CAS No.125323-99-1,BOC-LYS(Z)(ISOPROPYL)-OH Suppliers

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BOC-LYS(Z)(ISOPROPYL)-OH CAS 125323-99-1

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Nalpha-Boc-Nepsilon-isopropyl-Nepsilon-z-L-lysine dicyclohexylammonium salt

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L-Lysine,N2-[(1,1-dimethylethoxy)carbonyl]-N6-(1-methylethyl)-N6-[(phenylmethoxy)carbonyl]-

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Boc-Lys(Z)(isopropyl)-OH (oil)125323-99-1

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Boc-Lys(Z)(isopropyl)-OH (oil)

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Synthetic route

: 66880-55-5
Nα-tert-butyloxycarbonyl-Nε-isopropyl-L-lysine

: 501-53-1
benzyl chloroformate

: 125323-99-1
Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine

Conditions

Conditions	Yield
With sodium hydroxide Ambient temperature; Yield given;

: 15761-39-4
1-(tert-butoxycarbonyl)-L-proline

: 13139-15-6
N-tert-butoxycarbonyl-L-leucine

: 108-24-7
acetic anhydride

: 125323-99-1
Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine

: 114346-31-5
(R)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid

Boc-D-Ala-OHBoc-D-2Nal-OH: Boc-D-Ala-OHBoc-D-2Nal-OH

: C83H106ClN19O16

Conditions

Conditions	Yield
Multistep reaction;	42 mg

...Expand

: 13139-15-6
N-tert-butoxycarbonyl-L-leucine

: 3744-87-4, 7764-95-6, 15761-38-3
Boc-(R)-Ala

: 23680-31-1
BOC-O-benzyl-L-serine

: 108-24-7
acetic anhydride

: 125323-99-1
Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine

Boc-Leu: Boc-Leu

Boc-Pro: Boc-Pro

: acyline

Conditions

Conditions	Yield
Multistep reaction.;

...Expand

: polyethylene glycol polyamide resin

: 15761-39-4
1-(tert-butoxycarbonyl)-L-proline

: 13139-15-6
N-tert-butoxycarbonyl-L-leucine

: 3744-87-4, 7764-95-6, 15761-38-3
Boc-(R)-Ala

: 23680-31-1
BOC-O-benzyl-L-serine

: 98266-33-2
Boc-DPal

: 57292-44-1
N-Boc-D-(4-Cl)Phe-OH

: 76985-10-9
Boc-D-2Nal-OH

: 125323-99-1
Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine

: 114346-31-5
(S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid

: Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine

acetylating agent: acetylating agent

: C107H120ClN16O17Pol

Conditions

Conditions	Yield
Stage #1: polyethylene glycol polyamide resin; Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide for 4h; MBHA resin; Stage #2: With trifluoroacetic acid In dichloromethane MBHA resin; Stage #3: 1-(tert-butoxycarbonyl)-L-proline; N-tert-butoxycarbonyl-L-leucine; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine; acetylating agent Further stages;

Yield

Stage #1: polyethylene glycol polyamide resin; Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide for 4h; MBHA resin;
Stage #2: With trifluoroacetic acid In dichloromethane MBHA resin;
Stage #3: 1-(tert-butoxycarbonyl)-L-proline; N-tert-butoxycarbonyl-L-leucine; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine; acetylating agent Further stages;

...Expand

: polyethylene glycol polyamide resin

: 15761-39-4
1-(tert-butoxycarbonyl)-L-proline

: 3744-87-4, 7764-95-6, 15761-38-3
Boc-(R)-Ala

: 23680-31-1
BOC-O-benzyl-L-serine

: 6404-28-0
Boc-Nle-OH

: 98266-33-2
Boc-DPal

: 57292-44-1
N-Boc-D-(4-Cl)Phe-OH

: 76985-10-9
Boc-D-2Nal-OH

: 125323-99-1
Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine

: 114346-31-5
(S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid

: Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine

acetylating agent: acetylating agent

: C107H120ClN16O17Pol

Conditions

Conditions	Yield
Stage #1: polyethylene glycol polyamide resin; Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide for 4h; MBHA resin; Stage #2: With trifluoroacetic acid In dichloromethane MBHA resin; Stage #3: 1-(tert-butoxycarbonyl)-L-proline; BOC-O-benzyl-L-serine; Boc-Nle-OH; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine; acetylating agent Further stages;

Yield

Stage #1: polyethylene glycol polyamide resin; Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide for 4h; MBHA resin;
Stage #2: With trifluoroacetic acid In dichloromethane MBHA resin;
Stage #3: 1-(tert-butoxycarbonyl)-L-proline; BOC-O-benzyl-L-serine; Boc-Nle-OH; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine; acetylating agent Further stages;

...Expand

: polyethylene glycol polyamide resin

: 15761-39-4
1-(tert-butoxycarbonyl)-L-proline

: 13139-16-7
N-(tert-butyloxycarbonyl)-L-isoleucine

: 3744-87-4, 7764-95-6, 15761-38-3
Boc-(R)-Ala

: 23680-31-1
BOC-O-benzyl-L-serine

: 98266-33-2
Boc-DPal

: 57292-44-1
N-Boc-D-(4-Cl)Phe-OH

: 76985-10-9
Boc-D-2Nal-OH

: 125323-99-1
Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine

: 114346-31-5
(S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid

: Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine

acetylating agent: acetylating agent

: C107H120ClN16O17Pol

Conditions

Conditions	Yield
Stage #1: polyethylene glycol polyamide resin; Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide for 4h; MBHA resin; Stage #2: With trifluoroacetic acid In dichloromethane MBHA resin; Stage #3: 1-(tert-butoxycarbonyl)-L-proline; N-(tert-butyloxycarbonyl)-L-isoleucine; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine; acetylating agent Further stages;

Yield

Stage #1: polyethylene glycol polyamide resin; Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide for 4h; MBHA resin;
Stage #2: With trifluoroacetic acid In dichloromethane MBHA resin;
Stage #3: 1-(tert-butoxycarbonyl)-L-proline; N-(tert-butyloxycarbonyl)-L-isoleucine; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine; acetylating agent Further stages;

...Expand

: polyethylene glycol polyamide resin

: 15761-39-4
1-(tert-butoxycarbonyl)-L-proline

: 13734-41-3
t-Boc-L-valine

: 3744-87-4, 7764-95-6, 15761-38-3
Boc-(R)-Ala

: 23680-31-1
BOC-O-benzyl-L-serine

: 98266-33-2
Boc-DPal

: 57292-44-1
N-Boc-D-(4-Cl)Phe-OH

: 76985-10-9
Boc-D-2Nal-OH

: 125323-99-1
Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine

: 114346-31-5
(S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid

: Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine

acetylating agent: acetylating agent

: C106H118ClN16O17Pol

Conditions

Conditions	Yield
Stage #1: polyethylene glycol polyamide resin; Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide for 4h; MBHA resin; Stage #2: With trifluoroacetic acid In dichloromethane MBHA resin; Stage #3: 1-(tert-butoxycarbonyl)-L-proline; t-Boc-L-valine; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine; acetylating agent Further stages;

Yield

Stage #1: polyethylene glycol polyamide resin; Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide for 4h; MBHA resin;
Stage #2: With trifluoroacetic acid In dichloromethane MBHA resin;
Stage #3: 1-(tert-butoxycarbonyl)-L-proline; t-Boc-L-valine; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine; acetylating agent Further stages;

...Expand

: polyethylene glycol polyamide resin

: 15761-39-4
1-(tert-butoxycarbonyl)-L-proline

: 3744-87-4, 7764-95-6, 15761-38-3
Boc-(R)-Ala

: 23680-31-1
BOC-O-benzyl-L-serine

: 98266-33-2
Boc-DPal

: 57292-44-1
N-Boc-D-(4-Cl)Phe-OH

: 76985-10-9
Boc-D-2Nal-OH

: 88950-64-5
1-<(tert-butyloxy)carbonylamino>cyclopropane-1-carboxylic acid

: 125323-99-1
Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine

: 114346-31-5
(S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid

: Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine

acetylating agent: acetylating agent

: C105H114ClN16O17Pol

Conditions

Conditions	Yield
Stage #1: polyethylene glycol polyamide resin; Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide for 4h; MBHA resin; Stage #2: With trifluoroacetic acid In dichloromethane MBHA resin; Stage #3: 1-(tert-butoxycarbonyl)-L-proline; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; 1-<(tert-butyloxy)carbonylamino>cyclopropane-1-carboxylic acid; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine; acetylating agent Further stages;

Yield

Stage #1: polyethylene glycol polyamide resin; Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide for 4h; MBHA resin;
Stage #2: With trifluoroacetic acid In dichloromethane MBHA resin;
Stage #3: 1-(tert-butoxycarbonyl)-L-proline; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; 1-<(tert-butyloxy)carbonylamino>cyclopropane-1-carboxylic acid; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine; acetylating agent Further stages;

...Expand

: polyethylene glycol polyamide resin

: 15761-39-4
1-(tert-butoxycarbonyl)-L-proline

: 2488-15-5
N-tert-butoxycarbonyl-L-methionine

: 3744-87-4, 7764-95-6, 15761-38-3
Boc-(R)-Ala

: 23680-31-1
BOC-O-benzyl-L-serine

: 98266-33-2
Boc-DPal

: 57292-44-1
N-Boc-D-(4-Cl)Phe-OH

: 76985-10-9
Boc-D-2Nal-OH

: 125323-99-1
Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine

: 114346-31-5
(S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid

: Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine

acetylating agent: acetylating agent

: C106H118ClN16O17PolS

Conditions

Conditions	Yield
Stage #1: polyethylene glycol polyamide resin; Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide for 4h; MBHA resin; Stage #2: With trifluoroacetic acid In dichloromethane MBHA resin; Stage #3: 1-(tert-butoxycarbonyl)-L-proline; N-tert-butoxycarbonyl-L-methionine; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine; acetylating agent Further stages;

Yield

Stage #1: polyethylene glycol polyamide resin; Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide for 4h; MBHA resin;
Stage #2: With trifluoroacetic acid In dichloromethane MBHA resin;
Stage #3: 1-(tert-butoxycarbonyl)-L-proline; N-tert-butoxycarbonyl-L-methionine; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine; acetylating agent Further stages;

...Expand

: polyethylene glycol polyamide resin

: 15761-39-4
1-(tert-butoxycarbonyl)-L-proline

: 3744-87-4, 7764-95-6, 15761-38-3
Boc-(R)-Ala

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 23680-31-1
BOC-O-benzyl-L-serine

: 98266-33-2
Boc-DPal

: 57292-44-1
N-Boc-D-(4-Cl)Phe-OH

: 76985-10-9
Boc-D-2Nal-OH

: 125323-99-1
Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine

: 114346-31-5
(S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid

: Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine

acetylating agent: acetylating agent

: C110H118ClN16O17Pol

Conditions

Conditions	Yield
Stage #1: polyethylene glycol polyamide resin; Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide for 4h; MBHA resin; Stage #2: With trifluoroacetic acid In dichloromethane MBHA resin; Stage #3: 1-(tert-butoxycarbonyl)-L-proline; N-tert-butoxycarbonyl-L-phenylalanine; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine; acetylating agent Further stages;

Yield

Stage #1: polyethylene glycol polyamide resin; Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide for 4h; MBHA resin;
Stage #2: With trifluoroacetic acid In dichloromethane MBHA resin;
Stage #3: 1-(tert-butoxycarbonyl)-L-proline; N-tert-butoxycarbonyl-L-phenylalanine; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine; acetylating agent Further stages;

...Expand

: polyethylene glycol polyamide resin

: 15761-39-4
1-(tert-butoxycarbonyl)-L-proline

: 3744-87-4, 7764-95-6, 15761-38-3
Boc-(R)-Ala

: 23680-31-1
BOC-O-benzyl-L-serine

: 98266-33-2
Boc-DPal

: 57292-44-1
N-Boc-D-(4-Cl)Phe-OH

: 76985-10-9
Boc-D-2Nal-OH

: 125323-99-1
Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine

: 114346-31-5
(S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid

: Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine

: 179412-79-4
(S)-3-((tert-butoxycarbonyl)amino)-4-methylpentanoic acid

acetylating agent: acetylating agent

: C107H120ClN16O17Pol

Conditions

Conditions	Yield
Stage #1: polyethylene glycol polyamide resin; Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide for 4h; MBHA resin; Stage #2: With trifluoroacetic acid In dichloromethane MBHA resin; Stage #3: 1-(tert-butoxycarbonyl)-L-proline; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine; (S)-3-((tert-butoxycarbonyl)amino)-4-methylpentanoic acid; acetylating agent Further stages;

Yield

Stage #1: polyethylene glycol polyamide resin; Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide for 4h; MBHA resin;
Stage #2: With trifluoroacetic acid In dichloromethane MBHA resin;
Stage #3: 1-(tert-butoxycarbonyl)-L-proline; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine; (S)-3-((tert-butoxycarbonyl)amino)-4-methylpentanoic acid; acetylating agent Further stages;

...Expand

: polyethylene glycol polyamide resin

: 15761-39-4
1-(tert-butoxycarbonyl)-L-proline

: 3744-87-4, 7764-95-6, 15761-38-3
Boc-(R)-Ala

: 23680-31-1
BOC-O-benzyl-L-serine

: 98266-33-2
Boc-DPal

: 57292-44-1
N-Boc-D-(4-Cl)Phe-OH

: 76985-10-9
Boc-D-2Nal-OH

: 125323-99-1
Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine

: 114346-31-5
(S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid

: 52-52-8
1-amino-1-cyclopentanecarboxylic acid

: Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine

acetylating agent: acetylating agent

: C107H118ClN16O17Pol

Conditions

Conditions	Yield
Stage #1: polyethylene glycol polyamide resin; Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide for 4h; MBHA resin; Stage #2: With trifluoroacetic acid In dichloromethane MBHA resin; Stage #3: 1-(tert-butoxycarbonyl)-L-proline; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; 1-amino-1-cyclopentanecarboxylic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine; acetylating agent Further stages;

Yield

Stage #1: polyethylene glycol polyamide resin; Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide for 4h; MBHA resin;
Stage #2: With trifluoroacetic acid In dichloromethane MBHA resin;
Stage #3: 1-(tert-butoxycarbonyl)-L-proline; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; 1-amino-1-cyclopentanecarboxylic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine; acetylating agent Further stages;

...Expand

: polyethylene glycol polyamide resin

: 15761-39-4
1-(tert-butoxycarbonyl)-L-proline

: 3744-87-4, 7764-95-6, 15761-38-3
Boc-(R)-Ala

: 2756-85-6
1-aminocyclohexane carboxylic acid

: 23680-31-1
BOC-O-benzyl-L-serine

: 98266-33-2
Boc-DPal

: 57292-44-1
N-Boc-D-(4-Cl)Phe-OH

: 76985-10-9
Boc-D-2Nal-OH

: 125323-99-1
Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine

: 114346-31-5
(S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid

: Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine

acetylating agent: acetylating agent

: C108H120ClN16O17Pol

Conditions

Conditions	Yield
Stage #1: polyethylene glycol polyamide resin; Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide for 4h; MBHA resin; Stage #2: With trifluoroacetic acid In dichloromethane MBHA resin; Stage #3: 1-(tert-butoxycarbonyl)-L-proline; 1-aminocyclohexane carboxylic acid; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine; acetylating agent Further stages;

Yield

Stage #1: polyethylene glycol polyamide resin; Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide for 4h; MBHA resin;
Stage #2: With trifluoroacetic acid In dichloromethane MBHA resin;
Stage #3: 1-(tert-butoxycarbonyl)-L-proline; 1-aminocyclohexane carboxylic acid; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine; acetylating agent Further stages;

...Expand

: polyethylene glycol polyamide resin

: 15761-39-4
1-(tert-butoxycarbonyl)-L-proline

: 3744-87-4, 7764-95-6, 15761-38-3
Boc-(R)-Ala

: 23680-31-1
BOC-O-benzyl-L-serine

: 98266-33-2
Boc-DPal

: 57292-44-1
N-Boc-D-(4-Cl)Phe-OH

: 76985-10-9
Boc-D-2Nal-OH

: 125323-99-1
Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine

: 114346-31-5
(S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid

: Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine

acetylating agent: acetylating agent

Boc-Thr(pg)-OH: Boc-Thr(pg)-OH

: C105H116ClN16O18Pol

Conditions

Conditions	Yield
Stage #1: polyethylene glycol polyamide resin; Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide for 4h; MBHA resin; Stage #2: With trifluoroacetic acid In dichloromethane MBHA resin; Stage #3: 1-(tert-butoxycarbonyl)-L-proline; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine; acetylating agent; Boc-Thr(pg)-OH Further stages;

Yield

Stage #1: polyethylene glycol polyamide resin; Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide for 4h; MBHA resin;
Stage #2: With trifluoroacetic acid In dichloromethane MBHA resin;
Stage #3: 1-(tert-butoxycarbonyl)-L-proline; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine; acetylating agent; Boc-Thr(pg)-OH Further stages;

...Expand

: polyethylene glycol polyamide resin

: 15761-39-4
1-(tert-butoxycarbonyl)-L-proline

: 3744-87-4, 7764-95-6, 15761-38-3
Boc-(R)-Ala

: 23680-31-1
BOC-O-benzyl-L-serine

: 98266-33-2
Boc-DPal

: 57292-44-1
N-Boc-D-(4-Cl)Phe-OH

: 76985-10-9
Boc-D-2Nal-OH

: 125323-99-1
Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine

: 114346-31-5
(S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid

: 194206-80-9
Boc-Nleu-OH

: Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine

acetylating agent: acetylating agent

: C107H120ClN16O17Pol

Conditions

Conditions	Yield
Stage #1: polyethylene glycol polyamide resin; Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide for 4h; MBHA resin; Stage #2: With trifluoroacetic acid In dichloromethane MBHA resin; Stage #3: 1-(tert-butoxycarbonyl)-L-proline; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Boc-Nleu-OH; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine; acetylating agent Further stages;

Yield

Stage #1: polyethylene glycol polyamide resin; Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide for 4h; MBHA resin;
Stage #2: With trifluoroacetic acid In dichloromethane MBHA resin;
Stage #3: 1-(tert-butoxycarbonyl)-L-proline; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Boc-Nleu-OH; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine; acetylating agent Further stages;

...Expand

: 15761-39-4
1-(tert-butoxycarbonyl)-L-proline

: 13139-15-6
N-tert-butoxycarbonyl-L-leucine

: 3744-87-4, 7764-95-6, 15761-38-3
Boc-(R)-Ala

: 27144-18-9
3-(tritylthio) propanoic acid

: 23680-31-1
BOC-O-benzyl-L-serine

: 98266-33-2
Boc-DPal

: 57292-44-1
N-Boc-D-(4-Cl)Phe-OH

: 76985-10-9
Boc-D-2Nal-OH

: 125323-99-1
Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine

: 114346-31-5
(S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid

: 5988-19-2
L-dihydroorotic acid

: Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine

: Mer-D-Nal-D-Cpa-D-Pal-Ser-Aph(L-Hor)-D-Aph(Cbm)-Leu-ILys-Pro-D-Ala-NH2

Conditions

Conditions	Yield
Stage #1: Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide In N,N-dimethyl-formamide for 4h; Stage #2: With trifluoroacetic acid In dichloromethane for 0.416667h; Stage #3: 1-(tert-butoxycarbonyl)-L-proline; N-tert-butoxycarbonyl-L-leucine; 3-(tritylthio) propanoic acid; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; L-dihydroorotic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine Further stages;

Yield

Stage #1: Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide In N,N-dimethyl-formamide for 4h;
Stage #2: With trifluoroacetic acid In dichloromethane for 0.416667h;
Stage #3: 1-(tert-butoxycarbonyl)-L-proline; N-tert-butoxycarbonyl-L-leucine; 3-(tritylthio) propanoic acid; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; L-dihydroorotic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine Further stages;

...Expand

: 15761-39-4
1-(tert-butoxycarbonyl)-L-proline

: 13139-15-6
N-tert-butoxycarbonyl-L-leucine

: 3744-87-4, 7764-95-6, 15761-38-3
Boc-(R)-Ala

: 27144-18-9
3-(tritylthio) propanoic acid

: 23680-31-1
BOC-O-benzyl-L-serine

: 98266-33-2
Boc-DPal

: 57292-44-1
N-Boc-D-(4-Cl)Phe-OH

: 76985-10-9
Boc-D-2Nal-OH

: 125323-99-1
Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine

: 114346-31-5
(S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid

: 5988-19-2
L-dihydroorotic acid

: Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine

: Ac-D-Nal-D-Cpa-D-Pal-Ser-Aph(L-Hor)-D-Aph(Mer)-Leu-ILys-Pro-D-Ala-NH2

Conditions

Conditions	Yield
Stage #1: Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide In N,N-dimethyl-formamide for 4h; Stage #2: With trifluoroacetic acid In dichloromethane for 0.416667h; Stage #3: 1-(tert-butoxycarbonyl)-L-proline; N-tert-butoxycarbonyl-L-leucine; 3-(tritylthio) propanoic acid; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; L-dihydroorotic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine Further stages;

Yield

...Expand

: 15761-39-4
1-(tert-butoxycarbonyl)-L-proline

: 13139-15-6
N-tert-butoxycarbonyl-L-leucine

: 3744-87-4, 7764-95-6, 15761-38-3
Boc-(R)-Ala

: 27144-18-9
3-(tritylthio) propanoic acid

: 23680-31-1
BOC-O-benzyl-L-serine

: 98266-33-2
Boc-DPal

: 57292-44-1
N-Boc-D-(4-Cl)Phe-OH

: 76985-10-9
Boc-D-2Nal-OH

: 71989-20-3
N2-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-glutamine

: 125323-99-1
Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine

: 114346-31-5
(S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid

: Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine

: 5988-19-2
L-dihydroorotic acid

: Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine

: Ac-D-Nal-D-Cpa-D-Pal-Ser-Aph(L-Hor)-D-Aph(-Arg-Gln-Mer)-Leu-ILys-Pro-D-Ala-NH2

Conditions

Conditions	Yield
Stage #1: Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide In N,N-dimethyl-formamide for 4h; Stage #2: With trifluoroacetic acid In dichloromethane for 0.416667h; Stage #3: 1-(tert-butoxycarbonyl)-L-proline; N-tert-butoxycarbonyl-L-leucine; 3-(tritylthio) propanoic acid; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; N2-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-glutamine; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine; L-dihydroorotic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine Further stages;

Yield

Stage #1: Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide In N,N-dimethyl-formamide for 4h;
Stage #2: With trifluoroacetic acid In dichloromethane for 0.416667h;
Stage #3: 1-(tert-butoxycarbonyl)-L-proline; N-tert-butoxycarbonyl-L-leucine; 3-(tritylthio) propanoic acid; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; N2-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-glutamine; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine; L-dihydroorotic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine Further stages;

...Expand

: 15761-39-4
1-(tert-butoxycarbonyl)-L-proline

: 13139-15-6
N-tert-butoxycarbonyl-L-leucine

: 3744-87-4, 7764-95-6, 15761-38-3
Boc-(R)-Ala

: 27144-18-9
3-(tritylthio) propanoic acid

: 23680-31-1
BOC-O-benzyl-L-serine

: 98266-33-2
Boc-DPal

: 57292-44-1
N-Boc-D-(4-Cl)Phe-OH

: 76985-10-9
Boc-D-2Nal-OH

: 71989-20-3
N2-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-glutamine

: 125323-99-1
Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine

: 114346-31-5
(S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid

: Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine

: 5988-19-2
L-dihydroorotic acid

: Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine

: Mer-Gln-Arg-D-Nal-D-Cpa-D-Pal-Ser-Aph(L-Hor)-D-Aph(Cbm)-Leu-ILys-Pro-D-Ala-NH2

Conditions

Conditions	Yield
Stage #1: Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide In N,N-dimethyl-formamide for 4h; Stage #2: With trifluoroacetic acid In dichloromethane for 0.416667h; Stage #3: 1-(tert-butoxycarbonyl)-L-proline; N-tert-butoxycarbonyl-L-leucine; 3-(tritylthio) propanoic acid; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; N2-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-glutamine; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine; L-dihydroorotic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine Further stages;

Yield

Stage #1: Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide In N,N-dimethyl-formamide for 4h;
Stage #2: With trifluoroacetic acid In dichloromethane for 0.416667h;
Stage #3: 1-(tert-butoxycarbonyl)-L-proline; N-tert-butoxycarbonyl-L-leucine; 3-(tritylthio) propanoic acid; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; N2-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-glutamine; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine; L-dihydroorotic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine Further stages;

...Expand

: 15761-39-4
1-(tert-butoxycarbonyl)-L-proline

: 13139-15-6
N-tert-butoxycarbonyl-L-leucine

: 3744-87-4, 7764-95-6, 15761-38-3
Boc-(R)-Ala

: 27144-18-9
3-(tritylthio) propanoic acid

: 23680-31-1
BOC-O-benzyl-L-serine

: 98266-33-2
Boc-DPal

: 57292-44-1
N-Boc-D-(4-Cl)Phe-OH

: 76985-10-9
Boc-D-2Nal-OH

: 71989-20-3
N2-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-glutamine

: 125323-99-1
Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine

: 114346-31-5
(S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid

: Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine

: 5988-19-2
L-dihydroorotic acid

: Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine

: Mer-Gln-Arg-D-Nal-D-Cpa-D-Pal-Ser-Aph(L-Hor)-D-Aph(-Arg-Gln-Mer)-Leu-ILys-Pro-D-Ala-NH2

Conditions

Conditions	Yield
Stage #1: Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide In N,N-dimethyl-formamide for 4h; Stage #2: With trifluoroacetic acid In dichloromethane for 0.416667h; Stage #3: 1-(tert-butoxycarbonyl)-L-proline; N-tert-butoxycarbonyl-L-leucine; 3-(tritylthio) propanoic acid; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; N2-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-glutamine; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine; L-dihydroorotic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine Further stages;

Yield

Stage #1: Boc-(R)-Ala With benzotriazol-1-ol; diisopropyl-carbodiimide In N,N-dimethyl-formamide for 4h;
Stage #2: With trifluoroacetic acid In dichloromethane for 0.416667h;
Stage #3: 1-(tert-butoxycarbonyl)-L-proline; N-tert-butoxycarbonyl-L-leucine; 3-(tritylthio) propanoic acid; BOC-O-benzyl-L-serine; Boc-DPal; N-Boc-D-(4-Cl)Phe-OH; Boc-D-2Nal-OH; N2-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-glutamine; Nα-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-Nε-isopropyl-L-lysine; (S)-3-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)phenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid; Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine; L-dihydroorotic acid; Nα-(tert-butyloxycarbonyl)-p-ureido-D-phenylalanine Further stages;

...Expand

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