As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis
Cas:122-88-3
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inquiry1.quick response;2.competitive price with good quality product;3.flexible payment;4.fast delivery;5.superior after sell service. Appearance:White to off-white crystalline powder Storage:0-6°C Package:as customerized Application:plant growth promot
Cas:122-88-3
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:122-88-3
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inquiryHangzhou Dingyan Chem is a leading manufacturer and supplier of chemicals in China.We develop,produce and distribute high quality pharmaceuticals, intermediates, special chemicals and other fine chemicals. -------------------------------------
Cas:122-88-3
Min.Order:1 Kilogram
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Type:Trading Company
inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:122-88-3
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:122-88-3
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inquiryColorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on
Cas:122-88-3
Min.Order:1 Metric Ton
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inquiry
Cas:122-88-3
Min.Order:1 Metric Ton
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Type:Manufacturers
inquirychengdu and import and export trade co., LTD., who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do res
Cas:122-88-3
Min.Order:20 Metric Ton
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Type:Trading Company
inquiryAbout Product Details 4-Chlorophenoxyacetic acid C
Cas:122-88-3
Min.Order:1 Kilogram
FOB Price: $1.0 / 5.0
Type:Lab/Research institutions
inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Cas:122-88-3
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Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:122-88-3
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Type:Trading Company
inquiry1. Product advantages High purity, all above 98.5%, no impurities after dissolution We will test each batch to ensure quality OEM and private brand services designed for free Various cap colors available We can also provide MT1 peptide powd
Cas:122-88-3
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Type:Trading Company
inquiryProduct name Plant Hormones 4-CPA Chemical name 2-(4-Chloro-phenoxy) acetic acid; 4-Chlorophenoxyacetic acid CAS No. 122-88-3
Appearance:White to off-white powder Storage:room temperature Package:25kg/drum Application:2-(4-Chlorophenoxy)acetic Acid is used in the synthesis of a new class of hypoxia-inducible factor-1 inhibitors. Transportation:Express/Sea/Air Port:any por
Cas:122-88-3
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:122-88-3
Min.Order:1 Kilogram
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inquiryWe are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery
Cas:122-88-3
Min.Order:10 Gram
FOB Price: $1.32
Type:Trading Company
inquiry4-Chlorophenoxyacetic acid CAS:122-88-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic
Cas:122-88-3
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:122-88-3
Min.Order:1 Kilogram
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:122-88-3
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Type:Lab/Research institutions
inquiryMinimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,MoneyGram Package 10g,20g,50g,100g,500g,1KGS,
Cas:122-88-3
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:122-88-3
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Type:Lab/Research institutions
inquiryOur advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We have s
Cas:122-88-3
Min.Order:10 Kilogram
Negotiable
Type:Trading Company
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:122-88-3
Min.Order:0 Metric Ton
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Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:122-88-3
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Type:Lab/Research institutions
inquiryOur Advantages Production: Advanced chemical equipment with years of experience Staffs for producing various extract products. Quality Control:A complete set of Testing Professional and Analysis Equipment ensures the Quality Requirements and Specif
Cas:122-88-3
Min.Order:1 Kilogram
FOB Price: $75.0 / 150.0
Type:Trading Company
inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:122-88-3
Min.Order:1 Gram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:122-88-3
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryProduct name: 4-Chlorophenoxyacetic Acid CAS No.: 122-88-3 Molecule Formula:C8H6ClO3 Molecule Weight:185.59 Purity: 99.0% Package: 25kg/drum Description:White or off-white powder Manufacture Standards:Enterprise Standard TESTING
Cas:122-88-3
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
With sodium hydroxide Irradiation; | 98% |
With sodium hydroxide; dodecyltriethylammonium bromide for 0.0833333h; Irradiation; | 96% |
Stage #1: 4-chloro-phenol; chloroacetic acid With sodium hydroxide In water at 60 - 70℃; for 3h; Stage #2: With hydrogenchloride In water | 88% |
ethyl p-chlorophenoxyacetate
4-Chlorophenoxyacetic acid
Conditions | Yield |
---|---|
Stage #1: ethyl p-chlorophenoxyacetate With sodium hydroxide In tetrahydrofuran for 2h; Reflux; Stage #2: With hydrogenchloride In water pH=1; | 91% |
With sodium hydroxide In ethanol Reflux; | 88% |
With sodium hydroxide In ethanol; water Reflux; | 88% |
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol; water at 105℃; for 5h; | 85% |
Stage #1: 4-chloro-phenol With sodium hydroxide In ethanol; water at 20℃; for 0.333333h; Stage #2: sodium monochloroacetic acid In ethanol; water at 102℃; for 5h; | 77% |
With sodium hydroxide In ethanol; water for 1h; Reflux; | 74.6% |
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol; water at 0℃; for 2.5h; Reflux; | 95.6% |
With water; sodium hydroxide In ethanol at 0℃; for 2.58333h; Reflux; | 95.6% |
With water; sodium hydroxide In ethanol at 0℃; Reflux; | 95.6% |
Conditions | Yield |
---|---|
With sodium hydride In 1,4-dioxane; mineral oil at 0 - 100℃; for 3h; Inert atmosphere; Cooling with ice; | 60.3% |
Conditions | Yield |
---|---|
Stage #1: bromoacetic acid methyl ester; 4-chloro-phenol With caesium carbonate In acetone at 20℃; for 12h; Stage #2: With potassium hydroxide; water In tetrahydrofuran at 20℃; for 12h; | |
Stage #1: bromoacetic acid methyl ester; 4-chloro-phenol With caesium carbonate In acetone at 20℃; for 12h; Stage #2: With potassium hydroxide In tetrahydrofuran; water at 20℃; for 12h; | |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 12h; | |
Stage #1: bromoacetic acid methyl ester; 4-chloro-phenol With potassium phosphate In acetone at 60 - 95℃; for 18h; Stage #2: With sodium hydroxide In acetone for 1h; |
Conditions | Yield |
---|---|
With oxygen; molybdenum(VI) oxide In water at 80℃; under 750.075 Torr; | 187.16 g |
4-Chlorophenoxyacetic acid
Conditions | Yield |
---|---|
With phosphoric acid at 120℃; for 3h; | 186.29 g |
Stage #1: isooctyl 4-chlorophenoxyacetate With phosphoric acid at 120℃; for 3h; Stage #2: With water | 185.92 g |
With phosphoric acid at 120℃; for 3h; Large scale; | 1821.1 g |
With phosphoric acid at 120℃; for 3h; Large scale; | 1857.9 g |
Conditions | Yield |
---|---|
Stage #1: chloroacetic acid ethyl ester; 4-chloro-phenol With potassium carbonate; potassium iodide In N,N-dimethyl-formamide for 0.0666667h; Microwave irradiation; Stage #2: With sodium hydroxide In water; N,N-dimethyl-formamide for 0.0833333h; Microwave irradiation; Stage #3: With hydrogenchloride In water; N,N-dimethyl-formamide at 20℃; pH=6; | 91% |
Stage #1: chloroacetic acid ethyl ester; 4-chloro-phenol With potassium carbonate; potassium iodide In N,N-dimethyl-formamide for 0.0666667h; Microwave irradiation; Stage #2: With water; sodium hydroxide In N,N-dimethyl-formamide for 0.0833333h; Microwave irradiation; | 91% |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aq. NaOH solution; isopropyl alcohol 2: aq. NaOH solution View Scheme | |
Multi-step reaction with 2 steps 1: K2CO3 / acetone 2: aq. KOH View Scheme | |
Multi-step reaction with 2 steps 1.1: potassium carbonate / acetone / 14 h / Reflux 2.1: sodium hydroxide / tetrahydrofuran / 2 h / Reflux 2.2: pH 1 View Scheme |
2,4-Dichlorophenoxyacetic acid
A
(2-chlorophenoxy)acetic acid
B
4-Chlorophenoxyacetic acid
C
2-phenoxyacetic acid
Conditions | Yield |
---|---|
With hydrogen; palladium In water at 29.85℃; under 760 Torr; for 0.166667h; Product distribution; Further Variations:; Catalysts; Pressures; reaction times, reactant and catalyst concentrations; | A 23.0 % Chromat. B 4.1 % Chromat. C 37.6 % Chromat. |
With sodium chloride In water at 20℃; Kinetics; Electrochemical reaction; Inert atmosphere; | |
With palladium/alumina; titanium(IV) oxide for 1.5h; Irradiation; |
Conditions | Yield |
---|---|
With potassium phosphate In acetone at 40 - 60℃; for 10h; Reflux; Inert atmosphere; |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: potassium carbonate / 2 h / 80 °C 2: thionyl chloride; lead acetate; 2,3,4-trichlorothiophene / 0.5 h / 20 °C 3: sulfuric acid / 2 h / 80 °C View Scheme | |
Multi-step reaction with 3 steps 1: sodium carbonate / 5 h / 60 °C 2: zinc(II) chloride; bis(4-chlorophenyl)sulfide; sulfuryl dichloride / 0.5 h / 30 °C 3: phosphoric acid / 3 h / 120 °C View Scheme | |
Multi-step reaction with 3 steps 1.1: magnesium / 1 h / 70 °C 1.2: 0.5 h / 90 °C 2.1: thionyl chloride; 2,3,4-trichlorothiophene / 0.5 h / 20 °C 3.1: sulfuric acid / 2 h / 80 °C View Scheme |
A
4-Chlorophenoxyacetic acid
Conditions | Yield |
---|---|
With glucose dehydrogenase; D-glucose; YGL039w from saccharomyces cerevisiae; nicotinamide adenine dinucleotide phosphate In aq. acetate buffer at 30℃; for 1h; pH=5; Enzymatic reaction; stereoselective reaction; | A n/a B n/a |
A
4-Chlorophenoxyacetic acid
Conditions | Yield |
---|---|
With glucose dehydrogenase; D-glucose; SyADH from sphingobium yanoikuyae; nicotinamide adenine dinucleotide phosphate In aq. acetate buffer at 30℃; for 1h; pH=5; Enzymatic reaction; stereoselective reaction; | A n/a B n/a |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium carbonate / dimethylformamide / 20 °C 2: lithium hydroxide monohydrate / tetrahydrofuran; H2O / 20 °C View Scheme |
Conditions | Yield |
---|---|
Stage #1: ethyl bromoacetate; 4-chloro-phenol With potassium carbonate In dimethyl sulfoxide at 50℃; for 6h; Stage #2: With water; sodium hydroxide In acetone at 50℃; for 3h; Stage #3: With hydrogenchloride In water at 25℃; pH=1 - 2; |
Conditions | Yield |
---|---|
With iodine; acetic acid Einleiten von Chlor; | |
With phosphorus pentachloride Zersetzung des Reaktionsproduktes mit Wasser; | |
With sulfuryl dichloride |
2-(4-Chloro-phenoxy)-1-imidazol-1-yl-ethanone
A
4-Chlorophenoxyacetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium tert-butylate / tetrahydrofuran / 24 h / 20 °C 2: glucose dehydrogenase; D-glucose; YGL039w from saccharomyces cerevisiae; nicotinamide adenine dinucleotide phosphate / aq. acetate buffer / 1 h / 30 °C / pH 5 / Enzymatic reaction View Scheme |
2-(4-Chloro-phenoxy)-1-imidazol-1-yl-ethanone
A
4-Chlorophenoxyacetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium tert-butylate / tetrahydrofuran / 24 h / 20 °C 2: glucose dehydrogenase; D-glucose; SyADH from sphingobium yanoikuyae; nicotinamide adenine dinucleotide phosphate / aq. acetate buffer / 1 h / 30 °C / pH 5 / Enzymatic reaction View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: thionyl chloride; lead acetate; 2,3,4-trichlorothiophene / 0.5 h / 20 °C 2: sulfuric acid / 2 h / 80 °C View Scheme | |
Multi-step reaction with 2 steps 1: thionyl chloride; 2,3,4-trichlorothiophene / 0.5 h / 20 °C 2: sulfuric acid / 2 h / 80 °C View Scheme | |
Multi-step reaction with 2 steps 1: thionyl chloride; lead(IV) tetraacetate; 2,3,4-trichlorothiophene / 0.5 h / 20 °C 2: sulfuric acid / 2 h / 80 °C View Scheme | |
Multi-step reaction with 2 steps 1: thionyl chloride; lead(IV) tetraacetate; 2,3,4-trichlorothiophene / 0.5 h / 20 °C 2: sulfuric acid / 2 h / 80 °C View Scheme |
4-Chlorophenoxyacetic acid
Conditions | Yield |
---|---|
With sodium hydroxide; water Einleiten von Chlor; |
4-Chlorophenoxyacetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: zinc(II) chloride; bis(4-chlorophenyl)sulfide; sulfuryl dichloride / 0.5 h / 30 °C 2: phosphoric acid / 3 h / 120 °C View Scheme | |
Multi-step reaction with 2 steps 1: sulfuryl dichloride; / -20 °C / Large scale 2: phosphoric acid / 3 h / 120 °C / Large scale View Scheme | |
Multi-step reaction with 2 steps 1: sulfuryl dichloride; silica-supported ZnCl2 (30%); / -20 °C / Large scale 2: phosphoric acid / 3 h / 120 °C / Large scale View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: magnesium chloride; bis(4-chlorophenyl)sulfide; sulfuryl dichloride / 0.5 h / 30 °C 2: molybdenum(VI) oxide; oxygen / water / 80 °C / 750.08 Torr View Scheme |
meclofenoxate hydrochloride
A
4-Chlorophenoxyacetic acid
B
2-(N,N-dimethylamino)ethanol hydrochloride
Conditions | Yield |
---|---|
With water at 60℃; for 120h; Kinetics; educt as different commercial film coated tablets; var. temp.s, relative humidities, additives and reaction times; | |
With buffered to pH 3.9; water at 30℃; Rate constant; in the presence and absence of sodium bisulfite (SBS); | |
With water at 80℃; under 50 Torr; Rate constant; Kinetics; Mechanism; variation of humidity, temperature and pressure; |
2-phenoxyacetic acid
A
(2-chlorophenoxy)acetic acid
B
4-Chlorophenoxyacetic acid
Conditions | Yield |
---|---|
With 4-chloromorpholine In trifluoroacetic acid Ambient temperature; Yield given. Yields of byproduct given; |
2,4-Dichlorophenoxyacetic acid
A
4-Chlorophenoxyacetic acid
B
2-phenoxyacetic acid
Conditions | Yield |
---|---|
With tetraethylammonium bromide In acetonitrile at 20℃; Product distribution; var. cathode materials; | |
With 40 mA h; tetraethylammonium bromide In acetonitrile at 20℃; Product distribution; elecrolysis under various experimental conditions; | |
With current denisity 55 mA; tetraethylammonium bromide In dimethyl sulfoxide at 20℃; Product distribution; various reaction conditions and cathode nature; |
2,4-Dichlorophenoxyacetic acid
A
(2-chlorophenoxy)acetic acid
B
4-Chlorophenoxyacetic acid
C
2,4-dichlorophenol
Conditions | Yield |
---|---|
With water at 20℃; UV-irradiation; photodegradation; |
meclofenoxate hydrochloride
A
2-(N,N-dimethylamino)ethanol
B
4-Chlorophenoxyacetic acid
Conditions | Yield |
---|---|
With water In various solvent(s) at 25℃; for 8h; Rate constant; pH=5.5; effect of pH, buffer and human serum albumin concentration on hydrolysis; | |
With water Product distribution; Ambient temperature; in gastric medium; other medium; |
Conditions | Yield |
---|---|
In ethyl acetate |
Conditions | Yield |
---|---|
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane | 100% |
With thionyl chloride at 75℃; for 2h; | 94% |
With thionyl chloride In benzene for 3h; Reflux; | 91% |
4-Chlorophenoxyacetic acid
3-(2-ethoxy-phenyl)-7-nitro-2-(1-piperazin-1-yl-ethyl)-3H-quinazolin-4-one
2-(1-{4-[2-(4-chloro-phenoxy)-acetyl]-piperazin-1-yl}-ethyl)-3-(2-ethoxy-phenyl)-7-nitro-3H-quinazolin-4-one
Conditions | Yield |
---|---|
With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine In chloroform at 20℃; for 0.333333h; | 100% |
4-Chlorophenoxyacetic acid
Conditions | Yield |
---|---|
Stage #1: 4-Chlorophenoxyacetic acid; tert-butyl N-(1-amino-3-bicyclo[1.1.1]pentanyl)carbamate With triethylamine In dichloromethane at 0℃; for 0.0833333h; Stage #2: With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide In dichloromethane; ethyl acetate at 20℃; for 12h; | 100% |
Stage #1: 4-Chlorophenoxyacetic acid With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; triethylamine In dichloromethane; ethyl acetate at 0℃; for 0.166667h; Stage #2: tert-butyl N-(1-amino-3-bicyclo[1.1.1]pentanyl)carbamate In dichloromethane; ethyl acetate at 0 - 20℃; for 16h; | |
With 1-methyl-1H-imidazole; 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide In ethyl acetate; N,N-dimethyl-formamide at 20℃; for 4h; |
Conditions | Yield |
---|---|
99.5% | |
With sulfuric acid at 10 - 40℃; for 4 - 5h; | 73.8% |
With sulfuric acid at -5 - 50℃; for 58h; | 53.8% |
With sulfuric acid at -5 - 50℃; for 58h; | |
With sulfuric acid at 20℃; for 2h; |
Conditions | Yield |
---|---|
With iron(III) sulfate; bis[(2-pyridyl)methyl]amine In 1,2-dichloro-ethane at 20℃; for 12h; Inert atmosphere; Sealed tube; Irradiation; | 99% |
Conditions | Yield |
---|---|
With iron(III) sulfate; bis[(2-pyridyl)methyl]amine In 1,2-dichloro-ethane at 20℃; for 12h; Inert atmosphere; Sealed tube; Irradiation; | 99% |
Conditions | Yield |
---|---|
With iron(III) sulfate; bis[(2-pyridyl)methyl]amine In 1,2-dichloro-ethane at 20℃; for 12h; Inert atmosphere; Sealed tube; Irradiation; | 99% |
4-Chlorophenoxyacetic acid
3-phenyl-4-amino-5-mercapto-1,2,4-triazole
Conditions | Yield |
---|---|
With dmap; tetrabutylammomium bromide; trichlorophosphate Microwave irradiation; Heating; | 98% |
With trichlorophosphate for 4h; Heating; |
4-Chlorophenoxyacetic acid
Conditions | Yield |
---|---|
Stage #1: 4-Chlorophenoxyacetic acid With triethylamine In dichloromethane at 0℃; for 0.0833333h; Stage #2: With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide In dichloromethane; ethyl acetate at 0℃; for 0.166667h; Stage #3: 5-amino-2-azabicyclo[2.2.1]heptane-2-carboxylic acid tert-butyl ester In dichloromethane; ethyl acetate at 20℃; for 12h; | 98% |
4-Chlorophenoxyacetic acid
4-amino-5-mercapto-3-(4-chlorophenyl)-1,2,4-triazole
Conditions | Yield |
---|---|
With dmap; tetrabutylammomium bromide; trichlorophosphate Microwave irradiation; Heating; | 97% |
With trichlorophosphate for 4h; Heating; |
4-Chlorophenoxyacetic acid
4-amino-5-(3-fiuorophenyl)-2,4-dihydro-3H-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
With dmap; tetrabutylammomium bromide; trichlorophosphate Microwave irradiation; Heating; | 97% |
4-Chlorophenoxyacetic acid
4-amino-3,4-dihydro-6-phenyl-3-thioxo-1,2,4-triazin-5(2H)-one
Conditions | Yield |
---|---|
With trichlorophosphate for 5h; Condensation; Cyclization; Heating; | 96% |
4-amino-5-(pyridin-4-yl)-4H-1,2,4-triazole-3-thiol
4-Chlorophenoxyacetic acid
6-((4-chlorophenoxy)methyl)-3-(pyridin-4-yl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole
Conditions | Yield |
---|---|
With dmap; tetrabutylammomium bromide; trichlorophosphate Microwave irradiation; Heating; | 96% |
With trichlorophosphate for 1.5h; Reflux; | 90% |
With trichlorophosphate for 1.5h; Reflux; | 90% |
4-Chlorophenoxyacetic acid
triethanolamine
tris(2-hydroxyethyl)ammonium (4-chlorophenyloxy)acetate
Conditions | Yield |
---|---|
In ethanol | 95.8% |
In ethanol at 20 - 65℃; | 94% |
4-Chlorophenoxyacetic acid
4-amino-6-benzyl-3-mercapto-1,2,4-triazine-5(4H)-one
Conditions | Yield |
---|---|
With trichlorophosphate for 5h; Heating; | 95% |
4-Chlorophenoxyacetic acid
Conditions | Yield |
---|---|
With dmap; tetrabutylammomium bromide; trichlorophosphate Microwave irradiation; Heating; | 95% |
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 24h; | 95% |
Conditions | Yield |
---|---|
With magnesium sulfate In tetrahydrofuran; ethyl acetate | 94% |
4-Chlorophenoxyacetic acid
N,O-dimethylhydroxylamine*hydrochloride
N-methoxy-2-(4-chloro-phenoxy)-N-methyl-acetamide
Conditions | Yield |
---|---|
Stage #1: 4-Chlorophenoxyacetic acid With 1,1'-carbonyldiimidazole In dichloromethane at 0 - 23℃; Stage #2: N,O-dimethylhydroxylamine*hydrochloride With triethylamine In dichloromethane at 0 - 10℃; | 94% |
4-Chlorophenoxyacetic acid
4-amino-5-(4-methoxyphenyl)-4H-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
With dmap; tetrabutylammomium bromide; trichlorophosphate Microwave irradiation; Heating; | 94% |
4-Chlorophenoxyacetic acid
Conditions | Yield |
---|---|
With dmap; tetrabutylammomium bromide; trichlorophosphate Microwave irradiation; Heating; | 94% |
4-Chlorophenoxyacetic acid
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide at 20℃; for 3h; | 94% |
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; for 3h; | 94% |
With 2-(3H-[1,2,3]triazolo[4,5-b]pyridin-3-yl)-1,1,3,3-tetramethylisouronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 3h; | 94% |
With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide at 20℃; for 3h; | 94% |
4-Chlorophenoxyacetic acid
Conditions | Yield |
---|---|
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In 2-methyltetrahydrofuran; ethyl acetate at 0 - 80℃; for 17h; Inert atmosphere; | 94% |
Conditions | Yield |
---|---|
With iron(III) sulfate; bis[(2-pyridyl)methyl]amine In 1,2-dichloro-ethane at 20℃; for 12h; Catalytic behavior; Reagent/catalyst; Solvent; Inert atmosphere; Sealed tube; Irradiation; | 94% |
4-Chlorophenoxyacetic acid
4-cyanobenzylidenemalononitrile
Conditions | Yield |
---|---|
With iron(III) sulfate; bis[(2-pyridyl)methyl]amine In 1,2-dichloro-ethane at 20℃; for 12h; Inert atmosphere; Sealed tube; Irradiation; | 94% |