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inquiryName: 3-Chloro-4-methoxybenzenemethanamine Synonyms: 1-(3-Chloro-4-methoxyphenyl)methanamine CAS: 115514-77-7 MF: C8H10ClNO Appearance:White powder Storage:Store in cool and dry place, away from sun light. Package:25kg/drum Application: Organic in
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inquiry3-Chloro-4-methoxybenzenemethanamineAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:pharmaceutical intermediate Transportation:by air, by sea, by express
(3-chloro-4-methoxyphenyl)methanamine
Conditions | Yield |
---|---|
With hydrogenchloride at 50℃; for 1h; | 80% |
4-methoxy-benzylamine
(3-chloro-4-methoxyphenyl)methanamine
Conditions | Yield |
---|---|
With chlorine In acetic acid for 1h; Ambient temperature; | 34% |
With sulfuryl dichloride In acetic acid at 0 - 20℃; for 4h; |
(3-chloro-4-methoxyphenyl)methylamine hydrogen chloride
(3-chloro-4-methoxyphenyl)methanamine
Conditions | Yield |
---|---|
With sodium hydroxide In water; toluene at 25 - 30℃; |
3-chloro-4-methoxybenzyl alcohol
(3-chloro-4-methoxyphenyl)methanamine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: thionyl chloride / N,N-dimethyl-formamide; dichloromethane / Reflux 2: ethanol / 2 h / 20 - 30 °C / Reflux 3: hydrogenchloride / 1 h / 50 °C View Scheme |
4-chloro-2-methanesulfanylpyrimidine-5-carboxylic acid ethyl ester
(3-chloro-4-methoxyphenyl)methanamine
ethyl 4-[(3-chloro-4-methoxybenzyl)amino]-2-(methylsulfanyl)pyrimidine-5-carboxylate
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; | 100% |
With triethylamine In acetone at 20℃; for 3h; | 87% |
With triethylamine In dichloromethane at 20℃; for 10h; | 76% |
(3-chloro-4-methoxyphenyl)methanamine
2-methylsulfonyl-5-ethoxycarbonyl-4-(3-chloro-4-methoxybenzylamino)pyrimidine
Conditions | Yield |
---|---|
Stage #1: C8H10N2O5S With N-ethyl-N,N-diisopropylamine; trichlorophosphate In toluene Reflux; Green chemistry; Stage #2: (3-chloro-4-methoxyphenyl)methanamine With N-isopropylethylamine In toluene Reagent/catalyst; Green chemistry; | 97.2% |
Stage #1: C8H10N2O5S With N-ethyl-N,N-diisopropylamine; trichlorophosphate In toluene Reflux; Stage #2: (3-chloro-4-methoxyphenyl)methanamine With N-isopropylethylamine In toluene | 96.8% |
(3-chloro-4-methoxyphenyl)methanamine
3-chloro-4-methoxy-benzaldehyde
Conditions | Yield |
---|---|
With oxygen; [5,6]fullerene-C70 In chloroform; toluene at 20℃; for 24h; Sealed tube; Irradiation; | 96% |
Conditions | Yield |
---|---|
With sodium carbonate In N,N-dimethyl-formamide at 60℃; for 4h; Reflux; | 95% |
(3-chloro-4-methoxyphenyl)methanamine
2-aminomethylpyrimidine
Conditions | Yield |
---|---|
Stage #1: C6H6N2O5S With N-ethyl-N,N-diisopropylamine; trichlorophosphate In toluene Reflux; Stage #2: 2-aminomethylpyrimidine With N-ethyl-N,N-diisopropylamine In toluene at -8℃; Stage #3: (3-chloro-4-methoxyphenyl)methanamine With N-ethyl-N,N-diisopropylamine In toluene at 0℃; Temperature; | 93.8% |
(3-chloro-4-methoxyphenyl)methanamine
Conditions | Yield |
---|---|
Stage #1: 5-(4-{[4-(acetyloxy)piperidin-1-yl]methyl}-1,3-thiazol-2-yl)-1-ethyl-1H-indole-3-carboxylic acid With diphenyl phosphoryl azide; triethylamine In toluene at 20℃; for 0.5h; Stage #2: (3-chloro-4-methoxyphenyl)methanamine In toluene for 2h; Reflux; | 75% |
(3-chloro-4-methoxyphenyl)methanamine
3-(tert-butyl)-1-methyl-1H-pyrazole-5-carboxylic acid
Conditions | Yield |
---|---|
With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20 - 25℃; for 12h; Inert atmosphere; | 66% |
4-hydroxy-6-methyl-2-pyron
(3-chloro-4-methoxyphenyl)methanamine
1-(3-chloro-4-methoxybenzyl)-4-hydroxy-6-methylpyridin-2(1H)-one
Conditions | Yield |
---|---|
In water at 100℃; for 5.33333h; Heating / reflux; | 63% |
1,4-dichlorophthalazine
(3-chloro-4-methoxyphenyl)methanamine
Conditions | Yield |
---|---|
With sodium carbonate In N,N-dimethyl-formamide at 130℃; | 62% |
tert-butyl 10-chloro-8-cyano-3,4-dihydrobenzo[b][1,6]-naphthyridine-2(1H)-carboxylate
(3-chloro-4-methoxyphenyl)methanamine
tert-butyl 10-((3-chloro-4-methoxybenzyl)amino)-8-cyano-3,4-dihydrobenzo[b][1,6]naphthyridine-2-(1H)-carboxylate
Conditions | Yield |
---|---|
With triethylamine; sodium iodide In 1-methyl-pyrrolidin-2-one at 130℃; Inert atmosphere; | 49% |
(3-chloro-4-methoxyphenyl)methanamine
Conditions | Yield |
---|---|
With dicyclohexyl-(2′,4′,6′-triisopropyl-3,6-dimethoxy-[1,1′-biphenyl]-2-yl)phosphine; palladium diacetate; caesium carbonate In 1,4-dioxane at 120℃; Buchwald-Hartwig Coupling; Inert atmosphere; Sealed tube; | 44% |
(3-chloro-4-methoxyphenyl)methanamine
8-bromo-7-(3-chloropropyl)-1,3-dimethyl-3,7-dihydro-1H-purine-2,6-dione
Conditions | Yield |
---|---|
In propan-1-ol at 160℃; under 7500.75 Torr; for 1h; Microwave irradiation; Sealed tube; | 41% |
(3-chloro-4-methoxyphenyl)methanamine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; Inert atmosphere; | 31% |
styrene oxide
(3-chloro-4-methoxyphenyl)methanamine
N-(3-chloro-4-methoxybenzyl)-2-hydroxyphenethylamine
Conditions | Yield |
---|---|
In acetonitrile for 16h; Heating; | 25% |
(3-chloro-4-methoxyphenyl)methanamine
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene at 150℃; for 4h; Microwave irradiation; | 18% |
(3-chloro-4-methoxyphenyl)methanamine
Conditions | Yield |
---|---|
at 120℃; for 3h; | 5% |
(3-chloro-4-methoxyphenyl)methanamine
5-chloro-8-[5-(3-dimethylamino-pyrrolidine-1-sulfonyl)-2-propoxy-phenyl]-2-(4-methoxy-benzyl)-2,7-dihydro-2,3,4,7,9-pentaaza-cyclopenta[a]naphthalen-6-one
5-(3-chloro-4-methoxy-benzylamino)-8-[5-(3-dimethylamino-pyrrolidine-1-sulfonyl)-2-propoxy-phenyl]-2-(4-methoxy-benzyl)-2,7-dihydro-2,3,4,7,9-pentaaza-cyclopenta[a]naphthalen-6-one
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In propan-1-ol for 4h; Heating; |
4-(tert-butoxycarbonylamino)-1-(7H-pyrrolo[2,3-d]pyrimidin-4-yl)piperidine-4-carboxylic acid
(3-chloro-4-methoxyphenyl)methanamine
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In 1-methyl-pyrrolidin-2-one at 60℃; for 16h; |
(3-chloro-4-methoxyphenyl)methanamine
4,7-dichloro-6-nitro-quinazoline
C16H12Cl2N4O3
Conditions | Yield |
---|---|
With triethylamine In isopropyl alcohol | |
Stage #1: (3-chloro-4-methoxyphenyl)methanamine; 4,7-dichloro-6-nitro-quinazoline With triethylamine; N,N-dimethyl-formamide In isopropyl alcohol at 20℃; for 17h; Stage #2: With sodium hydrogencarbonate In water; ethyl acetate |
(3-chloro-4-methoxyphenyl)methanamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: DIEA / propan-1-ol / 4 h / Heating 2: TFA / 1 h / 60 °C View Scheme |
(3-chloro-4-methoxyphenyl)methanamine
7-chloro-6-hydroxy-4-phenyl-1,2,3,4-tetrahydroisoquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 25 percent / acetonitrile / 16 h / Heating 2: 92 percent / H2SO4 / 2 h / Ambient temperature 3: 21 percent / 48percent HBr / 12 h / 100 °C View Scheme |
(3-chloro-4-methoxyphenyl)methanamine
7-chloro-6-methoxy-4-phenyl-1,2,3,4-tetrahydroisoquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 25 percent / acetonitrile / 16 h / Heating 2: 92 percent / H2SO4 / 2 h / Ambient temperature View Scheme |
(3-chloro-4-methoxyphenyl)methanamine
sch 23390
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 25 percent / acetonitrile / 16 h / Heating 2: 92 percent / H2SO4 / 2 h / Ambient temperature 3: 74 percent / formic acid / 4 h / Heating 4: 83 percent / 48percent HBr / 12 h / 100 °C View Scheme |
(3-chloro-4-methoxyphenyl)methanamine
N-methyl-7-chloro-6-methoxy-4-phenyl-1,2,3,4-tetrahydroisoquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 25 percent / acetonitrile / 16 h / Heating 2: 92 percent / H2SO4 / 2 h / Ambient temperature 3: 74 percent / formic acid / 4 h / Heating View Scheme |
Methyl 3-(4-chlorobenzothieno[2, 3-d]pyrimid in-2-yl)propionate
(3-chloro-4-methoxyphenyl)methanamine
methyl 3-[4-(3-chloro-4-methoxybenzylamino)benzothieno-[2,3-d]pyrimidin-2-yl]propionate
Conditions | Yield |
---|---|
In 1-methyl-pyrrolidin-2-one at 110℃; for 5h; |
(3-chloro-4-methoxyphenyl)methanamine
Conditions | Yield |
---|---|
In 1-methyl-pyrrolidin-2-one at 110℃; for 4h; | |
With hydrogen sulfide; dimethyl amine; trichlorophosphate In 1-methyl-pyrrolidin-2-one |
(3-chloro-4-methoxyphenyl)methanamine
4-(aminomethyl)-2-chlorophenol hydrobromide
Conditions | Yield |
---|---|
With water; hydrogen bromide at 133℃; for 4h; |
2,6-dichloropyridine-3-carboxylic acid
(3-chloro-4-methoxyphenyl)methanamine
2-chloro-5-carboxy-6-(3-chloro-4-methoxybenzylamino)pyridine
Conditions | Yield |
---|---|
With 1-methyl-pyrrolidin-2-one; potassium carbonate; copper(I) bromide at 120℃; for 2.5h; |
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