As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiryOur Advantage 1. Rich experience We specialize in this filed for many years, our APIs exported to all over the world and and we established long friendly relations of cooperation with our clients. 2. Great quality,purity and favorable Good qual
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inquiryMethylamine hydrochloride Basic information Product Name: Methylamine hydrochloride Synonyms: Methylamine-hydrogenchloride(1/1);Methyl-ammonium;MERCURIALIN HYDROCHLORIDE;METHYLAMINE HYDROCHLORIDE;METHYLAMINE HCL;METHYLAMMONIUM CHLORIDE;AMINOMET
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inquirychengdu and import and export trade co., LTD., who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do res
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inquiryWe generally use secure shipping methods that do not require you to do any customs clearance. Free shipping to your address without worrying about any customs issues. We have a professional customs clearance team to 100% guarantee the safe delivery o
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inquiryHebei Mojin Biotechnology Co., Ltd, Our company is a professional in lead acetate, diphenyl ethylamine and other chemical raw materials and chemical reagents research and development production enterprises. Our business covers more than 30 countrie
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inquiryWuhan Bright Chemical Co., Ltd is set up in 2008. We mainly concentrate on producing, researching and trading electroplating intermediates, Fluoro -containing chemicals,Silicone oil, Lithium battery solvent and other fine chemicals. Our factory cov
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inquiryBeluga chemical professional supply High quality Methylamine hydrochloride CAS 593-51-1 Beluga Chemical has a professional RESEARCH and development team and strong technical force to ensure technical support and research capabilities. 2. Made in
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inquiryFACTORY Methylamine hydrochloride CAS 593-51-1 in stock Product name Methylamine hydrochloride CAS 593-51-1 MF CH5N.ClH MW 67.52 Melting point 231-233 °C(lit.) Boling point
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:593-51-1
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inquiryItems Standard Test Result Appearance White crystalline powder White crystalline powder Assay
Cas:593-51-1
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inquiryProduct Description Product Name
Cas:593-51-1
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inquirySuperiority 1.high purity 2.consistent quality 3.competitive price 4.Fast Shipping · ProName: Methylamine Hydrochloride · CasNo: 593-51-1 · Molecular Formula: CH6ClN · Appearance: powder
Cas:593-51-1
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inquiryT he company has advanced technology, as well as a large number of excellent R & D team, to provide customers from the grams to one hundred kilograms and tons of high-quality products, competitive prices and quality service Appearance:white
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiryShanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
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inquiry
Cas:593-51-1
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inquiryProduct Name: Methylamine hydrochloride Synonyms: Methylammonium Chloride Solution;Methylamine H20;Methylamine Hydrochloride / Methylamine HCl;methy hcl 593-51-1 kf-wang(at)kf-chem.com;Methylamine-hydrogenchloride(1/1);Methyl-ammonium;MERCURIALIN
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inquiryLIDE PHARMACEUTICALS LIMITED is a professional chemicals and APIs leading manufacturer in China. Our core business line covers APIs, Intermediates, Herb extract, etc.
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inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
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inquiryMethylamine HCl Appearance:White Powder Storage:Store in cool and dry place, away from sun light. Package:25kg Application:Cosmetic Raw Materials, Detergent Raw Materials, Hair Care Chemicals Transportation:By sea or by air Port:Qingdao Port
Our company advantages: Wuhan Han Sheng New Material Technology Co. Ltd 1. Liquid: 0.5liter/bottle, 1liter/bottle, 5liter/bottle, 25liter/box, we use corrosion-resistant chemical liquid packaging plastic barrels . and double layer metal bucke
Cas:593-51-1
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inquiry1. Product advantages High purity, all above 98.5%, no impurities after dissolution We will test each batch to ensure quality OEM and private brand services designed for free Various cap colors available We can also provide MT1 peptide powd
Cas:593-51-1
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by email in time prod
Cas:593-51-1
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inquiryAdvantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best s
Cas:593-51-1
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiryWe are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery
Cas:593-51-1
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:593-51-1
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inquiryProduct Detail Minimum Order Qty. 10 Gram
Cas:593-51-1
Min.Order:10 Gram
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Type:Trading Company
inquiry1.High Quality: Quality is life. Quality is the most important element for all goods. We have a lab doing research in Wuhan China and produce sarms in bulk quantity. We have 8 years experience making all kinds of sarms. And all our old customers
Cas:593-51-1
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inquiryConditions | Yield |
---|---|
With hydrogenchloride | A n/a B 99% |
N-Nitroso-N-methylmethoxymethylamine
methylamine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In methanol for 2h; Heating; | 97% |
(E)-2-Chloro-3-hydroxy-but-2-enoic acid methyl ester
diethylamine
A
methylamine hydrochloride
Conditions | Yield |
---|---|
In diethyl ether at -40℃; for 1h; | A n/a B 96% |
bis(trifluoromethyl)chlorophosphine
A
methylamino-bis-trifluoromethyl-phosphine
B
methylamine hydrochloride
Conditions | Yield |
---|---|
With CH3NH2 In gaseous matrix 0°C; | A 95% B n/a |
N-formyl-N-methylformamide
methylamine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol; water for 168h; Ambient temperature; | 94% |
formamide
methylamine hydrochloride
Conditions | Yield |
---|---|
Stage #1: formamide With bis(tetrahydrofuran)calcium di(bis(trimethylsilyl)amide); 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane In toluene at 120℃; for 36h; Inert atmosphere; Schlenk technique; Stage #2: With hydrogenchloride In diethyl ether; toluene Inert atmosphere; Schlenk technique; | 90% |
Stage #1: formamide With [(aNHC)KN(SiMe3)2]2; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane In toluene at 40℃; for 12h; Inert atmosphere; Glovebox; Schlenk technique; Stage #2: With water; sodium hydroxide In diethyl ether; toluene at 40℃; for 1h; Inert atmosphere; Glovebox; Schlenk technique; Stage #3: With hydrogenchloride In diethyl ether; water Inert atmosphere; Glovebox; Schlenk technique; | 98 %Spectr. |
Conditions | Yield |
---|---|
Stage #1: glycine With (R)-Carvone In propan-1-ol at 20 - 190℃; under 11251.1 Torr; for 0.216667h; Sealed tube; Microwave irradiation; Stage #2: With hydrogenchloride In propan-1-ol; water at 190℃; for 0.0833333h; Microwave irradiation; | 86% |
methylamine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In propan-1-ol at 190℃; for 0.216667h; Temperature; Microwave irradiation; Green chemistry; | 86% |
Conditions | Yield |
---|---|
In ethanol; dichloromethane under N2 soln. Mo(HB(Me2pyz)3)(NO)Cl2 in dichloromethane treated with methylamine (33% ethanolic soln.) and mixt. stirred at room temp. for 30 min; volume solvent reduced in vacuo, Et2O added, (NH3Me)Cl filtered off, filtrate reduced in vacuo; elem. anal.; | A 83% B n/a |
Conditions | Yield |
---|---|
Stage #1: nitromethane With hydrazine hydrate; zinc In methanol at 20℃; for 0.0666667h; Stage #2: With hydrogenchloride | 80% |
With hydrogenchloride; zinc; hydrazinium monoformate In water for 0.0416667h; | 75% |
Stage #1: nitromethane With formic acid; nickel In methanol at 20℃; for 0.0833333h; Reduction; Stage #2: With hydrogenchloride Addition; | 45% |
diethylamine
(E)-2-Chloro-4,4-difluoro-3-hydroxy-but-2-enoic acid methyl ester
A
methylamine hydrochloride
B
(E)-2-Chloro-4,4-difluoro-3-hydroxy-but-2-enoic acid methyl ester; compound with diethyl-amine
Conditions | Yield |
---|---|
In diethyl ether at -40℃; for 1h; | A n/a B 76% |
methylamine
phenylhydroxamoyl chloride
A
(Z)-N-Methylbenzamid-oxim
B
methylamine hydrochloride
Conditions | Yield |
---|---|
In diethyl ether for 48h; Ambient temperature; | A 76% B n/a |
methylamine
pentafluorophenyl dichlorophosphine
A
C6F5P{N(H)CH3}2
B
methylamine hydrochloride
Conditions | Yield |
---|---|
In diethyl ether byproducts: HCl; in presence of a trap for HCl; | A 75% B n/a |
In diethyl ether byproducts: HCl; in presence of a trap for HCl; | A 75% B n/a |
diethylamine
(E)-2-Chloro-4,4,4-trifluoro-3-hydroxy-but-2-enoic acid methyl ester
A
methylamine hydrochloride
B
(E)-2-Chloro-4,4,4-trifluoro-3-hydroxy-but-2-enoic acid methyl ester; compound with diethyl-amine
Conditions | Yield |
---|---|
In diethyl ether at -40℃; for 1h; | A n/a B 70% |
diethylamine
(E)-2-Chloro-4,4,5,5,6,6,7,7,7-nonafluoro-3-hydroxy-hept-2-enoic acid methyl ester
A
methylamine hydrochloride
B
(E)-2-Chloro-4,4,5,5,6,6,7,7,7-nonafluoro-3-hydroxy-hept-2-enoic acid methyl ester; compound with diethyl-amine
Conditions | Yield |
---|---|
In diethyl ether at -40℃; for 1h; | A n/a B 69% |
3-Methylcarbamoylsulfanyl-propionic acid methyl ester
A
3-methylcarbamoylsulfanyl-propionic acid
B
methylamine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride Heating; | A 58% B 15% |
(CO)5MoP(NHCH3)3
A
pentacarbonyl-[chloro-di(methylamino)phosphane]molybdenum(0)
B
methylamine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In toluene (N2), HCl introduced into a soln. of the Mo-complex at room temp. for 30 min; removed in vacuo, extd. with hexane, filtered, crystd. at -35°C,elem. anal.; | A 51.2% B >99 |
Conditions | Yield |
---|---|
With hydrogen cyanide; ammonium chloride In not given in basic soln.; NH4Cl is produced by partial hydrolysis of HCN; | A n/a B 44% |
With HCN; NH4Cl In not given in basic soln.; NH4Cl is produced by partial hydrolysis of HCN; | A n/a B 44% |
Dichloromethylsilane
methylamine
A
methylamine hydrochloride
B
1,3-dichloro 1,2,3-trimethyl disilazane
Conditions | Yield |
---|---|
In tetrahydrofuran at -30℃; for 15h; | A n/a B 43% |
Dichloromethylsilane
methylamine
A
methylamine hydrochloride
B
1,3-dichloro 1,2,3-trimethyl disilazane
Conditions | Yield |
---|---|
In pentane 1.) -30 deg C, 8 h; 2.) RT, 12 h; | A n/a B 39% C 15% |
Conditions | Yield |
---|---|
With hydrogenchloride; copper-salt; ammonium chloride at 370℃; unter Druck; | |
With hydrogenchloride; iron-salt; ammonium chloride at 370℃; unter Druck; | |
With copper-salt; ammonium chloride at 370℃; unter Druck; | |
With iron-salt; ammonium chloride at 370℃; unter Druck; |
Conditions | Yield |
---|---|
With water; ammonium chloride | |
With ammonium chloride at 120 - 210℃; |
trimethylamine hydrochloride
A
methylene chloride
B
methylamine hydrochloride
C
trimethylamine
Conditions | Yield |
---|---|
at 285℃; |
ephedrine hydrochloride
A
methylamine hydrochloride
B
1-phenyl-propan-1-one
Conditions | Yield |
---|---|
Destillation im CO2-Strom; |
Conditions | Yield |
---|---|
With hydrogenchloride; copper-salt at 370℃; unter Druck; | |
With hydrogenchloride; iron-salt at 370℃; unter Druck; |
methylene chloride
methylamine
A
methylamine hydrochloride
B
tetramethlyammonium chloride
propan-1-ol
2,4,6-trichloro-1,3,5-trimethylborazine
benzene
A
tri-n-propyl borate
B
methylamine hydrochloride
formaldehyd
A
formic acid
B
monomethanolamine
C
methylamine hydrochloride
D
N-methylhydroxylamine hydrochloride
Conditions | Yield |
---|---|
With ammonium chloride; water at 25℃; for 24h; Further byproducts given; |
formaldehyd
A
methylaminomethanol
B
monomethanolamine
C
methylamine hydrochloride
D
N-methyldiethanolamine
F
N-methylhydroxylamine hydrochloride
Conditions | Yield |
---|---|
With ammonium chloride In water at 25℃; for 24h; Mechanism; |
Octanal
methylamine hydrochloride
potassium cyanide
2-Methylamino-nonanenitrile
Conditions | Yield |
---|---|
With aluminum oxide In acetonitrile at 50℃; for 22h; ultrasound; | 100% |
2-benzyloxy-3-methoxybenzaldehyde
methylamine hydrochloride
1-(2-(benzyloxy)-3-methoxyphenyl)-N-methylmethanamine
Conditions | Yield |
---|---|
With sodium tetrahydroborate | 100% |
methylamine hydrochloride
N-[(R)-1-[(1,1-dimethylethoxy)carbonyl]-3-(1,3-dihydro-1,3-dioxo-2H-benz[f]isoindol-2-yl)propyl]-L-leucine
N-<1-(R)-<(1,1-dimethylethoxy)carbonyl>-3-(1,3-dihydro-1,3-dioxo-2H-benzisoindol-2-yl)propyl>-N'-methyl-L-leucinamide
Conditions | Yield |
---|---|
With 1-hydroxybenzotriazol-hydrate; triethylamine; dicyclohexyl-carbodiimide In dichloromethane for 18h; Ambient temperature; | 100% |
Conditions | Yield |
---|---|
With triethylamine In N,N-dimethyl-formamide for 72h; | 100% |
methylamine hydrochloride
potassium cyanide
acetophenone
2-methylamino-2-phenyl-propionitrile
Conditions | Yield |
---|---|
With aluminum oxide In acetonitrile at 50℃; for 24h; ultrasound; | 100% |
4'-carboxyl N-Boc-2',6'-dimethyl-L-phenylalanine methyl ester
methylamine hydrochloride
methyl (S)-2-((tert-butoxycarbonyl)amino)-3-(2,6-dimethyl-4-(methylcarbamoyl)phenyl)propanoate
Conditions | Yield |
---|---|
With ammonium chloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide; tert-butyl alcohol at 20℃; for 0.666667h; | 100% |
methylamine hydrochloride
methyl 4-<<<4-<<<4-<<(tert-butyloxy)carbonyl>amino>-1-methyl-pyrrol-2-yl>carbonyl>amino>-1-methyl-pyrrol-2-yl>carbonyl>amino>-1-methyl-pyrrole-2-carboxylic acid
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 25℃; for 14h; | 100% |
methylamine hydrochloride
5-bromo-2-difluoromethoxy-N-methyl-benzamide
Conditions | Yield |
---|---|
Stage #1: 5-bromo-2-difluoromethoxy-benzoic acid With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine In N,N-dimethyl-formamide at 20℃; for 1h; Stage #2: methylamine hydrochloride In N,N-dimethyl-formamide at 20℃; for 2h; | 100% |
Conditions | Yield |
---|---|
With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine In DMF (N,N-dimethyl-formamide) at 20℃; | 100% |
3,4-difluoronitrobenzene
methylamine hydrochloride
N-methyl-2-fluoro-4-nitroaniline
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 24h; | 100% |
3-methoxy-4-nitrobenzoic acid
methylamine hydrochloride
3-methoxy-N-methyl-4-nitrobenzamide
Conditions | Yield |
---|---|
Stage #1: 3-methoxy-4-nitrobenzoic acid; methylamine hydrochloride With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 0.0833333h; Stage #2: With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 18h; | 100% |
With benzotriazol-1-ol In N,N-dimethyl-formamide at 20℃; for 18h; |
methylamine hydrochloride
n-octanoic acid chloride
N-methyloctanoylamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 5℃; for 2.5h; | 100% |
With triethylamine In dichloromethane at 0 - 20℃; for 3h; | 100% |
With triethylamine In dichloromethane at 0 - 20℃; for 3h; | 100% |
5-bromo-1-(phenylsulfonyl)-1H-pyrrole-3-carbaldehyde
methylamine hydrochloride
1-[5-bromo-1-(phenylsulfonyl)-1H-pyrrol-3-yl]-N-methylmethanamine
Conditions | Yield |
---|---|
With sodium cyanoborohydride In methanol at 20℃; for 1h; | 100% |
With methanol; sodium cyanoborohydride at 20℃; for 1h; | 100% |
With methanol; sodium cyanoborohydride at 10 - 35℃; for 1h; | 100% |
4-(5-nitro-1H-indol-3-yl)cyclohex-3-enone
methylamine hydrochloride
N-methyl-4-(5-nitro-1H-indol-3-yl)cyclohex-3-enamine
Conditions | Yield |
---|---|
Stage #1: 4-(5-nitro-1H-indol-3-yl)cyclohex-3-enone; methylamine hydrochloride With sodium tris(acetoxy)borohydride; acetic acid In 1,2-dichloro-ethane at 20℃; for 14h; Stage #2: With sodium hydroxide In water; 1,2-dichloro-ethane | 100% |
Stage #1: 4-(5-nitro-1H-indol-3-yl)cyclohex-3-enone; methylamine hydrochloride With sodium tris(acetoxy)borohydride; acetic acid In 1,2-dichloro-ethane at 20℃; for 14h; Stage #2: With sodium hydroxide In water; 1,2-dichloro-ethane | 100% |
With sodium tris(acetoxy)borohydride; acetic acid In 1,2-dichloro-ethane at 20℃; for 14h; Inert atmosphere; | 54% |
L-N-Boc-Ala
methylamine hydrochloride
tert-butyl N-[(1S)-1-(methylcarbamoyl)ethyl]carbamate
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In N,N-dimethyl-formamide at 20℃; for 17.5h; | 100% |
With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine In acetonitrile at 25℃; for 10h; | 68% |
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane at 0 - 20℃; | 50% |
With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine In dichloromethane at 23℃; for 12h; | |
With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 0 - 20℃; for 2h; |
methylamine hydrochloride
1-(pyridin-4-yl)-4-oxopiperidine
N-methyl-1-(pyridin-4-yl)piperidin-4-amine
Conditions | Yield |
---|---|
With sodium cyanoborohydride In methanol at 20℃; for 17h; | 100% |
Stage #1: methylamine hydrochloride; 1-(pyridin-4-yl)-4-oxopiperidine; acetic acid In methanol at 20℃; for 0.333333h; Stage #2: With sodium cyanoborohydride In methanol at 20℃; for 16h; |
methylamine hydrochloride
2-((tert-butoxycarbonyl)amino)-3-fluoro-3-methylbutanoic acid
tert-butyl 3-fluoro-3-methyl-1-(methylamino)-1-oxobutan-2-ylcarbamate
Conditions | Yield |
---|---|
With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine In dichloromethane for 18h; | 100% |
benzyl 4-oxo-1-piperidinecarboxylate
methylamine hydrochloride
4-methylamino-piperidine-1-carboxylic acid benzyl ester
Conditions | Yield |
---|---|
Stage #1: benzyl 4-oxo-1-piperidinecarboxylate; methylamine hydrochloride With sodium tris(acetoxy)borohydride; acetic acid In 1,2-dichloro-ethane at 20℃; Stage #2: With sodium hydrogencarbonate In water; 1,2-dichloro-ethane | 100% |
N-benzhydryl 3-azetidinone
methylamine hydrochloride
Conditions | Yield |
---|---|
Stage #1: N-benzhydryl 3-azetidinone; methylamine hydrochloride With acetic acid In methanol at 20℃; for 0.0833333h; Stage #2: potassium cyanide at 60℃; for 19h; | 100% |
Stage #1: N-benzhydryl 3-azetidinone; methylamine hydrochloride With acetic acid In methanol at 20℃; for 0.0833333h; Stage #2: potassium cyanide at 60℃; for 19h; | 100% |
Stage #1: N-benzhydryl 3-azetidinone; methylamine hydrochloride With acetic acid In methanol at 20℃; for 0.0833333h; Stage #2: potassium cyanide In methanol at 60℃; for 19h; | 100% |
p-(chloromethyl)benzoyl chloride
methylamine hydrochloride
4-(chloromethyl)-N-methylbenzamide
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0℃; for 1h; | 100% |
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; |
3-Fluoro-4-{3-[(1S)-2-methoxy-1-methylethoxy]-5-[5-(1,3-thiazol-2-yl)-1H-pyrrol-2-yl]phenoxy}benzoic acid
methylamine hydrochloride
3-fluoro-4-{3-[(1S)-2-methoxy-1-methylethoxy]-5-[5-(1,3-thiazol-2-yl)-1H-pyrrol-2-yl]phenoxy}-N-methylbenzamide
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; HATU In tetrahydrofuran at 20℃; for 4h; Inert atmosphere; | 100% |
2-((2R,3R,4R,5R)-3,4-bis(benzyloxy)-5-((benzyloxy)methyl)-1-(tert-butoxycarbonyl)pyrrolidin-2-yl)acetic acid
methylamine hydrochloride
(2R,3R,4R,5R)-tert-butyl 3,4-bis(benzyloxy)-2-((benzyloxy)methyl)-5-(2-(methylamino)-2-oxoethyl)pyrrolidine-1-carboxylate
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide at 20℃; for 48h; | 100% |
1-(5-bromopentyl)-5-fluoro-3-iodo-1H-indazole
methylamine hydrochloride
5-(5-fluoro-3-iodo-1H-indazol-1-yl)-N-methylpentan-1-amine
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In tetrahydrofuran at 90℃; Sealed tube; | 100% |
methylamine hydrochloride
Z-D-proline
benzyl (2R)-2-(methylcarbamoyl)pyrrolidine-1-carboxylate
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane at 0 - 25℃; for 7h; | 100% |
Conditions | Yield |
---|---|
In dichloromethane; N,N-dimethyl-formamide | 100% |
Conditions | Yield |
---|---|
In dichloromethane; N,N-dimethyl-formamide | 100% |
methylamine hydrochloride
Conditions | Yield |
---|---|
Stage #1: (R)-tert-butyl 3-(5-iodo-2-(methoxycarbonyl)phenoxy)pyrrolidine-1-carboxylate With sodium hydroxide In tetrahydrofuran; methanol at 25℃; for 2h; Stage #2: methylamine hydrochloride With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In tetrahydrofuran; methanol for 2h; | 100% |
methylamine hydrochloride
1,1'-carbonyldiimidazole
imidazole-1-carboxylic acid N-methylamide
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide; acetonitrile at 20℃; for 2h; | 100% |
In N,N-dimethyl-formamide; acetonitrile at 20℃; for 2h; | 75% |
In N,N-dimethyl-formamide; acetonitrile at 20℃; for 2h; | 68% |
In N,N-dimethyl-formamide; acetonitrile at 20℃; for 3.25h; | 57% |
In N,N-dimethyl-formamide; acetonitrile at 20℃; | 9.87 g |
Conditions | Yield |
---|---|
With 1-hydroxy-7-aza-benzotriazole; 1,2-dichloro-ethane; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; | 100% |
methylamine hydrochloride
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In tetrahydrofuran | 100% |
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