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Cas:70258-18-3
Min.Order:250 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryDayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
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Type:Lab/Research institutions
inquiryItems Standard Result Assay 99.9%min 99.9% Hangzhou Dingyan Chem is a leading manufacturer and supplier of che
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Min.Order:1 Kilogram
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Type:Trading Company
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Cas:70258-18-3
Min.Order:0 Metric Ton
Negotiable
Type:Manufacturers
inquiryProduct Description Product Name 2-Chloro-5-chloromethylpyridine (CCPM) CAS No. 70258-18-3 Appearance White powder Assay ≥99% Capacity 1000mt/year Min.packing
Cas:70258-18-3
Min.Order:1 Gram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryISO Specifications 2-Chloro-5-Chloro-Methyl Pyridine Largest exporter to Indian/South American/European Market Stable supply Appearance:Colorless crystalloid Storage:dry environment Package:250kg/drum ,according to your requirements
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Min.Order:2 Kilogram
Negotiable
Type:Trading Company
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Min.Order:1 Kilogram
Negotiable
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Cas:70258-18-3
Min.Order:1
Negotiable
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Type:Manufacturers
inquiryOur company was built in 2009 with an ISO certificate.In the past 6 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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Type:Lab/Research institutions
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Min.Order:10 Gram
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Type:Trading Company
inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developmen
Cas:70258-18-3
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Type:Trading Company
inquiryProduct Name: 2-Chloro-5-chloromethylpyridine CAS No.: 70258-18-3 EINECS: 615-091-8 Molecular Formula: C6H5Cl2N Molecular Weight: 162.02 Appearance: white crystal powder Application: Pharmaceutical Intermediates Appearance: white powd
Cas:70258-18-3
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Other
inquiryAppearance:White crystals Storage:ln stock Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Any port in china
Cas:70258-18-3
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
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Negotiable
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inquiry2-Chloro-5-chloromethylpyridine CAS:70258-18-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality o
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Min.Order:1 Gram
Negotiable
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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Min.Order:1 Kilogram
Negotiable
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Min.Order:1 Kilogram
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inquiry2-Chloro-5-chloromethylpyridine CAS: 70258-18-3 Specification product name 2-chloro-5-chloromethylpyridine (ccpm) cas no. 70258-18-3 appearance white powder assay ≥99% capacity
Cas:70258-18-3
Min.Order:1 Kilogram
Negotiable
Type:Other
inquiryTriumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Business Custom Synthesis: Trading(Raw Mater
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Type:Lab/Research institutions
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low price high quality high purity good sevice stock Appearance:white Storage:Preserve In Well-Closed, Light-Resistant and Tight Containers. Store In Cool & Dry Place Package:1g,5g,10g...1kg,5kg...more Application:Pharmaceutical interme
Cas:70258-18-3
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry2,-chloro-2-(chloromethyl)-4-cyanobutyraldehyde
2-chloro-5-(chloromethyl)pyridine
Conditions | Yield |
---|---|
With phosgene In toluene at 50℃; for 6h; Temperature; | 97% |
In chlorobenzene at 105 - 110℃; for 0.283333h; Temperature; | 79.5% |
5-(hydroxymethyl)pyridin-2-ol
2-chloro-5-(chloromethyl)pyridine
Conditions | Yield |
---|---|
With phosphorus pentachloride In chloroform; water; trichlorophosphate | 95% |
2-chloro-5-methylpyridine
2-chloro-5-(chloromethyl)pyridine
Conditions | Yield |
---|---|
With chlorine at 115 - 120℃; for 5.5h; Temperature; | 93.5% |
With chlorine at 120℃; under 3750.38 Torr; Temperature; Pressure; Green chemistry; | 93.2% |
With 2,2'-azobis(isobutyronitrile); chlorine In dichloromethane at 120℃; under 7500.75 - 15001.5 Torr; for 1h; | 70% |
2-chloro-5-(chloromethyl)pyridine
Conditions | Yield |
---|---|
With phosgene In N,N-dimethyl-formamide; toluene at 20 - 30℃; for 4h; Temperature; | 91.2% |
2-chloro-5-(Trichloromethyl)-pyridine
2-chloro-5-(chloromethyl)pyridine
Conditions | Yield |
---|---|
With ammonium hydroxide; 5%-palladium/activated carbon; hydrogen In acetic acid methyl ester; water at 55 - 60℃; under 6000.6 Torr; for 7h; Reagent/catalyst; Pressure; Solvent; Temperature; Autoclave; | 88.6% |
1,3,5-trichloro-2,4,6-triazine
2,-chloro-2-(chloromethyl)-4-cyanobutyraldehyde
2-chloro-5-(chloromethyl)pyridine
Conditions | Yield |
---|---|
With N,N-dimethyl-formamide In toluene at 90 - 100℃; for 2.5h; Concentration; Temperature; Solvent; Reagent/catalyst; | 85.8% |
tert.-butyl lithium
2-chloro-5-(4,4, 5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine
A
2-chloro-5-(chloromethyl)pyridine
C
1-Methyl-4-((R)-2-methyl-propane-2-sulfinyl)-benzene
Conditions | Yield |
---|---|
With zinc(II) chloride In tetrahydrofuran; toluene; pentane at -78 - 20℃; for 22h; Inert atmosphere; | A 25% B 8% C 69% |
3-Methylpyridine
2-chloro-5-(chloromethyl)pyridine
Conditions | Yield |
---|---|
With chlorine at 250 - 282℃; for 0.25h; Reagent/catalyst; Inert atmosphere; | 51% |
Multi-step reaction with 3 steps 1: sodium amide / ethanol / 2.17 h / 66 °C / Reflux 2: methyl nitrite; hydrogenchloride / methanol / 5 h / 10 - 12 °C 3: methyl nitrite; hydrogenchloride / methanol / 5 h / 10 - 12 °C View Scheme |
2-Chloro-5-hydroxymethylpyridine
2-chloro-5-(chloromethyl)pyridine
Conditions | Yield |
---|---|
With thionyl chloride In dichloromethane for 3h; | |
With thionyl chloride In chloroform | |
With pyridine; thionyl chloride |
6-Chloronicotinic acid methyl ester
2-chloro-5-(chloromethyl)pyridine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: DIBAL-H / tetrahydrofuran; hexane / 1 h / 0 °C 2: SOCl2 / CH2Cl2 / 3 h View Scheme | |
Multi-step reaction with 2 steps 1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 20 °C 2: thionyl chloride / dichloromethane / 2 h View Scheme | |
Multi-step reaction with 2 steps 1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere 2: thionyl chloride / dichloromethane / 2 h / Inert atmosphere View Scheme |
2-chloro-5-chloromethylpyridine chydrochloride
2-chloro-5-(chloromethyl)pyridine
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In dichloromethane; water |
6-Chloro-3-pyridinecarboxylic acid
2-chloro-5-(chloromethyl)pyridine
Conditions | Yield |
---|---|
With phosphorus pentachloride; trichlorophosphate | |
Multi-step reaction with 2 steps 1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 0 °C / Reflux 2: thionyl chloride / dichloromethane / 1 h / Reflux View Scheme | |
Multi-step reaction with 2 steps 1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 0 - 20 °C / Reflux 2: thionyl chloride / dichloromethane / 1 h / 20 °C / Reflux View Scheme |
2,-chloro-2-(chloromethyl)-4-cyanobutyraldehyde
phosphorus pentachloride
2-chloro-5-(chloromethyl)pyridine
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In hydrogenchloride; N,N-dimethyl-formamide |
4-chloro-4-chloromethyl-5-oxopentamide
2-chloro-5-(chloromethyl)pyridine
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide |
oxalyl dichloride
2-chloro-5-acetaminomethylpyridine
2-chloro-5-(chloromethyl)pyridine
Conditions | Yield |
---|---|
In N-methyl-acetamide; acetonitrile |
(6-methoxypyridin-3-yl)methanol
N,N-dibutylformamide
2-chloro-5-(chloromethyl)pyridine
Conditions | Yield |
---|---|
With nitrogen; sodium carbonate In water; toluene |
5-(hydroxymethyl)-1,2-dihydropyridin-2-one
2-chloro-5-(chloromethyl)pyridine
Conditions | Yield |
---|---|
With phosphorus pentachloride; sodium carbonate; trichlorophosphate In ethyl acetate |
2-methoxy-5-bis-(methoxy)methyl-pyridine
phosphorus pentachloride
2-chloro-5-(chloromethyl)pyridine
Conditions | Yield |
---|---|
With sodium hydroxide; trichlorophosphate |
2-Chloro-5-hydroxymethylpyridine
1,2-dichloro-ethane
2-chloro-5-(chloromethyl)pyridine
Conditions | Yield |
---|---|
With thionyl chloride; sodium bicarbonate In chloroform; water |
2-((6-chloropyridin-3-yl)oxy)acetic acid
2-chloro-5-(chloromethyl)pyridine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: methanol / 16 h / 20 °C / Inert atmosphere 2: triphenylphosphine; tetrachloromethane / acetonitrile / 12 h / 20 °C / Inert atmosphere View Scheme |
(5-methyl-pyridin-2-yl)amine
2-chloro-5-(chloromethyl)pyridine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: methyl nitrite; hydrogenchloride / methanol / 5 h / 10 - 12 °C 2: methyl nitrite; hydrogenchloride / methanol / 5 h / 10 - 12 °C View Scheme |
2-chloro-5-(chloromethyl)pyridine
ethylenediamine
N'-((6-chloropyridin-3-yl)methyl)ethane-1,2-diamine
Conditions | Yield |
---|---|
100% | |
100% | |
With sodium hydroxide In acetonitrile at 20℃; for 24h; | 99% |
pyrrolidine
2-chloro-5-(chloromethyl)pyridine
2-chloro-5-(pyrrolidin-1-ylmethyl)pyridine
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile for 3.5h; Reflux; | 100% |
With potassium carbonate In acetonitrile Heating; | 96% |
2-chloro-5-(chloromethyl)pyridine
N-[3-(4-t-butylphenyl)-2,2-dimethylpropyl]-6-chloro-N-methyl-3-pyridylmethylamine
Conditions | Yield |
---|---|
With potassium carbonate In DMF (N,N-dimethyl-formamide) at 50℃; for 8h; | 100% |
2-chloro-5-(chloromethyl)pyridine
Conditions | Yield |
---|---|
With triethylamine In N,N-dimethyl-formamide at 60℃; for 5.5h; Inert atmosphere; | 100% |
2-chloro-5-(chloromethyl)pyridine
cis-13-1,4,7,10-tetraazatetracyclo<5.5.2.04,14010,13>tetradecane
Conditions | Yield |
---|---|
With sodium iodide In acetonitrile at 92℃; for 20 - 60h; | 99% |
2-chloro-5-(chloromethyl)pyridine
methylamine
1-(6-chloropyridin-3-yl)-N-methylmethanamine
Conditions | Yield |
---|---|
Stage #1: methylamine In toluene at -5 - 5℃; Large scale; Stage #2: 2-chloro-5-(chloromethyl)pyridine In toluene at -5 - 2℃; Large scale; | 98.5% |
In water at 62℃; under 1650.17 Torr; for 1h; Temperature; Pressure; | 97.7% |
In water at 60℃; for 6h; | 95.6% |
2-chloro-5-(chloromethyl)pyridine
Kryptofix 21
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In acetonitrile Reflux; | 98% |
2-chloro-5-(chloromethyl)pyridine
1,4,10,13-tetraoxa-7,16-diazacyclooctadecane
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In acetonitrile Reflux; | 98% |
2-chloro-5-(chloromethyl)pyridine
N-(2,2-difluoroethyl)prop-2-en-1-amine
N-[(6-chloropyridin-3-yl)methyl]-N-(2,2-difluoroethyl)prop-2-en-1-amine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine at 70℃; for 16h; | 97.9% |
Conditions | Yield |
---|---|
With N,N,N',N'-tetramethylguanidine In dichloromethane at 10 - 45℃; for 15h; Temperature; Solvent; Reagent/catalyst; Large scale; Green chemistry; | 97.6% |
2-thiazolylamine
2-chloro-5-(chloromethyl)pyridine
3-(6-chloro-pyridin-3-ylmethyl)-3H-thiazol-2-ylideneamine
Conditions | Yield |
---|---|
In isopropyl alcohol for 40h; Heating; | 97% |
2-chloro-5-(chloromethyl)pyridine
dimethyl amine
N,N-dimethyl-6-chloro-nicotinamide
Conditions | Yield |
---|---|
In tetrahydrofuran; dichloromethane at 0 - 20℃; | 97% |
(S)‐2‐nitro‐6,7‐dihydro‐5H‐imidazo[2,1‐b][1,3]oxazin‐6‐ol
2-chloro-5-(chloromethyl)pyridine
(6S)-6-[(6-chloro-3-pyridinyl)methoxy]-2-nitro-6,7-dihydro-5H-imidazo[2,1-b][1,3]oxazine
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 5 - 20℃; | 97% |
With sodium hydride In N,N-dimethyl-formamide; mineral oil at 5 - 20℃; for 16h; | 97% |
With sodium hydride In N,N-dimethyl-formamide at 5 - 20℃; |
2-chloro-5-(chloromethyl)pyridine
sodium cyanide
(6-chloro-pyridin-3-yl)-acetonitrile
Conditions | Yield |
---|---|
In ethanol; water at 0 - 100℃; for 20h; | 96% |
With potassium iodide In ethanol; water at 85℃; for 5h; | 45.6% |
In ethanol; water for 10h; Heating; |
2-chloro-5-(chloromethyl)pyridine
Conditions | Yield |
---|---|
With sodium azide In ethanol for 6h; Reflux; | 95% |
With sodium azide In ethanol Reflux; | 95% |
With sodium azide In ethanol Heating; | |
With sodium azide In ethanol Reflux; | |
With sodium azide In ethanol Reflux; |
N-methylcyclohexylamine
2-chloro-5-(chloromethyl)pyridine
(6-chloro-pyridin-3-ylmethyl)-cyclohexyl-methyl-amine
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 80℃; for 20h; | 95% |
tert-butyl 2,7-diazaspiro[3.5]nonane-7-carboxylate hydrochloride
2-chloro-5-(chloromethyl)pyridine
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 70℃; for 16h; | 95% |
2-chloro-5-(chloromethyl)pyridine
tert-butyl (1R,5S)-3,8-diazabicyclo[3.2.1]octane-3-carboxylate
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 70℃; for 16h; | 95% |
2-aminopyridine
2-chloro-5-(chloromethyl)pyridine
ethyl trifluoroacetate,
N-[1-[(6-chloro-3-pyridinyl)methyl]-2(1H)-pyridinylidene]-2,2,2-trifluoro-acetamide
Conditions | Yield |
---|---|
Stage #1: 2-aminopyridine; ethyl trifluoroacetate, With sodium methylate In methanol; N,N-dimethyl-formamide at 20 - 25℃; for 1h; Stage #2: 2-chloro-5-(chloromethyl)pyridine In N,N-dimethyl-formamide at 60℃; for 3.25h; Temperature; Solvent; Reagent/catalyst; | 94.7% |
Stage #1: 2-aminopyridine; ethyl trifluoroacetate, In N,N-dimethyl-formamide; toluene at 60 - 65℃; for 8h; Stage #2: 2-chloro-5-(chloromethyl)pyridine With potassium carbonate In N,N-dimethyl-formamide; toluene at 60 - 65℃; for 15h; Solvent; | 81.2% |
2-chloro-5-(chloromethyl)pyridine
sodium thiomethoxide
2-chloro-5-[(methylthio)methyl]-pyridine
Conditions | Yield |
---|---|
In ethanol | 94% |
In ethanol at 20℃; | 94% |
In methanol at 50℃; for 20h; Solvent; Temperature; |
2-chloro-5-(chloromethyl)pyridine
potassium ethyl xanthogenate
S-[(6-chloropyridin-3-yl)methyl] O-ethyl carbonodithioate
Conditions | Yield |
---|---|
In acetone Inert atmosphere; | 94% |
In acetone at 23℃; for 16h; Inert atmosphere; stereoselective reaction; | 94% |
4-ethylpiperazine
2-chloro-5-(chloromethyl)pyridine
5-((4-ethylpiperazin-1-yl)methyl)-6-methylpyridin-2-amine
Conditions | Yield |
---|---|
at 60 - 70℃; for 2h; Time; Green chemistry; | 94% |
2-chloro-5-(chloromethyl)pyridine
potassium phtalimide
((2-chloro-5-pyridinyl)methyl)isoindol-1,3-dione
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; for 5h; | 93.3% |
In N,N-dimethyl-formamide at 20℃; | 19.5 g |
2-chloro-5-(chloromethyl)pyridine
5-(ethoxycarbonyl)-4-(4-methoxyphenyl)-6-methyl-3,4-dihydropyrimidin-2(1H)-thione
ethyl 1-[1-(6-chloropyridin-3-yl-methyl)-2-(6-chloropyridin-3-yl-methylthio)-6-(4-methoxyphenyl)-4-methyl-1,6-dihydropyrimidin-5-yl]carboxylate
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 20℃; | 93% |
2-chloro-5-(chloromethyl)pyridine
nitroguanidine
ethylenediamine
1-(6-chloronicotinyl)-2-nitroiminoimidazoline
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol; water at 50℃; for 3h; pH=4 - 5; Reagent/catalyst; Temperature; pH-value; Ionic liquid; | 93% |
2-chloro-5-(chloromethyl)pyridine
methyl N-cyanoacetimidate
methylamine
Conditions | Yield |
---|---|
Stage #1: 2-chloro-5-(chloromethyl)pyridine; methylamine In toluene at 3 - 25℃; for 6h; Large scale; Stage #2: methyl N-cyanoacetimidate With ethanol In toluene at 35℃; for 4h; Temperature; Large scale; | 93% |
2-chloro-5-(chloromethyl)pyridine
(6-chloro-pyridin-3-yl)-acetonitrile
Conditions | Yield |
---|---|
In ethanol; water at 50℃; for 20h; | 92% |
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