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Name: nitenpyram CAS no. : 120738-89-8 Molecular formula: C11H15ClN4O2 Molecular weight:270.7154 Product Quality 12 years of chemical raw materials Mature operation of the industry System stability Data storage Security without vulnerabil
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inquirycas 120738-89-8 Nitenpyram powder Product Name: Nitenpyram CAS: 120738-89-8 MF: C11H15ClN4O2 MW: 270.72 Appearance:white Storage:room Package:drum Application:Artemisia annua is used as anti
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inquiryProduct name: Nitenpyram CAS No.: 120738-89-8 Molecule Formula:C11H15ClN4O2 Molecule Weight:270.72 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS
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Product Name: Nitenpyram Synonyms: (e)-n-((6-chloro-3-pyridinyl)methyl)-n-ethyl-n'-methyl-2-nitro-1,1-ethenediamine;(E)-N-(6-chloro-3-pyridylmethyl )-N-ethyl-N'-methyl-2-nitrovinylidenediamine;N-((6-chloro-3-pyridinyl)methyl)-N-ethyl-N'
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1. GMP AVALIABLE ; 2. IN STOCK 3. FAST REPLY QUALIFED ; EFFICIENCY; RESPONSIBLE Appearance:white crystalline powder Storage:in cool Package:as request Application:active pharmaceutical ingredient Transportation:Air / SEA BOTH OK Port:any po
high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
methylamine
nitenpyram
Conditions | Yield |
---|---|
at 3 - 7℃; | 58% |
N-(6-chloro-pyridin-3-yl)methyl-N-ethylamine
2-methylamino-2-methylthio-1-nitroethene
nitenpyram
Conditions | Yield |
---|---|
With silver(I) acetate In ethanol at 25℃; | 38.1% |
N-((6-chloropyridin-3-yl)methyl)-N-ethyl-1-(methylthio)-2-nitroethenamine
methylamine
nitenpyram
Conditions | Yield |
---|---|
In ethanol Reflux; | 29.5% |
In ethanol at 0℃; | 27% |
In ethanol at 0℃; | 19.1% |
N-(6-chloro-pyridin-3-yl)methyl-N-ethylamine
nitenpyram
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: chloroform / 2 - 7 °C 2: 3 - 7 °C View Scheme | |
Multi-step reaction with 2 steps 1: ethanol / Reflux 2: ethanol / 0 °C View Scheme | |
Multi-step reaction with 2 steps 1: ethanol / Reflux 2: ethanol / Reflux View Scheme | |
Multi-step reaction with 2 steps 1: ethanol / 8 h / Reflux 2: ethanol / 0 °C View Scheme |
2-chloro-5-(chloromethyl)pyridine
nitenpyram
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 2: chloroform / 2 - 7 °C 3: 3 - 7 °C View Scheme | |
Multi-step reaction with 3 steps 1: acetonitrile / 3.5 h / 0 °C 2: ethanol / Reflux 3: ethanol / 0 °C View Scheme | |
Multi-step reaction with 2 steps 1: acetonitrile / 0 - 5 °C 2: silver(I) acetate / ethanol / 25 °C View Scheme |
thiocyanogen
nitenpyram
N-((6-chloropyridin-3-yl)methyl)-N-ethyl-2-imino-3-methyl-5-nitro-2,3-dihydrothiazol-4-amine
Conditions | Yield |
---|---|
With piperidine In dichloromethane at -15 - 20℃; for 1.5h; | 84% |
formaldehyd
ethyl γ-aminobutyrate hydrochloride
nitenpyram
4-[(4Z)-4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl] butyric acid ethyl ester
Conditions | Yield |
---|---|
With triethylamine In ethanol at 65℃; for 0.416667h; Microwave irradiation; | 78.8% |
formaldehyd
glycine 1-propyl ester hydrochloride
nitenpyram
2-[(4Z)-4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl] acetic acid propyl ester
Conditions | Yield |
---|---|
With triethylamine In ethanol at 65℃; for 0.416667h; Microwave irradiation; | 78.7% |
formaldehyd
methyl 3-aminopropanoate hydrochloride
nitenpyram
3-[(4Z)-4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl] propionic acid methyl ester
Conditions | Yield |
---|---|
With triethylamine In ethanol at 65℃; for 0.416667h; Microwave irradiation; | 78.2% |
formaldehyd
methyl γ-aminobutyrate hydrochloride
nitenpyram
4-[(4Z)-4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl] butyric acid methyl ester
Conditions | Yield |
---|---|
With triethylamine In ethanol at 65℃; for 0.416667h; Microwave irradiation; | 78.1% |
formaldehyd
glycine isopropyl ester hydrochloride
nitenpyram
2-[(4Z)-4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl] acetic acid 1-methylethyl ester
Conditions | Yield |
---|---|
With triethylamine In ethanol at 65℃; for 0.416667h; Microwave irradiation; | 77.9% |
formaldehyd
ethyl β-alaninate hydrochloride
nitenpyram
3-[(4Z)-4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl] propionic acid ethyl ester
Conditions | Yield |
---|---|
With triethylamine In ethanol at 65℃; for 0.416667h; Microwave irradiation; | 76.9% |
formaldehyd
nitenpyram
4-[(4Z)-4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl] butyric acid 1-methylethyl ester
Conditions | Yield |
---|---|
With triethylamine In ethanol at 65℃; for 0.416667h; Microwave irradiation; | 76.4% |
formaldehyd
4-aminobutyric acid propyl ester hydrochloride
nitenpyram
4-[(4Z)-4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl] butyric acid propyl ester
Conditions | Yield |
---|---|
With triethylamine In ethanol at 65℃; for 0.416667h; Microwave irradiation; | 75.7% |
formaldehyd
β-alanine propyl ester hydrochloride
nitenpyram
3-[(4Z)-4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl] propionic acid propyl ester
Conditions | Yield |
---|---|
With triethylamine In ethanol at 65℃; for 0.416667h; Microwave irradiation; | 75.5% |
formaldehyd
C6H13NO2*ClH
nitenpyram
2-[(4Z)-4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl] acetic acid 1-methylpropyl ester
Conditions | Yield |
---|---|
With triethylamine In ethanol at 65℃; for 0.416667h; Microwave irradiation; | 75.1% |
formaldehyd
i-propyl β-alaninate hydrochloride
nitenpyram
3-[(4Z)-4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl] propionic acid 1-methylethyl ester
Conditions | Yield |
---|---|
With triethylamine In ethanol at 65℃; for 0.416667h; Microwave irradiation; | 74.4% |
formaldehyd
glycine n-butyl ester hydrochloride
nitenpyram
2-[(4Z)-4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl] acetic acid butyl ester
Conditions | Yield |
---|---|
With triethylamine In ethanol at 65℃; for 0.416667h; Microwave irradiation; | 74.2% |
formaldehyd
C7H15NO2*ClH
nitenpyram
3-[(4Z)-4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl] propionic acid 2-methylpropyl ester
Conditions | Yield |
---|---|
With triethylamine In ethanol at 65℃; for 0.416667h; Microwave irradiation; | 73.7% |
formaldehyd
glycine isobutyl ester; hydrochloride
nitenpyram
2-[(4Z)-4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl] acetic acid 2-methylpropyl ester
Conditions | Yield |
---|---|
With triethylamine In ethanol at 65℃; for 0.416667h; Microwave irradiation; | 73.6% |
formaldehyd
nitenpyram
3-[(4Z)-4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl] propionic acid butyl ester
Conditions | Yield |
---|---|
With triethylamine In ethanol at 65℃; for 0.416667h; Microwave irradiation; | 73.1% |
formaldehyd
C7H15NO2*ClH
nitenpyram
3-[(4Z)-4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl] propionic acid 1-methylpropyl ester
Conditions | Yield |
---|---|
With triethylamine In ethanol at 65℃; for 0.416667h; Microwave irradiation; | 72.8% |
formaldehyd
nitenpyram
3-[(4Z)-4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl] propionic acid 1,1-dimethylethyl ester
Conditions | Yield |
---|---|
With triethylamine In ethanol at 65℃; for 0.416667h; Microwave irradiation; | 72.6% |
formaldehyd
glycine ethyl ester hydrochloride
nitenpyram
2-[(4Z)-4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl] acetic acid methyl ester
Conditions | Yield |
---|---|
With triethylamine In ethanol at 65℃; for 0.416667h; Microwave irradiation; | 72.5% |
formaldehyd
glycine ethyl ester hydrochloride
nitenpyram
2-[(4Z)-4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl] acetic acid ethyl ester
Conditions | Yield |
---|---|
With triethylamine In ethanol at 65℃; for 0.416667h; Microwave irradiation; | 72% |
formaldehyd
glycine tert-butyl ester hydrochloride
nitenpyram
2-[(4Z)-4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl] acetic acid 1,1-dimethylethyl ester
Conditions | Yield |
---|---|
With triethylamine In ethanol at 65℃; for 0.416667h; Microwave irradiation; | 71.5% |
Conditions | Yield |
---|---|
Stage #1: nitenpyram With sodium hydride In N,N-dimethyl-formamide at 20℃; for 1h; Cooling with ice; Stage #2: monomethyl oxalyl chloride In N,N-dimethyl-formamide at 20℃; for 5h; | 70.5% |
Stage #1: nitenpyram With sodium hydride In N,N-dimethyl-formamide at 20℃; for 1h; Cooling with ice; Stage #2: monomethyl oxalyl chloride In N,N-dimethyl-formamide at 20℃; for 5h; | 61.1% |
furfural
nitenpyram
N-((6-chloropyridin-3-yl)methyl)-N-ethyl-3-(furan-2-yl)-N'-methyl-2-nitroacrylamidine
Conditions | Yield |
---|---|
With hydrogenchloride In water; acetonitrile at 20℃; for 6h; | 70.1% |
hydrogenchloride In water; acetonitrile at 20℃; for 6h; | 70.1% |
Malondialdehyde
nitenpyram
Conditions | Yield |
---|---|
hydrogenchloride In water; acetonitrile at 20℃; | 56% |
Malondialdehyde
nitenpyram
Conditions | Yield |
---|---|
hydrogenchloride In water; acetonitrile at 20℃; | 56% |
butanedial
nitenpyram
N-((6-chloropyridin-3-yl)methyl)-N-ethyl-2-methyl-4-nitro-8-oxa-2-aza-bicyclo[3.2.1]oct-3-en-3-amine
Conditions | Yield |
---|---|
hydrogenchloride In water; acetonitrile at 20℃; | 40% |
hydrogenchloride In water; acetonitrile at 20℃; | 40% |
thiazole-5-carboxaldehyde
nitenpyram
Conditions | Yield |
---|---|
Stage #1: thiazole-5-carboxaldehyde; nitenpyram With hydrogenchloride In acetonitrile at 20℃; for 6h; Stage #2: With hydrogen; nickel In methanol at 20℃; | 34% |
Conditions | Yield |
---|---|
In water at 20℃; | 32% |
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