Product name: N-Methylcyclohexylamine Cas No: 100-60-7 Assay: 99%min Hangzhou Verychem Science And Technology Co. Ltd. was set up in year 2004, it’s a young but fast growing company. In the twe
Cas:100-60-7
Min.Order:1 Kilogram
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inquiryDayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:100-60-7
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:100-60-7
Min.Order:1 Kilogram
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inquiryProduct description: Product name N-Methylcyclohexylamine CAS number 100-60-7 Assay ≥99% Appearance Colorless transparent liquid Capacity 500mt/year Application Pharmaceutica
Cas:100-60-7
Min.Order:100 Gram
FOB Price: $12.0
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inquiryProperties N-Methylcyclohexylamine CAS100-60-7 is a kind of colorless transparent liquid, with melting point −9-−7 °C(lit.),boiling point 149 °C(lit.),can soluble in water. It is mainly used for dyestuffs area and drug interme
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Cas:100-60-7
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inquiryTIANFUCHEM--100-60-7--N-Methylcyclohexylamine in stock Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable business rela
Cas:100-60-7
Min.Order:1 Metric Ton
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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Min.Order:10 Gram
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:100-60-7
Min.Order:10 Kilogram
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inquiryProduct Name N-Methylcyclohexylamine Synonyms N-Cyclohexylmethylamine CAS: 100-60-7 MF: C7H16N MW: - EINECS: -
Cas:100-60-7
Min.Order:5 Metric Ton
FOB Price: $1.0 / 2.0
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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Min.Order:1 Kilogram
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inquiryN-Methylcyclohexylamine CAS: 100-60-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic in
Cas:100-60-7
Min.Order:1 Gram
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:100-60-7
Min.Order:1 Kilogram
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Min.Order:0
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inquiryhangzhou zeerrui chemical co., ltd. located in lingang industrial areas, our plant covers an area of 6000 square meters.zeerrui dedicated to the development, production and marketing of chemicals. we have earned ourselves a good reputation at home
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Min.Order:200 Liter
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
Cas:100-60-7
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:100-60-7
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:100-60-7
Min.Order:100 Gram
FOB Price: $100.0 / 2000.0
Type:Lab/Research institutions
inquiryProduct name: N-Methylcyclohexylamine CAS No.:100-60-7 Molecule Formula:C7H16N Molecule Weight:114.21 Purity: 99.0% Package: 170kg/drum Description:Colorless to yellowish transparent oily liquid Manufacture Standards:Enterprise Standa
Cas:100-60-7
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:100-60-7
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
N-Methylcyclohexylamine Basic information Product Name: N-Methylcyclohexylamine Synonyms: 1-Methylcyclohexylamine;Cyclohexanamine,N-methyl-;Cyclohexylamine, N-methyl-;Cyclohexylmethylamine;cyclohexyl-methyl-amine;Methylcyclohexylamine;methylcy
Cas:100-60-7
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:100-60-7
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryHangzhou Keying Chem Co., Ltd. Is a comprehensive enterprise, dedicated to the development, production and marketing of chemicals. As a technology innovative and service professional enterprise, Our company mainly engages in global pharmaceutical,
Cas:100-60-7
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:100-60-7
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:100-60-7
Min.Order:1 Metric Ton
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Type:Trading Company
inquirycyclohexanone
dimethyl amine
A
N-methylcyclohexylamine
B
N,N-dimethyl-cyclohexanamine
C
cyclohexanol
Conditions | Yield |
---|---|
With hydrogen at 160 - 220℃; under 67506.8 - 97509.8 Torr; for 100 - 1000h; Product distribution / selectivity; | A 0.1% B 96% C 0.5% |
With hydrogen at 160 - 180℃; under 63756.4 - 97509.8 Torr; for 100 - 400h; Product distribution / selectivity; | A 0.1% B 94% C 2% |
N-butylamine
A
butyl-(3-methyl-3H-benzothiazol-2-ylidene)-amine
B
N-methylcyclohexylamine
Conditions | Yield |
---|---|
at 25℃; for 3h; | A 95% B 83% |
In dichloromethane at 25℃; for 3h; | A 95% B 83% |
Conditions | Yield |
---|---|
With Zr12(μ3-O)5[(μ3-O)CoCl]8[(μ2-O)2(μ3-O)CoCl]3Li3(triphenyldicarboxylate)9; hydrogen In toluene at 110℃; under 30003 Torr; for 42h; Catalytic behavior; Inert atmosphere; Schlenk technique; | 92% |
With dimethyl sulfoxide In water at 100℃; Green chemistry; | 65% |
Conditions | Yield |
---|---|
With hydrogen In neat (no solvent) at 80℃; under 7600.51 Torr; for 24h; Catalytic behavior; Autoclave; | 91% |
With dichloro(μ-chloro)(μ-hydrido)bis(η-p-cymene)diruthenium(II); hydrogen In neat (no solvent) at 75℃; under 37503.8 Torr; for 24h; | 80% |
With lithium; methylamine |
Conditions | Yield |
---|---|
With iridium bromide; zinc In 1,4-dioxane; water at 30℃; for 72h; | 85% |
With titanium(IV) isopropylate; sodium tetrahydroborate; triethylamine 1.) EtOH, 25 deg C, 10 h, 2.) EtOH, 25 deg C, 8 h; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
With hydrogenchloride; Zr(BH4)2Cl2(dabco)2 In methanol for 1h; Heating; | 78% |
With D-glucose; glucose dehydrogenase CDX-901; imine reductase 48 from Rhizobium sullae; nicotinamide adenine dinucleotide phosphate In aq. buffer at 25℃; for 24h; pH=9; Enzymatic reaction; | 66% |
With sodium tetrahydroborate; lithium chloride In tetrahydrofuran; methanol Flow reactor; chemoselective reaction; | 37% |
Conditions | Yield |
---|---|
With rhodium(III) chloride hydrate; potassium tert-butylate at 130℃; for 48h; Sealed tube; High pressure; | 75% |
With thorium dioxide at 320℃; | |
rhodium hydrido (PEt3)3 complex for 10h; | 99 % Chromat. |
With platinum on carbon; hydrogen; sodium hydroxide at 130℃; under 30003 Torr; for 36h; Autoclave; | 74 %Chromat. |
With palladium 10% on activated carbon; potassium tert-butylate at 130℃; for 12h; |
N-(6-Methoxy-1,2,3,4-tetrahydro-naphthalen-1-yl)-N-methyl-hydroxylamine
N-methylcyclohexylamine
Conditions | Yield |
---|---|
With carbon disulfide In acetonitrile for 1.5h; Ambient temperature; | 71% |
Conditions | Yield |
---|---|
Stage #1: chloromethyltriethoxysilane; cyclohexylamine at 87℃; for 18h; Stage #2: With water In ethanol for 48h; Heating; Further stages.; | 68% |
N-methylcyclohexylamine
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In diethyl ether -60 degC -> room temp.; | 67% |
N-(benzenesulfenyl)-N-methylcyclohexylamine
N-methylcyclohexylamine
Conditions | Yield |
---|---|
With tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) In cyclohexane Heating; | 53% |
With tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) In cyclohexane for 0.25h; Mechanism; Product distribution; Heating; other conditions: other solvent, no reagents and catalysts; other sulpenamides as starting material; Competitive reaction of C-SPh compound 11 with Bu3nH: comparison of the reactivities of N-SPh and C-SPh bonds; |
cyclohexanone
methylamine
A
N-methylcyclohexylamine
B
cyclohexanol
Conditions | Yield |
---|---|
With hydrogenchloride; sodium tetrahydroborate In isopropyl alcohol at 20 - 30℃; | A 45% B 40% |
With potassium hydroxide; potassium phosphate In water at 18 - 20℃; pH 12, electrochemical reaction; |
cyclohexylamine
carbonic acid dimethyl ester
A
N-methylcyclohexylamine
B
N,N-dimethyl-cyclohexanamine
Conditions | Yield |
---|---|
With binder-free NaY zeolite Heating; | A 5% B n/a |
diazomethane
cyclohexylamine
A
N-methylcyclohexylamine
B
N,N-dimethyl-cyclohexanamine
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate |
Conditions | Yield |
---|---|
With sodium hydroxide; potassium hexacyanoferrate(III) | |
With diethyl ether; bromocyane und Erhitzen des hierbei erhaltenen Reaktionsprodukts mit wss. H2SO4; | |
With naphthalene-1,4-dicarbonitrile In methanol; acetonitrile for 0.166667h; UV-irradiation; | 11 % Chromat. |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride; diethyl ether |
N-(cyanomethyl)cyclohexylamine
A
N-methylcyclohexylamine
B
N-cyclohexylethylenediamine
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride; diethyl ether |
N-methylaniline hydrochloride
A
N-methylcyclohexylamine
B
N-Methyldicyclohexylamine
Conditions | Yield |
---|---|
With ethanol; platinum at 70℃; under 1520 - 2280 Torr; Hydrogenation; |
4-methylamino-phenol; hydrochloride
A
N-methylcyclohexylamine
B
4-(methylamino)cyclohexanol
Conditions | Yield |
---|---|
With water; platinum under 2280 Torr; Hydrogenation.entsteht ein Gemisch von cis- und trans-Form; |
N-Methylformamide
cyclohexanone
A
N-methylcyclohexylamine
B
N-Methyldicyclohexylamine
Conditions | Yield |
---|---|
With formic acid |
diethyl ether
cyclohexylamine
dimethyl sulfate
A
N-methylcyclohexylamine
B
N,N-dimethyl-cyclohexanamine
Conditions | Yield |
---|---|
With diethyl ether |
N-(α-phenylbenzylidene)cyclohexylamine
methyl iodide
A
benzophenone
B
N-methylcyclohexylamine
Conditions | Yield |
---|---|
anschliessend beim Kochen mit 90prozentigem Alkohol; |
N-chloromethylamine
cyclohexyl-dimethylborane
N-methylcyclohexylamine
Conditions | Yield |
---|---|
a) 0 deg C, 5-10 min, b) RT, 60 min; Yield given; |
Diphenylmethane
lithium cyclohexyl(methyl)amide
A
N-methylcyclohexylamine
B
diphenylmethyllithium
Conditions | Yield |
---|---|
In tetrahydrofuran at 30℃; Equilibrium constant; |
triphenylmethane
lithium cyclohexyl(methyl)amide
A
N-methylcyclohexylamine
B
trityllithium
Conditions | Yield |
---|---|
In tetrahydrofuran at 30℃; Equilibrium constant; |
Conditions | Yield |
---|---|
With hydrogenchloride; zinc |
methanol
cyclohexylamine
A
N-methylcyclohexylamine
B
N,N-dimethyl-cyclohexanamine
Conditions | Yield |
---|---|
ruthenium trichloride; tri-n-butyl phosphite In 1,4-dioxane at 180℃; for 15h; | A 3 % Chromat. B 14 % Chromat. |
With carbonylhydrido(tetrahydroborato)[bis(2-diphenylphosphinoethyl)amino]ruthenium(II); hydrogen at 120℃; under 30003 Torr; for 24h; Glovebox; | A n/a B 31 %Spectr. |
With C19H37IrN4(2+)*2Cl(1-)*2H2O; potassium carbonate at 50℃; for 17h; Reagent/catalyst; Inert atmosphere; Schlenk technique; Sealed tube; | A 14 %Chromat. B 61 %Chromat. |
With hydrogen at 55℃; under 750.075 Torr; for 24h; Irradiation; Green chemistry; |
Methyltrimethoxyphosphonium tetrafluoroborate
cyclohexylamine
A
N-methylcyclohexylamine
B
N,N-dimethyl-cyclohexanamine
Conditions | Yield |
---|---|
for 12h; Ambient temperature; Yield given. Yields of byproduct given; |
N-methylcyclohexylamine
2-(vinyloxy)ethyl isothiocyanate
1-Cyclohexyl-1-methyl-3-(2-vinyloxy-ethyl)-thiourea
Conditions | Yield |
---|---|
100% |
N-methylcyclohexylamine
2-phenyl-1-(2-thioxothiazolidin-3-yl)ethan-1-one
N-cyclohexyl-N-methyl-2-phenylacetamide
Conditions | Yield |
---|---|
100% | |
In dichloromethane for 0.0333333h; Ambient temperature; | 100% |
N-methylcyclohexylamine
benzenesulfenyl chloride
N-(benzenesulfenyl)-N-methylcyclohexylamine
Conditions | Yield |
---|---|
With triethylamine In diethyl ether for 0.166667h; | 100% |
N-methylcyclohexylamine
bis(trichloromethyl) carbonate
N-methyl-N-cyclohexylaminocarbonyl chloride
Conditions | Yield |
---|---|
With pyridine In toluene | 100% |
With pyridine In toluene | |
With pyridine In dichloromethane at 20℃; for 2h; |
Conditions | Yield |
---|---|
chloro(cyclopentadienyl)bis(triphenylphosphine)ruthenium (II) at 100℃; | 100% |
With rhodium(III) chloride hydrate; potassium tert-butylate at 130℃; for 48h; Sealed tube; High pressure; | 45% |
With Ru(OAc)2(1,1′-bis(diisopropylphosphino)ferrocene)(CO); trifluoroacetic acid at 100℃; for 24h; Temperature; Inert atmosphere; Schlenk technique; | |
With palladium 10% on activated carbon; potassium tert-butylate at 130℃; for 14h; |
Conditions | Yield |
---|---|
With trichloroisocyanuric acid; silica gel; sodium nitrite In dichloromethane at 20℃; for 0.25h; | 99% |
With sulfuric acid; silica gel; sodium nitrite In dichloromethane at 20℃; for 0.166667h; | 98% |
With N,N,N’,N’-tetrabromobenzene-1,3-disulfonamide; water; silica gel; sodium nitrite In dichloromethane at 20℃; for 0.0666667h; Reagent/catalyst; | 98% |
N-methylcyclohexylamine
1-(2-Thioxo-thiazolidin-3-yl)-hexadecan-1-one
N-cyclohexyl-N-methylhexadecanamide
Conditions | Yield |
---|---|
In dichloromethane for 0.166667h; Ambient temperature; | 99% |
N-methylcyclohexylamine
2-bromobenzoic acid chloride
2-bromo-N-cyclohexyl-N-methylbenzamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 2h; Ambient temperature; | 99% |
With N-ethyl-N,N-diisopropylamine In diethyl ether at 0 - 20℃; Inert atmosphere; | 4.5 g |
N-methylcyclohexylamine
4-chloro-1H-pyrrolo[2,3-d]pyrimidine
N-cyclohexyl-N-methyl-7H-pyrrolo[2,3-d]pyrimidin-4-amine
Conditions | Yield |
---|---|
In 1,4-dioxane at 110℃; for 9h; Microwave irradiation; Sealed tube; | 99% |
Stage #1: N-methylcyclohexylamine; 4-chloro-1H-pyrrolo[2,3-d]pyrimidine In tert-butyl alcohol at 100℃; for 24h; Stage #2: With hydrogenchloride In water; tert-butyl alcohol pH=1; Stage #3: With sodium hydroxide In water; tert-butyl alcohol pH=14; | 88% |
In tert-butyl alcohol at 85℃; |
2,4,6-trimethyl-pyridine
N-methylcyclohexylamine
sulfuric acid
tetrabutylammomium bromide
Conditions | Yield |
---|---|
In 1,1,2,2-tetrachloroethylene | 99% |
N-methylcyclohexylamine
1-Bromo-2-bromomethyl-benzene
N-(2-bromobenzyl)-N-methylcyclohexylamine
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With C50H61Cl2N3Pd; potassium tert-butylate In 1,4-dioxane at 100℃; for 2h; | 99% |
2-chloro-1,3-benzoxazole
N-methylcyclohexylamine
N-cyclohexyl-N-methylbenzo[d]oxazol-2-amine
Conditions | Yield |
---|---|
With C50H61Cl2N3Pd; potassium tert-butylate In 1,4-dioxane at 100℃; for 2h; | 99% |
N-methylcyclohexylamine
zirconium(IV) chloride
tetrakis(cyclohexylmethylamide)zirconium
Conditions | Yield |
---|---|
With Li-n-Bu In hexane; toluene in oxygen and moisture free atmosphere; soln. of ligand in toluene addeddropwise to soln. of Li-n-Bu in hexane; stirred at room temp. for 2.5 h ; ZrCl4 added gradually for 30 min; stirred for 18 h; filtered; filtrate reduced to oil under reduced pressure; elem. anal.; | 98.7% |
Conditions | Yield |
---|---|
In methanol at 50℃; under 6000480 Torr; for 96h; | 98% |
N-methylcyclohexylamine
methyl 2-isothiocyanatobenzoate
methyl 2-(3-cyclohexyl-3-methylthioureido)benzoate
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 3h; | 98% |
In dichloromethane at 20℃; |
5-methyl-1,3-benzoxazole
N-methylcyclohexylamine
N-cyclohexyl-N'-(2-hydroxy-5-methylphenyl)-N-methylmethanimidamide
Conditions | Yield |
---|---|
at 80℃; for 12h; | 98% |
In acetonitrile at 80℃; for 10h; |
N-methylcyclohexylamine
2-Iodobenzoyl chloride
N-cyclohexyl-2-iodo-N-methylbenzamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0℃; for 5h; | 98% |
N-methylcyclohexylamine
1-tosyl-4-vinyl-1,4-dihydro-2H-benzo[d] [1,3]oxazin-2-one
Conditions | Yield |
---|---|
Stage #1: N-methylcyclohexylamine With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 1-((11bS)-dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-yl)-1,2,3,4-tetrahydroquinoline In tetrahydrofuran at -10 - 20℃; for 0.166667h; Schlenk technique; Inert atmosphere; Stage #2: 1-tosyl-4-vinyl-1,4-dihydro-2H-benzo[d] [1,3]oxazin-2-one In tetrahydrofuran at -10℃; for 5h; Schlenk technique; Inert atmosphere; enantioselective reaction; | 98% |
N-methylcyclohexylamine
ethyl 4-chloro-1-(4-methoxybenzyl)-1H-pyrazolo[3,4-b]pyridine-5-carboxylate
Conditions | Yield |
---|---|
In ethanol at 80℃; for 2h; Inert atmosphere; | 98% |
N-methylcyclohexylamine
di-tert-butyl dicarbonate
Conditions | Yield |
---|---|
With saccharin sulfonic acid In hexane at 20℃; for 1h; | 97% |
With piperazine functionalized zirconium-Fe3O4-MCM-41 magnetic nanoparticles In neat (no solvent) at 20℃; for 0.166667h; Time; | 91% |
With 1,3-disulfonic acid imidazolium hydrogen sulfate In neat (no solvent) at 20℃; for 0.166667h; Green chemistry; chemoselective reaction; | 90% |
N-methylcyclohexylamine
Propiolic acid
N-cyclohexyl-N-methylpropiolamide
Conditions | Yield |
---|---|
Stage #1: Propiolic acid With pivaloyl chloride; potassium carbonate In tetrahydrofuran for 1h; Inert atmosphere; Cooling; Stage #2: N-methylcyclohexylamine In tetrahydrofuran for 1h; Inert atmosphere; | 97% |
potassium cyanate
N-methylcyclohexylamine
para-nitrophenyl bromide
1-cyclohexyl-3-(4-nitrophenyl)-1-methyl-urea
Conditions | Yield |
---|---|
With copper(I) oxide; 2-(2,6-dimethylphenyl-amino)-2-oxoacetic acid potassium salt In acetonitrile at 110℃; Schlenk technique; Inert atmosphere; | 97% |
Conditions | Yield |
---|---|
With [Pd{C6H4(CH2N(CH2Ph)2)}(μ-Br)]2; potassium hydroxide In dimethyl sulfoxide at 120℃; for 0.5h; | 97% |
With sodium t-butanolate In dimethyl sulfoxide at 110℃; for 12h; Buchwald-Hartwig Coupling; Green chemistry; | 95% |
With sodium t-butanolate In dimethyl sulfoxide at 110℃; for 12h; Buchwald-Hartwig Coupling; | 87% |
With potassium hydroxide In dimethyl sulfoxide at 120℃; for 0.666667h; | 75% |
With copper(l) iodide; cesium fluoride In dimethyl sulfoxide at 130℃; for 24h; Ullmann Condensation; Inert atmosphere; Glovebox; |
Conditions | Yield |
---|---|
In methanol; water for 0.25h; Inert atmosphere; | 97% |
N-methylcyclohexylamine
ethyl 2-isothiocyanato-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylate
2-(3-Cyclohexyl-3-methyl-thioureido)-4,5,6,7-tetrahydro-benzo[b]thiophene-3-carboxylic acid ethyl ester
Conditions | Yield |
---|---|
In dichloromethane for 5h; Ambient temperature; | 96% |
In dichloromethane at 20℃; for 3h; |
N-methylcyclohexylamine
cyclohexanone
N-cyclohexyl-N-methylcyclohex-1-enamine
Conditions | Yield |
---|---|
With titanium tetrachloride In cyclohexane at 0 - 20℃; Inert atmosphere; | 96% |
N-methylcyclohexylamine
o-bromobenzenesulfonyl chloride
2-bromo-N-cyclohexyl-N-methylbenzenesulfonamide
Conditions | Yield |
---|---|
With dmap; triethylamine In tetrahydrofuran at 20℃; for 16h; Inert atmosphere; | 96% |
Conditions | Yield |
---|---|
Stage #1: N-methylcyclohexylamine; 4-tert-butylphenyl triflate With potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); XPhos In tetrahydrofuran at 80℃; for 16h; Buchwald-Hartwig Coupling; Inert atmosphere; Sealed tube; Stage #2: With hydrogenchloride In diethyl ether Inert atmosphere; | 96% |
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