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Cas:118-29-6
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inquiryEnglish name:N-(Hydroxymethyl)phthalimide CAS number:118-29-6 Purity:99% Best quality and Competitive price Specifications N-(Hydroxymethyl)phthalimide White crystal powder 99.0% min. N-(Hydroxymethyl)phth
Cas:118-29-6
Min.Order:1 Kilogram
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inquiryUnique advantages of N-(Hydroxymethyl)phthalimide Cas 118-29-6 Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White crystalline powder Storage:cool dry place Package:25kg/drum Appl
Cas:118-29-6
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inquiryAppearance: white crystalline powder Purity (%, dry): 99 min. Iron ion(wt%): 20ppm max Melting point: 140--145C Appearance:white powder Storage:Warehouse ventilation, away from open flame, high temperature, and antioxidant Package:
high quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
Cas:118-29-6
Min.Order:1 Kilogram
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inquiryN-(Hydroxymethyl)phthalimide Product Name: N-(Hydroxymethyl)phthalimide Molecular Weight: 177.16 CAS NO: 118-29-6 EC NO: 204-241-4 Molecular Form
Cas:118-29-6
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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Cas:118-29-6
Min.Order:1 Kilogram
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Cas:118-29-6
Min.Order:5 Kiloliter
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inquiryProduct Name: N-(Hydroxymethyl)phthalimide Synonyms: oxymethylphthalimide;Phthalimide, N-(hydroxymethyl)-;Phthalimidomethyl alcohol;phthalimidomethylalcohol;4-(Hydroxymethyl)phthalimide, 97%;1H-Isoindole-1,3(2H)-dione, 2-(hydroxymethyl)-;N-Hydroxy
Cas:118-29-6
Min.Order:1 Kilogram
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inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/547.html Product Name N-(Hydroxymethyl)phthalimide CAS No. 118-29
Cas:118-29-6
Min.Order:1 Gram
FOB Price: $22.0
Type:Lab/Research institutions
inquiryHebei Nengqian Chemical Import and Export Co., LTD.. is located in xingtai City, Hebei Province, China. It is a biotechnology enterprise engaged in the research, development, production and sales of animal and plant extracts, cosmetics, pharmaceutica
Cas:118-29-6
Min.Order:1 Gram
FOB Price: $12.0 / 15.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:118-29-6
Min.Order:1 Kilogram
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inquiry1. Product advantages ♦ High purity, all above 98.5%, no impurities after the dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available &diam
Cas:118-29-6
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inquiryProduct Name: N-(Hydroxymethyl)phthalimide Molecular Weight: 177.16 CAS NO: 118-29-6 EC NO:
Hebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car
Cas:118-29-6
Min.Order:1 Metric Ton
FOB Price: $1.0 / 2.0
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inquiryOur Adwantage: 1.We have stock so we can delivery quickly at the very day when receive the payment. 2.Best price, first class service, high successful delivery rate. A discount would be given when you make a large order. 3.High quality gua
Cas:118-29-6
Min.Order:10 Gram
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Cas:118-29-6
Min.Order:1 Kilogram
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inquiryN-(Hydroxymethyl)phthalimide CAS:118-29-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organi
Cas:118-29-6
Min.Order:1 Gram
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:118-29-6
Min.Order:1 Kilogram
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inquiryProduct Detail Minimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,
Cas:118-29-6
Min.Order:20 Metric Ton
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Type:Trading Company
inquiryN-(Hydroxymethyl)phthalimide CAS: 118-29-6 Specification Items Specification Product name N-(Hydroxymethyl)phthalimide CAS# 118-29-6 Appearance
Cas:118-29-6
Min.Order:1 Kilogram
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inquiryPRODUCT DETAILS
Cas:118-29-6
Min.Order:500 Kilogram
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Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:118-29-6
Min.Order:0
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:118-29-6
Min.Order:0 Metric Ton
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:118-29-6
Min.Order:10 Kilogram
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Type:Trading Company
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:118-29-6
Min.Order:1 Gram
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Type:Lab/Research institutions
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Cas:118-29-6
Min.Order:10 Gram
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Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
In water at 100℃; for 4h; | 99% |
In water for 0.0666667h; hydroxymethylation; Heating; ultrasound irradiation; | 97% |
In water for 1.5h; Reflux; | 96% |
Conditions | Yield |
---|---|
With cesium formate In methanol for 18h; Reflux; Inert atmosphere; | 95% |
With water |
phthalimide
formaldehyd
phosphonic acid diethyl ester
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
Conditions | Yield |
---|---|
In 1,1,2,2-tetrachloroethylene at 110℃; for 8h; | 84% |
2-(2-Hydroperoxy-2-methoxy-ethyl)-isoindole-1,3-dione
A
N-methylphthalimide
B
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
C
Methyl formate
D
N-phthaloylglycine methyl ester
Conditions | Yield |
---|---|
In acetonitrile at 0℃; Irradiation; | A 3% B 72% C 79% D 5% |
In acetonitrile at 0℃; Irradiation; other solvents; other phthalimide; | A 3% B 72% C 79% D 5% |
2-(iodomethyl)isoindoline-1,3-dione
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
Conditions | Yield |
---|---|
With dimethyl zinc(II) In n-heptane; dichloromethane at 20℃; for 18h; Inert atmosphere; | 43% |
2-(2-Hydroperoxy-2-methoxy-ethyl)-isoindole-1,3-dione
A
N-methylphthalimide
B
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
C
N-phthaloylglycine methyl ester
Conditions | Yield |
---|---|
In dimethyl sulfoxide Irradiation; | A 15% B 35% C 40% |
2-(iodomethyl)isoindoline-1,3-dione
A
N-methylphthalimide
B
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
C
1,3,4,5-tetrahydro-2,4-benzoxazepine-1,5-dione
Conditions | Yield |
---|---|
With diethylzinc In hexane; dichloromethane at 20℃; for 2h; Inert atmosphere; | A 39% B 14% C 22% |
N-(bromomethyl)phtalimide
diisopropylamine
A
phthalimide
B
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
Conditions | Yield |
---|---|
In benzene for 12h; Heating; Title compound not separated from byproducts; |
methanol
phthalimide DBU salt
A
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
Conditions | Yield |
---|---|
With sodium methylate 1.) electrolysis, current density 0.05 A/cm2, 1.5 h, 2.) electrolysis, current density 0.02 A/cm2, 5 h; Yield given. Multistep reaction. Yields of byproduct given; |
Conditions | Yield |
---|---|
With sodium methylate 1.) electrolysis, current density 0.05 A/cm2, 2 h, 2.) electrolysis, current density 0.02 A/cm2, 5 h; Yield given. Multistep reaction. Yields of byproduct given; |
phthalimide
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
Conditions | Yield |
---|---|
at 100℃; |
Phosmet
isopropyl alcohol
A
phthalimide
B
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
C
N-(methoxymethyl)phthalimide
D
2-<(isopropyloxy)methyl>-isoindole-1,3(2H)-dione
Conditions | Yield |
---|---|
for 15h; UV-irradiation; | A n/a B n/a C n/a D 5 mg |
Phosmet
A
phthalimide
B
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
C
N-(methoxymethyl)phthalimide
Conditions | Yield |
---|---|
In methanol for 7h; Product distribution; Further Variations:; Solvents; UV-irradiation; |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: water / Destillation des entstandenen sauren phthalsauren Methylamins 2: bromine / 160 - 170 °C 3: water View Scheme | |
Multi-step reaction with 2 steps 1: urea / 0.33 h / 140 °C 2: water / 1 h / Reflux View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: bromine / 160 - 170 °C 2: water View Scheme |
N-(chloromethyl)phthalimide
A
N-methylphthalimide
B
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
C
1,3,4,5-tetrahydro-2,4-benzoxazepine-1,5-dione
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium iodide / acetone / 4 h / 20 °C / Darkness 2: diethylzinc / hexane; dichloromethane / 2 h / 20 °C / Inert atmosphere View Scheme |
N-(chloromethyl)phthalimide
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium iodide / acetone / 4 h / 20 °C / Darkness 2: dimethyl zinc(II) / n-heptane; dichloromethane / 18 h / 20 °C / Inert atmosphere View Scheme |
phthalimide
tert-butyl methyl ether
A
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
B
2-(tert-butoxymethyl)isoindoline-1,3-dione
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide at 75℃; for 5h; Sealed tube; Overall yield = 65 %; |
1,3-Dioxo-1,3-dihydro-isoindole-2-carbaldehyde
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
Conditions | Yield |
---|---|
With methanol; sodium tetrahydroborate at 0 - 20℃; Inert atmosphere; Sealed tube; |
1,2,3,4-tetrahydrocarbazole
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
N-(5,6,7,8-tetrahydro-carbazol-3-ylmethyl)-phthalimide
Conditions | Yield |
---|---|
In sulfuric acid for 30h; Ambient temperature; | 100% |
2,3-dimethylindole
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
N-(2,3-dimethyl-indol-5-ylmethyl)-phthalimide
Conditions | Yield |
---|---|
In sulfuric acid for 30h; Ambient temperature; | 98% |
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
2,8-Dimethyl-4-phenoxathiinessigsaeure-10,10-dioxid
2,8-dimethyl-4-(carboxymethyl)-6-(phthalimidomethyl)-phenoxathiin S-dioxide
Conditions | Yield |
---|---|
With sulfuric acid for 168h; Ambient temperature; | 98% |
Conditions | Yield |
---|---|
With trifluoromethylsulfonic anhydride In trifluoroacetic acid | 98% |
Conditions | Yield |
---|---|
Stage #1: 2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione; MINOCYCLINE With hydrogenchloride; sulfuric acid; trifluoroacetic acid at 40 - 50℃; Inert atmosphere; Stage #2: With monomethanolamine | 97% |
Conditions | Yield |
---|---|
With sulfuric acid; hydrogen bromide In water at 0 - 70℃; for 17.25h; | 96.4% |
With sulfuric acid; hydrogen bromide In water at 70℃; Cooling with ice; | 95% |
With phosphorus tribromide In dichloromethane | 80% |
2-methyl-1H-indole
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
2-methyl-5-(phtalimidomethyl)indole
Conditions | Yield |
---|---|
In sulfuric acid for 30h; Ambient temperature; | 96% |
Conditions | Yield |
---|---|
With tris(2,4-pentanedionato)ruthenium(III); methanesulfonic acid; hydrogen; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine] at 130℃; under 11251.1 Torr; for 18h; Autoclave; | 96% |
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
Conditions | Yield |
---|---|
Stage #1: 2,3,3-trimethyl-3H-indolium With sulfuric acid for 0.333333h; Inert atmosphere; Reflux; Stage #2: 2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione for 70h; | 95.8% |
Conditions | Yield |
---|---|
With sulfuric acid In tetrahydrofuran at 20℃; Cooling with ice; | 95% |
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
2-bromo-5-nitrotoluene
2-[(2-bromo-3-methyl-5-nitrophenyl)methyl]-2,3-dihydro-1H-isoindole-1,3-dione
Conditions | Yield |
---|---|
Stage #1: 2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione With trifluorormethanesulfonic acid at 0℃; for 0.333333h; Tcherniak-Einhorn reaction; Stage #2: 2-bromo-5-nitrotoluene at 0 - 20℃; for 18h; Tcherniak-Einhorn reaction; | 94% |
Stage #1: 2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione With trifluorormethanesulfonic acid at 0℃; for 0.333333h; Stage #2: 2-bromo-5-nitrotoluene at 0 - 20℃; for 18h; | 94% |
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
N-(chloromethyl)phthalimide
Conditions | Yield |
---|---|
With thionyl chloride In dichloromethane; N,N-dimethyl-formamide at 20℃; for 2.5h; | 93% |
With trichlorophosphate | |
With hydrogenchloride at 50℃; |
2,3-dimethyl-5-methoxyindole
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
2,3-dimethyl-5-methoxy-6-(phtalimidomethyl)indole
Conditions | Yield |
---|---|
In sulfuric acid for 30h; Ambient temperature; | 93% |
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
ethyl acetoacetate
ethyl 2-[(1,3-dioxo-2,3-dihydro-1H-isoindol-2-yl)methyl]-3-oxobutanoate
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate at 20℃; for 24h; | 93% |
With boron trifluoride diethyl etherate at 0 - 20℃; for 0.5h; |
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
1,2-Dichloroethylene
2-chloro-3-phthalimido-propionaldehyde
Conditions | Yield |
---|---|
With sulfuric acid | 93% |
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
1-methyl-1'-forrnyl-spiro[piperidine-4,3'-(2H)-indole]
5'-(1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl)-1'-formyl-1-methyl-spiro[piperidine-4,3'-(2H)-indole]
Conditions | Yield |
---|---|
With sulfuric acid Tscherniac-Einhorn reaction; | 93% |
Stage #1: 2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione; 1-methyl-1'-forrnyl-spiro[piperidine-4,3'-(2H)-indole] With sulfuric acid at 5 - 20℃; Inert atmosphere; Stage #2: With sodium carbonate In water pH=10; | 93% |
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid Ambient temperature; | 92% |
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
3-benzyl-2,3-dihydropyrimidin-4(1H)-one
diamide
Conditions | Yield |
---|---|
With triphenylphosphine In N,N-dimethyl-formamide | A 0.3 % Chromat. B 92% |
Conditions | Yield |
---|---|
With sulfuric acid for 2h; Ambient temperature; | 90% |
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
9-methoxy-7H-furo[3,2-g][1]benzopyran-7-one
A
5,5'-Bis-N-Phthalimidomethyl-8-methoxypsoralen
B
5-N-Phthalimidomethyl-8-methoxypsoralen
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid; trifluoroacetic acid In dichloromethane for 6h; Ambient temperature; | A 90% B n/a |
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate | 90% |
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
(S)-10-hydroxycamptothecin
C29H21N3O7
Conditions | Yield |
---|---|
With sulfuric acid at 0 - 20℃; for 12h; | 90% |
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
tetramethylammonium trifluoromethylselenate(0)
Conditions | Yield |
---|---|
With calcium chloride In acetonitrile at 80℃; for 2h; Time; Inert atmosphere; Sealed tube; Glovebox; | 90% |
Conditions | Yield |
---|---|
With sulfuric acid In water at -5 - 20℃; for 24h; | 90% |
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
acrylonitrile
N-(acryloylamino-methyl)-phthalimide
Conditions | Yield |
---|---|
With sulfuric acid 0 deg C, than 18 deg C., 20 h; | 89.7% |
With sulfuric acid; acetic acid |
7-methoxy-2,3-dimethyl-1H-indole
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
2-(7-Methoxy-2,3-dimethyl-1H-indol-6-ylmethyl)-isoindole-1,3-dione
Conditions | Yield |
---|---|
In sulfuric acid for 30h; Ambient temperature; | 89% |
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
2,8-dimethylphenoxathiin 10,10-dioxide
2,8-dimethyl-4,6-bis(phthalimidomethyl)-phenoxathiin-10,10-dioxide
Conditions | Yield |
---|---|
With sulfuric acid for 168h; Ambient temperature; | 89% |
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione
D-glucal triacetate
phthalimidomethyl 4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In toluene at -20℃; Ferrier rearrangement; | 89% |
With niobium pentachloride In tetrahydrofuran for 0.833333h; Ferrier rearrangement; Heating; | 80% |
With montmorillonite K-10 for 0.166667h; Ferrier rearrangement; microwave irradiation; | 77% |
With boron trifluoride diethyl etherate In benzene at 20℃; for 1.25h; | 76.3% |
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