidin-3-one
methylamine
N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride
Conditions | Yield |
---|---|
Stage #1: 1-benzyl-4-methyl-piperidin-3-one; methylamine With titanium tetrachloride; triethylamine In tetrahydrofuran at 20℃; for 4h; Stage #2: With sodium tris(acetoxy)borohydride; acetic acid In tetrahydrofuran at 25℃; Stage #3: With hydrogenchloride In ethanol | 85% |
1-benzyl-4-methyl-piperidin-3-one
methylamine acetate
A
N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride
Conditions | Yield |
---|---|
Stage #1: 1-benzyl-4-methyl-piperidin-3-one; methylamine acetate With bis(1,5-cyclooctadiene)diiridium(I) dichloride; (S)-3,5-di-tert-butyl-4-methoxyphenyl-(6,6’-dimethoxybiphenyl-2,2’-diyl)-bis(diphenylphosphine); hydrogen In dichloromethane; isopropyl alcohol at 70℃; under 37503.8 Torr; for 18h; Stage #2: With hydrogenchloride In dichloromethane; water; isopropyl alcohol Overall yield = 86%; Overall yield = 498 mg; enantioselective reaction; | A n/a B 74% |
(1-benzyl-4-methyl-piperidin-3-yl)-methyl-amine
A
N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In diethyl ether; acetone for 1h; Inert atmosphere; Overall yield = 498 mg; |
1-benzyl-4-methyl-piperidin-3-one
A
N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: ethanol / 5 h / 20 °C / Inert atmosphere 2: hydrogen; bis(1,5-cyclooctadiene)diiridium(I) dichloride; (R)-diMe-PipPhos / isopropyl alcohol / 18 h / 20 °C / 37503.8 Torr / Glovebox; Inert atmosphere 3: hydrogenchloride / acetone; diethyl ether / 1 h / Inert atmosphere View Scheme |
A
N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: hydrogen; bis(1,5-cyclooctadiene)diiridium(I) dichloride; (R)-diMe-PipPhos / isopropyl alcohol / 18 h / 20 °C / 37503.8 Torr / Glovebox; Inert atmosphere 2: hydrogenchloride / acetone; diethyl ether / 1 h / Inert atmosphere View Scheme |
N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: lithium aluminium tetrahydride / tetrahydrofuran / 2.83 h / 0 °C / Reflux 2: hydrogenchloride / isopropyl alcohol; n-heptane / 0.67 h / 20 °C / Reflux View Scheme |
(1-benzyl-4-methyl-1,2,5,6-tetrahydropyridin-3-yl)carbamic acid methyl ester
N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: hydrogen; bis(1,5-cyclooctadiene)rhodium(I) trifluoromethanesulfonate; (R)-1-[(Sp)-2-(di-tert-butylphosphino)ferrocenyl]ethylbis(2-methylphenyl)phosphine / 2,2,2-trifluoroethanol / 6 h / 30 - 50 °C / 2625.26 Torr 2: lithium aluminium tetrahydride / tetrahydrofuran / 2.83 h / 0 °C / Reflux 3: hydrogenchloride / isopropyl alcohol; n-heptane / 0.67 h / 20 °C / Reflux View Scheme |
3-amino-4-methylpyridine
N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: dichloromethane; toluene / 10 h / 20 - 25 °C / Large scale 1.2: 70 - 80 °C / Large scale 1.3: 14 h / 10 °C / Large scale 2.1: hydrogenchloride / water; n-heptane / 70 - 75 °C / Large scale 2.2: 0 - 5 °C / Large scale 3.1: Di-p-toluoyl-L-tartaric acid / methanol / 1 h / 50 - 55 °C / Large scale 3.2: 2 h / pH 3 / Large scale View Scheme |
N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: hydrogenchloride / water; n-heptane / 70 - 75 °C / Large scale 1.2: 0 - 5 °C / Large scale 2.1: Di-p-toluoyl-L-tartaric acid / methanol / 1 h / 50 - 55 °C / Large scale 2.2: 2 h / pH 3 / Large scale View Scheme |
1-benzyl-4-methyl-piperidin-3-one
N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride
Conditions | Yield |
---|---|
Stage #1: 1-benzyl-4-methyl-piperidin-3-one With Di-p-toluoyl-L-tartaric acid In methanol at 50 - 55℃; for 1h; Large scale; Stage #2: With hydrogenchloride In methanol; water for 2h; pH=3; Large scale; | 1.7 kg |
benzyl chloride
N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: dichloromethane; toluene / 10 h / 20 - 25 °C / Large scale 1.2: 70 - 80 °C / Large scale 1.3: 14 h / 10 °C / Large scale 2.1: hydrogenchloride / water; n-heptane / 70 - 75 °C / Large scale 2.2: 0 - 5 °C / Large scale 3.1: Di-p-toluoyl-L-tartaric acid / methanol / 1 h / 50 - 55 °C / Large scale 3.2: 2 h / pH 3 / Large scale View Scheme |
N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride
2,4-dichloro-7H-pyrrolo[2,3-d]pyrimidine
Conditions | Yield |
---|---|
Stage #1: N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride; 2,4-dichloro-7H-pyrrolo[2,3-d]pyrimidine With potassium carbonate In water at 98 - 102℃; for 10h; Stage #2: at 20 - 25℃; for 4h; | 93.6% |
With potassium carbonate In water at 90℃; Reagent/catalyst; Solvent; Temperature; | 89.5% |
With potassium carbonate In water for 10h; Reflux; | 82.3% |
Stage #1: N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride With potassium carbonate In water Large scale; Stage #2: 2,4-dichloro-7H-pyrrolo[2,3-d]pyrimidine In water at 100℃; Large scale; | 4.72 kg |
4-chloro-7-[(4-methylphenyl)sulfonyl]-7H-pyrrolo[2,3-d]pyrimidine
N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride
N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methyl-(7-p-toluenesulfonyl)-7H-pyrrolo[2,3-d]pyrimidin-4-amine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In water; dimethyl sulfoxide at 107℃; for 9h; Temperature; Large scale; | 93% |
Stage #1: N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride With potassium carbonate In water Stage #2: 4-chloro-7-[(4-methylphenyl)sulfonyl]-7H-pyrrolo[2,3-d]pyrimidine In water at 90 - 95℃; | 155 g |
N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide at 115 - 120℃; for 12h; | 82% |
N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride
Conditions | Yield |
---|---|
With potassium carbonate; p-toluenesulfonyl chloride; sodium hydroxide In water; acetone; acetonitrile at 0 - 95℃; for 1h; | 77% |
N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride
Conditions | Yield |
---|---|
Stage #1: N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride With N-ethyl-N,N-diisopropylamine In ethanol at 20℃; for 0.166667h; Stage #2: 3,4,6-trichloro-1H-pyrazolo[3,4-d]pyrimidine In ethanol at 100℃; for 2h; | 24.9% |
N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride
4-chloro-1H-pyrrolo[2,3-d]pyrimidine
Conditions | Yield |
---|---|
With potassium carbonate In water for 24h; Reflux; | 0.48% |
With potassium carbonate In water at 90℃; | 145 g |
N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride
Conditions | Yield |
---|---|
With potassium carbonate In ethanol; water Reagent/catalyst; Solvent; Reflux; | 280 g |
N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide; water / 9 h / 107 °C / Large scale 2: sodium hydroxide; water / dimethyl sulfoxide / 1 h / 80 °C / Large scale 3: 10 wt% Pd(OH)2 on carbon; hydrogen / ethanol / 3 h / 61 °C / 760.05 Torr / Large scale 4: 1,8-diazabicyclo[5.4.0]undec-7-ene / ethanol / 1 h / 49 °C / Large scale 5: water / 96 °C / Large scale View Scheme | |
Multi-step reaction with 3 steps 1: potassium carbonate / water / 10 h / Reflux 2: acetic acid; 5%-palladium/activated carbon; triethylsilane / methanol / 0.17 h / 30 °C 3: 1,8-diazabicyclo[5.4.0]undec-7-ene / butan-1-ol / 0.17 h / 80 °C View Scheme | |
Multi-step reaction with 4 steps 1: potassium carbonate / water / 90 °C 2: hydrogen; hydrogenchloride; palladium on carbon / water / 120 °C / 2068.65 Torr 3: dichloromethane / -20 °C 4: water; ethanol / 0 °C View Scheme | |
Multi-step reaction with 4 steps 1: potassium carbonate / water / 90 °C 2: hydrogen; hydrogenchloride; palladium on carbon / water / 120 °C / 2068.65 Torr 3: tetrahydrofuran / 45 °C 4: water; ethanol / 0 °C View Scheme | |
Multi-step reaction with 4 steps 1: potassium carbonate / water / 90 °C 2: hydrogen; hydrogenchloride; palladium on carbon / water / 120 °C / 2068.65 Torr 3: tetrahydrofuran / 45 °C 4: water; ethanol / 0 °C View Scheme |
N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide; water / 9 h / 107 °C / Large scale 2: sodium hydroxide; water / dimethyl sulfoxide / 1 h / 80 °C / Large scale View Scheme | |
Multi-step reaction with 2 steps 1.1: potassium carbonate / water 1.2: 90 - 95 °C 2.1: potassium hydroxide; methanol / 40 - 45 °C View Scheme |
N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide; water / 9 h / 107 °C / Large scale 2: sodium hydroxide; water / dimethyl sulfoxide / 1 h / 80 °C / Large scale 3: 10 wt% Pd(OH)2 on carbon; hydrogen / ethanol / 3 h / 61 °C / 760.05 Torr / Large scale View Scheme |
N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide; water / 9 h / 107 °C / Large scale 2: sodium hydroxide; water / dimethyl sulfoxide / 1 h / 80 °C / Large scale 3: 10 wt% Pd(OH)2 on carbon; hydrogen / ethanol / 3 h / 61 °C / 760.05 Torr / Large scale 4: 1,8-diazabicyclo[5.4.0]undec-7-ene / ethanol / 1 h / 49 °C / Large scale View Scheme | |
Multi-step reaction with 3 steps 1: potassium carbonate / water / 90 °C 2: acetic acid; 20% palladium hydroxide-activated charcoal; hydrogen / water 3: 1,8-diazabicyclo[5.4.0]undec-7-ene / butan-1-ol View Scheme | |
Multi-step reaction with 3 steps 1: potassium carbonate / water / 90 °C 2: hydrogen; hydrogenchloride; palladium on carbon / water / 120 °C / 2068.65 Torr 3: dichloromethane / -20 °C View Scheme | |
Multi-step reaction with 3 steps 1: potassium carbonate / water / 90 °C 2: hydrogen; hydrogenchloride; palladium on carbon / water / 120 °C / 2068.65 Torr 3: tetrahydrofuran / 45 °C View Scheme | |
Multi-step reaction with 3 steps 1: potassium carbonate / water / 90 °C 2: hydrogen; hydrogenchloride; palladium on carbon / water / 120 °C / 2068.65 Torr 3: tetrahydrofuran / 45 °C View Scheme |
N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride
tert-butyl (3R,4R)-4-methyl-3-(methyl(7H-pyrrolo[2,3-d]pyrimidin-4-yl)amino)piperidine-1-carboxylate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium carbonate / water / 24 h / Reflux 2: palladium 10% on activated carbon; hydrogen / methanol / 24 h View Scheme | |
Multi-step reaction with 2 steps 1: potassium carbonate / water / 10 h / Reflux 2: acetic acid; 5%-palladium/activated carbon; triethylsilane / methanol / 0.17 h / 30 °C View Scheme | |
Multi-step reaction with 2 steps 1: potassium carbonate / water / 90 °C 2: acetic acid; 20% palladium hydroxide-activated charcoal; hydrogen / water View Scheme | |
Multi-step reaction with 2 steps 1: potassium carbonate / water / 90 °C 2: hydrogen; hydrogenchloride; palladium on carbon / water / 120 °C / 2068.65 Torr View Scheme | |
Multi-step reaction with 3 steps 1.1: potassium carbonate / water 1.2: 90 - 95 °C 2.1: potassium hydroxide; methanol / 40 - 45 °C 3.1: hydrogenchloride / water / 20 °C / pH 3.5 - 4.5 3.2: 45 - 50 °C View Scheme |
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