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inquiryConfirm; RH-5992; Tebufenozide suspension; N-tert-butyl-N'-(4-ethylbenzoyl)-3,5-dimethylbenzohydrazide; 3,5-dimethylbenzoic acid 1-(1,1-dimethylethyl)-2-(4-ethylbenzoyl)hydrazide Common name tebufenozide IUPAC name N-tert-butyl-N'-(4-
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inquiryAdvantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best service is
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inquiryBest quality/price/service Professional manufacturing FAO Standards Appearance:white powder Package:Solid:50g,100g,200g,250g,400g,500g,1kg,10kg bag ,20kg, 25kg,40kg bag,50kg,600kg, 900kg; Aluminum Foil Bag,plastic bag, fiber bag, fiber drum,wa
Cas:112410-23-8
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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Cas:112410-23-8
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inquiryHangzhou Fandachem Co.,Ltd, a China-based chemical company, specialize in exporting Tebufenozide,CAS:112410-23-8, Please contact us by email freely. We are leading exporter in China. If you really need this cargo, please do not hesitat
Cas:112410-23-8
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inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
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Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
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inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
3,5-dimethylbenzoyl chloride
1-(4-ethylbenzoyl)-2-t-butyl hydrazine
tebufenozide
Conditions | Yield |
---|---|
With sodium hydroxide In diethyl ether for 48h; Ambient temperature; |
p-ethylbenzoyl chloride
N-(3,5-Dimethylbenzoyl)-N-tert-Butyl-Hydrazine
tebufenozide
Conditions | Yield |
---|---|
With sodium hydroxide In dichloromethane; water at 20℃; |
3,5-dimethylbenzoic acid
tebufenozide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 84.2 percent / SOCl2 / 5 h / 80 °C 2: 1N aq. NaOH / diethyl ether / 48 h / Ambient temperature View Scheme |
p-ethylbenzoic acid
tebufenozide
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: SOCl2 / 5 h / 80 °C 2: aq. NaOH / dioxane / 48 h / Ambient temperature 3: 1N aq. NaOH / diethyl ether / 48 h / Ambient temperature View Scheme |
p-ethylbenzoyl chloride
tebufenozide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aq. NaOH / dioxane / 48 h / Ambient temperature 2: 1N aq. NaOH / diethyl ether / 48 h / Ambient temperature View Scheme |
p-ethylbenzoyl chloride
tertbutylhydrazine hydrochloride
3,5-dimethylbenzoyl chloride
tebufenozide
Conditions | Yield |
---|---|
With sodium hydroxide In toluene |
phosgene
tebufenozide
Conditions | Yield |
---|---|
Stage #1: tebufenozide With potassium tert-butylate In tetrahydrofuran at 20℃; for 1h; Stage #2: phosgene In tetrahydrofuran; ethyl acetate at -78℃; for 0.5h; | 95% |
thiophosgene
tebufenozide
Conditions | Yield |
---|---|
Stage #1: tebufenozide With potassium tert-butylate In tetrahydrofuran at 20℃; Stage #2: thiophosgene In tetrahydrofuran; ethyl acetate at -78℃; | 80% |
ethyl bromoacetate
tebufenozide
Conditions | Yield |
---|---|
Stage #1: tebufenozide With sodium hydride In N,N-dimethyl-formamide at 20℃; for 2h; Stage #2: ethyl bromoacetate In N,N-dimethyl-formamide at 35 - 40℃; for 10h; | 62% |
tebufenozide
Conditions | Yield |
---|---|
With pyridine; oxalyl dichloride In 1,2-dichloro-ethane at 20℃; for 6h; | 60.8% |
With pyridine; oxalyl dichloride In dichloromethane at 20℃; |
chlorosulfenyl[O-(1-methylthioethylimino)-N-methylcarbamate]
tebufenozide
Conditions | Yield |
---|---|
Stage #1: tebufenozide With sodium hydride In xylene for 2h; Heating; Stage #2: chlorosulfenyl[O-(1-methylthioethylimino)-N-methylcarbamate] In xylene at 20℃; for 6h; Further stages.; | 52% |
bromoacetic acid methyl ester
tebufenozide
Conditions | Yield |
---|---|
Stage #1: tebufenozide With sodium hydride In N,N-dimethyl-formamide at 20℃; for 2h; Stage #2: bromoacetic acid methyl ester In N,N-dimethyl-formamide at 35 - 40℃; for 10h; | 50% |
oxalyl dichloride
tebufenozide
Conditions | Yield |
---|---|
In 1,2-dichloro-ethane for 8h; Heating; | A 45.3% B 32% |
In 1,2-dichloro-ethane Heating; |
tebufenozide
Conditions | Yield |
---|---|
Stage #1: tebufenozide With sodium hydride In tetrahydrofuran at 20℃; for 0.5h; Stage #2: chlorooxalyl-methyl-carbamic acid m-tolyl ester In tetrahydrofuran at 20℃; for 4h; | 42.8% |
tebufenozide
Conditions | Yield |
---|---|
Stage #1: tebufenozide With sodium hydride In tetrahydrofuran at 20℃; for 0.5h; Stage #2: chlorooxalyl-methyl-carbamic acid 2-isopropyl-phenyl ester In tetrahydrofuran at 20℃; for 4h; | 40.5% |
phenyl oxalyl chloride
tebufenozide
Conditions | Yield |
---|---|
Stage #1: tebufenozide With sodium hydride In tetrahydrofuran at 20℃; for 1h; Stage #2: phenyl oxalyl chloride In tetrahydrofuran at 20℃; for 5h; |
tebufenozide
Conditions | Yield |
---|---|
Stage #1: tebufenozide With sodium hydride In tetrahydrofuran at 20℃; for 1h; Stage #2: 4-chlorooxalyloxy-benzoic acid methyl ester In tetrahydrofuran at 20℃; for 5h; |
tebufenozide
Conditions | Yield |
---|---|
Stage #1: tebufenozide With sodium hydride In tetrahydrofuran at 20℃; for 1h; Stage #2: 2-chlorooxalyloxy-benzoic acid methyl ester In tetrahydrofuran at 20℃; for 5h; |
tebufenozide
Conditions | Yield |
---|---|
Stage #1: tebufenozide With sodium hydride In tetrahydrofuran at 20℃; for 1h; Stage #2: 3-chlorooxalyloxy-benzoic acid methyl ester In tetrahydrofuran at 20℃; for 5h; |
tebufenozide
Conditions | Yield |
---|---|
Stage #1: tebufenozide With sodium hydride In tetrahydrofuran at 20℃; for 1h; Stage #2: 4-chlorooxalyloxy-benzoic acid isopropyl ester In tetrahydrofuran at 20℃; for 5h; |
tebufenozide
Conditions | Yield |
---|---|
Stage #1: tebufenozide With sodium hydride In tetrahydrofuran at 20℃; for 1h; Stage #2: 2-chlorooxalyloxy-benzoic acid isopropyl ester In tetrahydrofuran at 20℃; for 5h; |
tebufenozide
Conditions | Yield |
---|---|
Stage #1: tebufenozide With sodium hydride In tetrahydrofuran at 20℃; for 1h; Stage #2: 3-chlorooxalyloxy-benzoic acid isopropyl ester In tetrahydrofuran at 20℃; for 5h; |
tebufenozide
Conditions | Yield |
---|---|
Stage #1: tebufenozide With sodium hydride In tetrahydrofuran at 20℃; for 1h; Stage #2: 4-chlorooxalyloxy-benzoic acid butyl ester In tetrahydrofuran at 20℃; for 5h; |
tebufenozide
Conditions | Yield |
---|---|
Stage #1: tebufenozide With sodium hydride In tetrahydrofuran at 20℃; for 1h; Stage #2: 2-chlorooxalyloxy-benzoic acid butyl ester In tetrahydrofuran at 20℃; for 5h; |
tebufenozide
Conditions | Yield |
---|---|
Stage #1: tebufenozide With sodium hydride In tetrahydrofuran at 20℃; for 1h; Stage #2: 3-chlorooxalyloxy-benzoic acid butyl ester In tetrahydrofuran at 20℃; for 5h; |
tebufenozide
4-chlorooxalyloxy-benzoic acid benzyl ester
Conditions | Yield |
---|---|
Stage #1: tebufenozide With sodium hydride In tetrahydrofuran at 20℃; for 1h; Stage #2: 4-chlorooxalyloxy-benzoic acid benzyl ester In tetrahydrofuran at 20℃; for 5h; |
tebufenozide
2-chlorooxalyloxy-benzoic acid benzyl ester
2-{[N'-tert-butyl-N'-(3,5-dimethyl-benzoyl)-N-(4-ethyl-benzoyl)-hydrazino]-oxo-acetoxy}-benzoic acid benzyl ester
Conditions | Yield |
---|---|
Stage #1: tebufenozide With sodium hydride In tetrahydrofuran at 20℃; for 1h; Stage #2: 2-chlorooxalyloxy-benzoic acid benzyl ester In tetrahydrofuran at 20℃; for 5h; |
tebufenozide
3-chlorooxalyloxy-benzoic acid benzyl ester
3-{[N'-tert-butyl-N'-(3,5-dimethyl-benzoyl)-N-(4-ethyl-benzoyl)-hydrazino]-oxo-acetoxy}-benzoic acid benzyl ester
Conditions | Yield |
---|---|
Stage #1: tebufenozide With sodium hydride In tetrahydrofuran at 20℃; for 1h; Stage #2: 3-chlorooxalyloxy-benzoic acid benzyl ester In tetrahydrofuran at 20℃; for 5h; |
tebufenozide
C22H27ClN2O2S
Conditions | Yield |
---|---|
With pyridine; sulfur dichloride In dichloromethane at 20℃; for 4h; |
tebufenozide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 45.3 percent / 1,2-dichloro-ethane / 8 h / Heating 2: 92.7 percent / 2 h / Heating View Scheme |
tebufenozide
4-ethyl-N-phenyl benzamide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: tBuOK / tetrahydrofuran / 1 h / 20 °C 1.2: 95 percent / tetrahydrofuran; ethyl acetate / 0.5 h / -78 °C 2.1: 300 mg / tetrahydrofuran / 4 h View Scheme |
tebufenozide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: tBuOK / tetrahydrofuran / 1 h / 20 °C 1.2: 95 percent / tetrahydrofuran; ethyl acetate / 0.5 h / -78 °C 2.1: 250 mg / tetrahydrofuran / 4 h View Scheme |
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